水銀分析マニュアル
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1 1960 P197PHg nm UV HgP0P 3 1 HgP2+P nm L/ ng 50 ml 10
2 (10 cm ) HNOB3B HClOB4B HB2BSOB4B P 1)
3 a HNOB3B HClOB4B ml 100 ml HB2BSOB4B HCl 10% SnClB2B 10 g HCl 9 ml 100 ml NB2B 100 ml/min N NaOH 20 g 100 ml 0.1N NaOH 5N NaOH % L L HSCHB2BCH(NHB2B)COOH HCl HB2BO 10 mg 0.1N NaOH 10 ml P 2)P CHB3BHgCl 12.5 mg 100 ml ml 1.0 µg Hg 0.5 ml 0.1% L 5 ml 10 ml rpm ml 0.1 µg Hg 1N HB2BSOB4B30 ml 1000 ml 1% KMnOB4B 1 g 1N HB2BSOB4B 100 ml 0.5% KMnOB4B 0.5 g 100 ml CB6BHB5BCHB3B b Hg P 3)P 50 ml 150 mm 13 mm 10, ml 0.2, 0.5, 1, 5 10 ml 12
4 20 ml 10 ml V4 0.5% KMnOB4B KMnOB4B c 0.5 g 0.1 g 0.5 ml 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml 1 2 ml 4 P P 0.10 µg Hg/ml ml Hg 0.10 µg 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml d V ml 5 ml 20 ml 10% SnClB2B 1 ml P 5)P 13
5 V ml 5 ml 20 ml P 6)P mm Pbl, Pstd PsP 7)P µg /g = 0.10 µg (Ps-Pbl)/(Pstd-Pbl) 1/ (g) ng/g or ml = 100 ng (Ps-Pbl)/(Pstd-Pbl) 1/ (g or ml) 1 Hg 201 2II 1 ppm II 13.5 mg 100 ml HNOB3B HClOB4B ml HB2BSOB4B 10 ml 1 ml 100 µg Hg ml 0.10 µg Hg 3 21 mm 200 mm 4 HNOB3B HClOB4B
6 µg Hg/50 ml g 10 mg, 1 ml HNOB3B HClOB4B 1 1, 2 ml HB2BSOB4B, 5 ml , ml 5 ml 10% SnClB2B, 1 ml AAS U 1 U U 15
7 HNOB3B HClOB4B 1 1, 2 ml HB2BSOB4B, 5 ml 2 ml , ml, 5 ml 10% SnClB2B, 1 ml AAS U 2U 16
8 3 1 2 mg ml a CHB3BCOCHB3B CB2BHB5BOH HNOB3B HClOB4B ml 100 ml HB2BSOB4B HCl 10% SnClB2B 10 g HCl 9 ml 100 ml NB2B 100 ml/min N NaOH 20 g 100 ml 0.1N NaOH 5N NaOH % L L HSCHB2BCH(NHB2B)COOH HCl HB2BO 10 mg 0.1N NaOH 10 ml CHB3BHgCl 12.5 mg 100 ml ml 1.0 µg Hg 0.5 ml 0.1% L 5 ml 10 ml rpm ml 0.1 µg Hg 1N HB2BSOB4B30 ml 1000 ml 1% KMnOB4B 1 g 1N HB2BSOB4B 100 ml 0.5% KMnOB4B 0.5 g 100 ml CB6BHB5BCHB3B 17
9 b Hg ml 150 mm 13 mm 10, ml 0.2, 0.5, 1, 5 10 ml 20 ml 10 ml V4 0.5% KMnOB4B KMnOB4B c 10 mg 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml ng Hg/ml ml Hg 100 ng 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml d V ml 5 ml 20 ml 10% SnClB2B 1 ml
10 V ml 5 ml 20 ml mm Pbl, Pstd Ps ng/mg = 100 ng (Ps-Pbl)/(Pstd-Pbl) 1/ (mg) 0.5 g 10 mg, 1 ml HNOB3B HClOB4B 1 1, 2 ml HB2BSOB4B, 5 ml , ml 5 ml 10% SnClB2B, 1 ml AAS U 1 UU 19
11 mm a HNOB3B HClOB4B ml 100 ml HB2BSOB4B HCl 10% SnClB2B 10 g HCl 9 ml 100 ml NB2B 100 ml/min N NaOH 20 g 100 ml 0.1N NaOH 5N NaOH % L L HSCHB2BCH(NHB2B)COOH HCl HB2BO 10 mg 0.1N NaOH 10 ml CHB3BHgCl 12.5 mg 100 ml ml 1.0 µg Hg 0.5 ml 0.1% L 5 ml 10 ml rpm ml 0.1 µg Hg 1N HB2BSOB4B30 ml 1000 ml 1% KMnOB4B 1 g 1N HB2BSOB4B 100 ml 0.5% KMnOB4B 0.5 g 100 ml CB6BHB5BCHB3B b Hg
12 50 ml 150 mm 13 mm 10, ml 0.2, 0.5, 1, 5 10 ml 10 ml V4 0.5% KMnOB4B KMnOB4B c 0.5 g 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml µg Hg/ml ml Hg 0.10 µg 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml g / WW/DW d V ml 5 ml 20 ml 10% SnClB2B 1 ml
