The Behaviors of Gluconic Acid Derivative in Hydration of CaO EAl2O3 Naomitsu TSUYUKI, Osamu HISASHI*, Tsugio MIYAKAWA and Junichi KASAI** Department
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1 The Behaviors of Gluconic Acid Derivative in Hydration of CaO EAl2O3 Naomitsu TSUYUKI, Osamu HISASHI*, Tsugio MIYAKAWA and Junichi KASAI** Department of Chemistry, College of Science and Technology, Nihon University , Narashinodai, Funabashi-shi 274 Central Research Laboratory, Kowa Chemical Industry Co., Ltd. Department of Industrial Chemistry, College of Industrial Technology, Nihon University The hydration of cements with additives were often changed remarkably by the added amounts. Authors studied the hydration of CaO EAl2O3 in the presence of calcium 2-oxo gluconate, whic hhave two functional groups of -COON and -C=O. When this compound was dissolved in Ca(OH)2 solution, Ca-complex was formed in some cases, and Ca-coprecipitate in other cases. The process is given as reaction formula (3). The hydration of CaO EAl2O3 dispersed in admixture solution at 25 Ž proceeded in three different ways (Types A, B and C) according to the admixture concentration. Anyhow, to be common with initial hydration stage passes into as follows; inherent effluent of calcium and aluminium from CaO EAl2O3 formation of Ca-complex production of Ca-coprecipitate. Above process is an application of formula (3). These differences were supposed to be caused by the different quantities of reacted calcium and aluminium. The setting time was determined by the retention period of effluent phenomenon or the formation of Ca-complex, when admixture concentration was lower. And coprecipitate was formed as the coating on CaO Al2O3 surface at higher concentration. Consequently, the states is classified into three ways such as the extremely thin coating of coprecipitate or the detaching phenomenon of coating or the stable thicker coating of grape state. These hydration model was illustrated in Fig. 12. Ca-complex is stable (1:1) complex in liquid phase. On the other hand, Ca-coprecipitate is amorphous substance, it is not simply Ca-salt of 2-oxogluconate. The gel in hardened bodies using this admixture has been induced by the formation of Ca-complex given as formula (3), its
2 Key-words: CaO-Al2O3, Gluconic acid derivative, Cement admixture Ca-complex, Ca-coprecipitate, Setting retardation,
3 Fig. 2. Calcium 2-oxogluconate 0wt%. Fig. 3. Calcium 2-oxogluconate 0.1wt%. Fig. 1. The solubility of total [Ca(OH)2] ( ) in aqueous solution of calcium 2-oxogluconate involved Ca(OH)2 and ph of the solution ( œ) as a function of concentration of calcium 2 oxogluconate, at 25 Ž. Fig. 4. Calcium 2-oxogluconate 0.3wt%.
4 Fig. 5. Calcium 2-oxogluconate 0.5wt%. Fig. 8. IR spectra of (1) calcium 2-oxogluco nate and (2) Ca-complex of Ca(OH)2-calcium 2-oxogluconate system. Fig. 6. Calcium 2-oxogluconate 1.0wt%. Fig. 7. Calcium 2-oxogluconate 2.0wt%.
5 Fig. 10. The changes of X-ray powder diffrac tion intensity of anhydrous CA in solid phase of CA-calcium 2-oxogluconate system as a function of hydra
![476 Yogyo-Kyokai-Shi 89 [9] 1981 N. TSUYUKI (1) (2) (3) 3h 1h 3h 1 day 8h 1 day 5 days Fig. 11.](/docs-images/94/121300936/images/6-0.jpg "various 1 day Scanning hydration electron times, at (1) Type A: calcium (3) Type C: calcium 過 程 で-COOH基 micrographs ビ ノー ス とCO2と 2-oxogluconate 0.")
