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1 254nm UV TiO 2 20nm :Sr 5 Ta 4 O 15 3
2 4
3 KEY-1 KEY-2 (Ti,Nb,Ta) 5
4 KEY-1 KEY-2 6
5 7 NiO/ Sr 2 Ta 2 O 7 mmol h -1 g H 2 O 2 H 2 O
6 NiO/Sr 2 Ta 2 O 7 The synthesis of photocatalysts using polymerizable complex method M.Kakihana and K.Domen, MRS Bulletin 25 (2000) p.27. Polymerizable complex synthesis of pure Sr 2 Nb x Ta 2-x O 7 solid solutions with high photocatalytic activities for water decompostion into H 2 and O 2 M.Yoshino et al. Chem. Mater. 14 (2002) p
7 (- ') Bi 2 Sr 2 Ca 0.8 Y 0.2 Cu 2 O h + 3 x 24 h 77K 2h + 10 h / K
8 p Synthesis and characteristics of complex multicomponent oxides prepared by polymer complex method M.Kakihana and M.Yoshimura, Bulletin of the Chemical Society of Japan 72 (1999) p
9 11 Step 1 : HOOC HOOC OH COOH : HO OH A B A A B B B A B
10 12
11 Step 2 13 HOOC OH OH HOOC OH OH HOOC COOH HO HOOC COOH HO A B A A B B B A B Step 3 ABO 3
12 14
13 15
14 16
15 A=Y, La, Eu, Ce, Nd, Al, Ga, etc. 17 B=Ti, Zr, Si, Mn, etc. C=V, Nb, Ta, P, etc. Ex. 278 nm Ex. 265nm Em. 518 nm Em. 612 nm
16 18 Use of polymerizable complex method for synthesis of novel phosphor materials K.Watanabe et al. Proceedings for 13 th International Workshop on Inorganic and Organic Electroluminescence and 2006 International Conference on Science and Technology of Emissive Displays and Lighting, (2006) P.356.
17
18 Y 2 O 2 S:Eu 3+ 20
19 21
20 22 ph ph 0.02mol/l 0.5mol/l Y 2 O 2 S:Eu 3+
21 23
22 24 PG HGY 2 O 2 S:Eu nm Synthesis of high brightness submicron Y 2 O 2 S red phosphor powders by complex homogeneous precipitation method Y.Kawahara et al. Chem. Mater., 18 (2006) p Preparation of submicron Y 2 O 2 S red phosphor powders with high emission intensity by complex homogeneous precipitation method V.Petrykin et al. Proceedings for 13th International Workshop on Inorganic and Organic Electroluminescence and 2006 International Conference on Science and Technology of Emissive Displays and Lighting, (2006) P.273.
23 25 3 m 21 m 8 m 0.5 m m 2.4 m
24 26
25 Sc Ti V Cr Mn Y Zr Nb Mo Tc Hf Ta W Re
26 28
27 29
28 3 (2000) P (2005) P
29 31 ph 6
30 32
31 33
32 ph ph 34
33 H2O2 NH3 36
34 36 Structure and stability of water-soluble (NH 4 ) 8 [Ti 4 (C 6 H 4 O 7 ) 4 (O 2 ) 4 ]8H 2 O M.Kakihana et al. Inorg. Chem. 40 (2001) p.891. Chelating of titanium by lactic acid In the water-soluble diammonium tris (2- hydroxypropionato) titanate(iv) M.Kakihana et al. Inorg. Chem. 43 (2004) p A water-soluble titanium complex for selective synthesis of nanocrystalline brookite, rutile and anatase by a hydrothermal method K.Tomita et al. Angewandte Chemie, Int. Ed. 45 (2006) p Synthesis and structure of new water soluble and stable tantalum compound: ammonium tetralactatodiperoxo- -oxo-dititanate(v) V.Petrykin et al. Inorg.Chem. 45 (2006) p.9251.
35 37 Ti Kakihana, Tomita et al. Inorg. Chem. 43 (2004) 4546.
36 CH 3 -CH(OH)COOH OH H COOH H [CH 3 CH(O)COO] 2- NH 4+ 38
37 39 1 mm 0.5 mm [Ti4(C6H4O7)4(O2)4] 8- Inorg. Chem. 40 (2001) 891 [Ti4(C2H2O3)4 (C2H3O3)2O2] 6- Ang. Chem. Int. Ed. 45 (2006) 2378
38 [O 2 ] 2- [O 2 ] 2- Ti-O-Ti 40
39 41 YNbO 4 NaTaO 3 TiO 2 TiO 2
40 Material Stage, 3 (2004) p (2005) p (2006)p
41 43 a.u. 126% 109% 254nm UV YVO 4 :Eu 3+ NiO/NaTaO 3 H 2 O H 2 + 1/2O 2 h /nm
42 YNbO 4 :Eu 3+ YVO 4 :Eu 3+ NaTaO 3 NiO/NaTaO 3 mmol 44
43 45 (NH 4 ) 8 [Ti 4 (O 2 ) 4 CA 4 ]
44 nm 46
45 47
46 48 A new water-soluble ammonium citratoperoxotitanate as an environmentally beneficial precursor for TiO 2 thin film and RuO 2 /BaTi 4 O 9 photocatalysts M.Tada et al. Chem. Mater., 14 (2002) p Synthesis of SrTiO 3 from aqueous solution using lactate titanium complex K.Tomita et al. Trans. Mater. Res. Soc. Jpn., 28 (2003) p (2006)p.13.
47 nm 10 15nm or 200nm 50nm 150nm
48 ph ph TiO 2 TiO
49 51 50nm 150nm Intensity / arb. units ph10 HN 3 aq ph6 100nm 2 / degrees, CuK 50nm 150nm 200nm
50 ph ph 52 Hydrothermal synthesis of nanosized titania photocatalysts using novel water- soluble titanium complexes M.Kobayashi et al. Solid State Phenomena, (2006) p.723. A water-soluble titanium complex for selective synthesis of nanocrystalline brookite, rutile and anatase by a hydrothermal method K.Tomita et al. Angewandte Chemie, Int. Ed. 45 (2006) p.2378.
51 53 Ti TAS FINE 1 NH 4 OH 2 H 2 O 2 3
52 54
53 55
54 56
55 Si-Bi 4 T 3 O Pt Bi 4 Ti 3 O 12 Si 1 m SEM
56 58
57 59
58 60
59 61
60 vs vs vsvs 62
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M R A 対 応 製 品 ISO/IEC 17025 ISO/IEC 17025は 試験所及び校正機関が特定の試験又は 校正を実施する能力があるものとして認定を 受けようとする場合の一般要求事項を規定した国際規格 国際相互承認 MRA Mutual Recognition Arrangement 相互承認協定 とは 試験 検査を実施する試験所 検査機関を認定する国際組織として ILAC 国際試験所認定協力機構
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