13 V ml 5 ml 20 ml mm Pbl, Pstd Ps µg/g µg/g =0.10 µg (Ps-Pbl)/(Pstd-Pbl) 1/ (g) WW/DW WW/DW/ 0.5 g 10 mg, 1 ml HNOB3B HClOB4B 1 1, 2 ml HB2BSOB4B, 5 ml , ml 5 ml AAS 10% SnClB2B, 1 ml U 1 UU 22
14 3 1 4 P 1)P 0.45 µm a HNOB3B HClOB4B ml 100 ml HB2BSOB4B HCl 10% SnClB2B 10 g HCl 9 ml 100 ml NB2B 100 ml/min N NaOH 20 g 100 ml 0.1N NaOH 5N NaOH % P 2)P 200 ml CB6BHB5BN:NCSNHNHCB6BHB5B g 100 ml 0.1N NaOH 50 ml 1N HCl 100 ml 0.01% 0.1% L L HSCHB2BCH(NHB2B)COOH HCl HB2BO 10 mg 0.1N NaOH 10 ml CHB3BHgCl 12.5 mg 100 ml ml 1.0 µg Hg 0.5 ml 0.1% L 5 ml 10 ml rpm ml 0.1 µg Hg 1N HB2BSOB4B30 ml 1000 ml 1% KMnOB4B 1 g 1N HB2BSOB4B 100 ml 0.5% KMnOB4B 0.5 g 100 ml 23
15 20N HB2BSOB4B 1L 350 ml 600 ml 1000 ml 10N NaOH 400 g 1000 ml 10% NHB2BOH HCl 10 g 100 ml 10% EDTA CB10BHB12BNB2BOB8BNaB4B 4HB2BO 10 g 100 ml CB6BHB5BCHB3B b Hg ml 150 mm 13 mm 10, ml 0.2, 0.5, 1, 5 10 ml 2L 10 ml V4 0.5% KMnOB4B KMnOB4B c 2L 2L20N HB2BSOB4 B10 ml 0.5% KMnOB4B 5 ml 5 10N NaOH 20 ml 10% NHB2BOH HCl 5 ml 20 P 3)P 10% EDTA 5 ml 0.01% 10 ml ml 1200 rpm g 24
16 7 ml 60 1 ml HNOB3B HClOB4B ml HB2BSOB4B 5 ml L 100 ng Hg/ml ml Hg 20 ng d V ml 10 ml 20 ml 10% SnClB2B 1 ml V ml 10 ml 20 ml mm Pbl Pstd Ps Hg ng/l 20 ng (Ps-Pbl)/(Pstd-Pbl) 1/(L) 1 ng/l 25
17 2 3 ClP P ClP PClB2B ClB2B 5 20 EDTA P
18 2L 2L 20N HB2BSOB4B 10 ml 0.5% KMnOB4B 5 ml5 10N NaOH 20 ml 10% NHB2BOH HCl 5 ml20 10% EDTA 5 ml 0.01%, 10 ml 1 10 ml NaB2BSOB4B 0.5 g 1200 rpm, 3 7 ml, 1 ml HNOB3B HClOB4B 1 1, 2 ml HB2BSOB4B, 5 ml , ml, 10 ml 10% SnClB2B, 1 ml AAS U 3U 27
水銀分析マニュアル
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10 12 A 12 C 12 13 13 13 13 16 16 18 18 18 23 23 23 23 23 A 24 25 25 26 28 28 30 32 38 38 41 42 43 10 43 11 45 48 48 120g 51 52 12 3 12 3 350g 120g 1 7 10 260g 90g 90g 30g 9 11 2 gg1 g 1 120g 10 1 12 6
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24 11 10 24 12 10 30 1 0.45m1.00m 1.00m 1.00m 0.33m 0.33m 0.33m 0.45m 1.00m 2 23% 29% 71% 67% 6% 4% n=1525 n=1137 6% +6% -4% -2% 21% 30% 5% 35% 6% 6% 11% 40% 37% 36 172 166 371 213 226 177 54 382 704 216
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3--2-3-Iodo-2-propynyl butylcarbamate (IPBC) Carbamic acid, butyl-, 3-iodo-2-propynyl ester Iodocarb CAS 55406-53-6 C 8 H 12 NO 2 I C (g/cm 3 ) (mmhg) log P ow 281.09 (280.9910) 64 68 1.51 1.57 (20 C)
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HPLC 1M KH 2 PO 4 ph ml Anthranilic acid: AnA 600 ml ml AnA 1.0 ml / min Anthranilic acid= PRESSURE 140 kgf / cm 2
15 10-1-3. 1. HPLC 1M KH 2 PO 4 ph 3.0 50 ml Anthranilic acid: AnA 600 ml 1-1. 350 ml AnA 1.0 ml / min Anthranilic acid=137.14 PRESSURE140 kgf / cm 2 TOSOH TSK-GEL ODS- 80 Ts 1) mg / ml AnA in (φ4.6 250
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第18回海岸シンポジウム報告書