6 476 Yogyo-Kyokai-Shi 89 [9] 1981 N. TSUYUKI (1) (2) (3) 3h 1h 3h 1 day 8h 1 day 5 days Fig. 11. various 1 day Scanning hydration electron times, at (1) Type A: calcium (3) Type C: calcium 過 程 で-COOH基 micrographs ビ ノー ス とCO2と 2-oxogluconate 0.1wt% 2-oxogluconate が 起 こ りや す い に分 解 す る こ とが知 られ てい る21). 液 中 にCAを 分 散 させ ら溶 出 され る カル シ ウム分 に も適 用 で き る. す なわ ち, アル カ リ性 の 条 件 で あれ ばCa錯 成, Ca共 4.2 体 の形 沈 体 の 生成 は 可 能 で あ る. り, 純 水 中 にCAを 分 散 させ た場 合 の 曲線 は水 求 め た結 果, 極 大 現 象 が 終 了 し た 時 点 で, 2CaO Al2O3 8H2O 記 す) 水 和 物 の生 成 が ほ ぼ完 了 す る と考 え られ る. (2) Type 2-oxogluconate system in B: calcium 2-oxogluconate 1.0wt% 潜 在 的 溶 出 とい う) され る カル シ ウ ム分 もア ル カ リ性 の 条 件 でCa錯 体 を 形成 す る と考 え られ る. しか し, CA か らの溶 出 カ ル シ ウ ム分 が 増 加 す る と, 4.1節 に述 べ たCa共 な現 象 を基 に して, 図3 図7に と, Ca KGの (2) 項 沈 体 が 生 成 す る と考 え られ る. こ の よ う 示 す 液 相 組 成 を考 え る 濃 度 に よ って 次 の三 つ の パ タ ー ン に類 別 (1) Ca KGの 濃 度 が0.1, 0.3wt%の 場 合, 図3, の 量 は 水 和 初 期 で 純水 中 に分 散 さ せ た と き よ りも低 下 し, む しろCAか ら の潜 在 的 溶 出 を抑 えて い る. しか し, 水 和 の 後 半 で溶 存 量 の増 加 が起 こ る (タ イ プA). (2) Ca KGの 濃度 が0.5, 1.0wt%の 場 合, 図5, 図6に 示 す よ うに液 相 中 の カ ル シ ウム分, ア ル ミ ニ ウ ム 次 に, Ca KG溶 液 中 にCAを 化 学 的 に 考 え て み た い. 4.1節 (OH)2と CA-calcium 4に 示 す よ うに液 相 中 の カル シ ウ ム分, ア ル ミニ ウム分 和 初 期 に極 大 値 が 存 在 す る. 沈 殿 のXRDを (以下C2AH8と of で き る. 2-オ キ ソグ ル コン 酸 カル シ ウム の 濃 度 に よ る 液 相 組 成 の差 異 図2よ 7 days phase 2.0wt% 当然 脱 炭 酸 が起 こ り, ア ラ 以上 四 つ の知 見 は, Ca KG溶 た とき, CAか solid 25. よ り脱 炭 酸 (-CO2) と され て い る18) 21).KGも of et al. 28 はCa錯 り, Ca KG溶 分 散 させ た 場 合 を錯 塩 (1) 項 でCa KGとCa 体 を形 成 す る こ と を述 べ た. 液 中 で はCAか ら溶 出 これ よ (以下 本 報 で は 分 の 溶 存量 は, 水 和 直 後 か ら急 速 に増 加 す るが 直 ちに 減 少 し, 再 び微 弱 な増 加 が起 こ る. す なわ ち, 1次, 2次 の極 大 (又 は1次 極 小) 現 象 が存 在 す る (タ イ プB). (3) Ca KGの 濃 度 が2.0wt%の 場 合, 図7に 示
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Die life improvement of flat type punches for hot forging Morihiko Nakasaki, Koji Era, Hiroyuki Myochin and Ichiro Takasu Synopsis: Since forged products have been required more complex and net-shape,
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No.432008pp.287 302 Climatological Characteristics of Local Wind in the Tokachi District, Hokkaido, JAPAN Takashige KAWAI, Mai NAKAJYO, Hisashi KATO and Shuji YAMAKAWA Received September 30, 2007 Climatological
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Title 泌尿器科領域に於ける17-Ketosteroidの研究 17-Ketosteroidの臨床的研究 第 III 篇 : 尿 Author(s) 卜部, 敏入 Citation 泌尿器科紀要 (1958), 4(1): 3-31 Issue Date URL
Title 泌尿器科領域に於ける17-Ketosteroidの研究 17-Ketosteroidの臨床的研究 第 III 篇 : 尿 Author(s) 卜部, 敏入 Citation 泌尿器科紀要 (1958), 4(1): 3-31 Issue Date 1958-01 URL http://hdl.handle.net/2433/111559 Right Type Departmental Bulletin
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GIS Simulation analysis of disseminate of disaster information using GIS * ** *** Toshitaka KATADAJunsaku ASADA and Noriyuki KUWASAWA GIS GIS AbstractWe have developed the simulation model expressing the
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九州大学学術情報リポジトリ Kyushu University Institutional Repository 熊本県水俣市の限界集落における耕作放棄地の拡大とその要因 寺床, 幸雄九州大学大学院人文科学府 : 博士後期課程 : 農村 農業地理学 Teratoko, Yukio http://hdl.handle.net/2324/20036 出版情報 : 地理学評論. 82 (6), pp.588-603,
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お 知 ら せ ( 薬 ) 0 0 5 平 成 2 0 年 8 月 2 9 日 医 薬 品 マ ス タ ー の 改 定 に つ い て 今 般 下 記 の と お り 医 薬 品 マ ス タ ー を 改 定 し ま し た の で お 知 ら せ し ま す 記 次 の 医 薬 品 に つ い て は 平 成 2 0 年 3 月 5 日 付 け 厚 生 労 働 省 告 示 第 7 2 号 に 基 づ