2011.6.25 2011.6.26 L1 2011.6.27 L2 2011.7.6 2011.12.7 2011.10-12 2011.9-10 2012.3.9 23 2012.4, 2013.8.30 2012.6.13 2013.9 2011.7-2011.12-2012.4 2011.12.27 2013.9 1m30 1 2 3 4 5 6 m 5.0m 2.0m -5.0m 1.0m
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1 1 36 223 42 14 92 4 3 2 1 4 3 4 3429 13536 5 6 7 8 9 2.4m/ (M) (M) (M) (M) (M) 6.67.3 6.57.2 6.97.6 7.27.8 8.4 5 6 5 6 5 5 74 1,239 0 30 21 ( ) 1,639 3,898 0 1,084 887 2 5 0 2 2 4 22 1 3 1 ( :) 426 1500
1 C 2 C 3 C 4 C 1 C 2 C 3 C
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平成２４年財政投融資計画ＰＤＦ出後８／０１６‐０３０
24 23 28,707,866 2,317,737 26,390,129 29,289,794 2,899,665 24 23 19,084,525 21,036,598 1952,073 24 23 8,603,613 8,393,427 967,631 925,404 202,440 179,834 217,469 219,963 66,716 64,877 3,160,423 2,951,165
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1 2 http://www.japan-shop.jp/ 3 4 http://www.japan-shop.jp/ 5 6 http://www.japan-shop.jp/ 7 2,930mm 2,700 mm 2,950mm 2,930mm 2,950mm 2,700mm 2,930mm 2,950mm 2,700mm 8 http://www.japan-shop.jp/ 9 10 http://www.japan-shop.jp/
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1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 ( ) 24 25 26 27 28 29 30 ( ) ( ) ( ) 31 32 ( ) ( ) 33 34 35 36 37 38 39 40 41 42 43 44 ) i ii i ii 45 46 47 2 48 49 50 51 52 53 54 55 56 57 58
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i ii (1) (1) (2) (1) (3) (1) (1) (2) (1) (3) (1) (1) (2) (1) (3) (2) (3) (1) (2) (3) (1) (1) (1) (1) (2) (1) (3) (1) (2) (1) (3) (1) (1) (1) (2) (1) (3) (1) (1) (2) (1) (3)
23 15961615 1659 1657 14 1701 1711 1715 11 15 22 15 35 18 22 35 23 17 17 106 1.25 21 27 12 17 420,845 23 32 58.7 32 17 11.4 71.3 17.3 32 13.3 66.4 20.3 17 10,657 k 23 20 12 17 23 17 490,708 420,845 23
平成１８年度「商品先物取引に関する実態調査」報告書
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( ) M5, 2007 67.3 67.3 N=97 34.9 34.9 N=97 PBL- PBL- () PBL- PBL- 48.1 48.1 N=97 86.9 86.9 N=97 36.2 36.2 N=97 55.6 55.6 N=97 M5, 2007 N=101 CBT r 0.146 PBL- 4%2% 7% 5% 2% 5% 9% 66% N=82 : 1020 : 301 :
2
1 3 11 21 2 3 28 42 33 12 31 11 4 21 46.5 30.0vol 30 36 16 DXNs 46 19 B 42 22 5 0.44 10 15 20 20 1.5 1.5 0.1 0.37 6 4.5 1.7 16 1.5 1.5 4.5 1.5 7 3.6 4.4 12 8 1.5 9 46 19 19 10 500ml 11 33 3.6 3.9 12 2.1
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2 (FDA) 1 1 A D E K 1 LC UV 15 HPLC 3.5 UHPLC Agilent 12 Infinity LC Agilent 12 Infinity (G1311B) Agilent 12 Infinity (G13E) Agilent 12 Infinity (G131
1 Agilent 12 Infinity 1 Siji Joseph Agilent Technologies, Inc. Bangalore, India 12 1 2 4 5 3 2 1 4 1 12 14 4 2 Agilent 12 Infinity 2 4 5 3 2.5 1. 1.5 2. 2.5 3. 2 (RP-HPLC) Agilent Poroshell EC-C1 Agilent
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2002 (1) (2) (3) (4) (5) (1) (2) (3) (4) (5) (1) (2) (3) (4) (5) (6) (7) (8) (1) (2) (3) (4) (1) (2) (3) (4) (5) (6) (7) (8) No 2,500 3 200 200 200 200 200 50 200 No, 3 1 2 00 No 2,500 200 7 2,000 7