A comparison of abdominal versus vaginal hysterectomy for leiomyoma and adenomyosis Kenji ARAHORI, Hisasi KATAYAMA, Suminori NIOKA Department of Obstetrics and Gnecology, National Maizuru Hospital,Kyoto,
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* * * * * * * 要旨 : キーワード : 1. はじめに 2. 融雪 融氷剤による物理 化学的劣化現象の特徴 393 Table 1 Chemical compositions of ordinary Portland cement and crushed andesitic stone(%) * * * * Table 2 Types of alkaline and alkaline
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The Current Status of and Future Prospects for the Automobile Industry in the Central Liaoning City Cluster (with a focus on the core city of Shenyang) (Part One) YASUGI Osamu Deputy Senior Researcher,
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E-mailxiangzhijp@yahoo.co.jp p p Understanding of Asia by Students of Commercial College under the Old System ACaseStudyofTaihoku Commercial College Kaori Yokoi Abstract Using the Taihoku
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Friction welding of ADC 12 aluminum alloy diecastings Kazuyoshi KATO* and Hiroshi TOKISUE* Both squeeze and gravity castings of ADC 12 aluminum alloy were friction-welded, using a brake type welding machine.
Title 外傷性脊髄損傷患者の泌尿器科学的研究第 3 報 : 上部尿路のレ線学的研究並びに腎機能について Author(s) 伊藤, 順勉 Citation 泌尿器科紀要 (1965), 11(4): Issue Date URL
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(3) (5) (6) 162 青 山 充 て ん層 厚 さ と流 量 計 水 柱 高 さの 関係 を 示 した 付 属 チ ャ ー トに よ り直 ち に平 均 粒子 径 を知 る よ う にな って い る. しか し,試 料 重 量 を 変 え て実 験 す る場 合,チ ρp/w=1を ャー
161 Tadaaki Aoyama: Measurement of Mean Particle Size of Tungsten and Tungsten Carbide Powders by Fisher Sub-Sieve Sizer not Dependent on Porosity. An equation for the specific surface area of powder,
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Key words: intestinal nerve plexus, hypoxic perfusion, immunohistochemistry, 5-100 protein Table I (A) Sroo staining reactivity of nerve tissue normal partly mildly declined all mildly declined partly
1 Department of Legal Medicine, Toyama University School of Medicine 2 3 4 5 6 7 8 Department of Ophthalmology, Graduate School of Medicine and Pharmaceutical Sciences, University of Toyama VEGF Key words
日本消化器外科学会雑誌第31巻第7号
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;-~-: からなだらかな水深 15-20 ~mmature 及び乙の水域で量的に少ない種は, 各混群内の個体数の 20~ ぢ以下の乙とが多かった また, ある混群で多 全長 11-15cm のクラスは, 全長 16-30cm のクラスと重複するが, 全長 31cm~ のクラスとは重複しなかっ T~ta!_~equ_ency + ヱ n~ 120 SUMMARY 1) The
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12 The eect of a surrounding light to color discrimination 1010425 2001 2 5 NotePC 8 10cd=m 2 965cd=m 2 1.2 Note-PC Weber L,M,S { i { Abstract The eect of a surrounding light to color discrimination Ynka
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Table 2 Cases of Nail Deformity Associated with upward Distortion of Distal Soft Tissue No. Age Sex Affected RegionsDuration Results M Both grea
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21 Effects of background stimuli by changing speed color matching color stimulus
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12 61 1 2011 原著 1)2)5) 1) 1)2) 1)2)5) 1)3)5) 1)2) 1)2)5) 1)2) 1)2) 2) 2) 4) 1) 1) 2) 3) 4) 5) 2010 10 6 2010 12 6 A Comparative Study of the Effect and Discomfort Produced by Pharyngeal Anesthesia with
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201 Presenteeism 202 203 204 Table 1. Name Elements of Work Productivity Targeted Populations Measurement items of Presenteeism (Number of Items) Reliability Validity α α 205 α ä 206 Table 2. Factors of