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- しまな ほうねん
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1 1 HPLC 1 24 (ergosterol 2). 24- campe- sterol (3) dihydrobrassicasterol(4) sitosterol(5).stigmsterol(6) clionasterol(7).poriferasterol(8) HPLC (3),(4) HPLC S-adenosylmetionine(SAM) ( lanosterol. cycloartenol) (9) 24(25)
2 25 SAM Re- Si- 25 cis trans 9 E Z pro-r C-26 pro-s(c-27) C 26 c 27 13CNMR NMR yeast E Z Ruzicka "Biogenetic isoprene rule"l lanosterol 3 mevalonic acid (MVA) isopentenyy PyroPhosphate (IPP,dimethylallyl pyrophsphate isoprene unit 6unit C30 squalene.squalene cyclase lanosterol 14-demethylation S sf-109 [1.2-13C2]Acetate lanosterol(18) (Fig.1 HPLC C30 18 C27 cholesterol r.t 18 13CNMR l.2 13C]ace- tate E Z 2. MVA(13 lpp 14) MVA C 1 13C 13C HVA C 2 13C lanosterol E MVA C 2 Z SSF-109 [2-13CD3]acetate(20) 26 lanosterol 18
3
4 E CD2H Z CD3 lanosterol cycloartenol Phylis peruviana C2 Acetate CD3 Acetate 20 C cyc10artenol 19 CD cyc10artenol E Z lanosterol SSF C2 Acetate CD3 Acetate 20 13C cholesterol 28 13CD cholesterol 29 Fig 2 26 D]-12R-cholesterol 26 D]-25S Cholester ol 25 Pro-R C 26 Pro-S(C 27 13CNMR C C lanosterol E cholesterol C-26 Z C 27 lanosterol 25 Popjak 25 Si
5 Si cis cycloartenol 19 3 Dioscorea tokoro tokorogenin neotokrogenin C2 Ace tate 12 13C tokorogenin 30 neotokrogenin 31 4 cyclo artenol(19) 25-Si yeast C2 Acetate CD3 Acetate 20 13C ergosterol 32 13CD ergosterol Re D D 24 methyl-d3 methionine yeast ergosterol D 2 lano Sterol
6 Amsonia elliptica C2 Acetate 12 Fig 3 HPLC 20mm YMCA pack ODS LC NMR ca sterol CMP dihydrobrassicasterol DHB Deve1oSil ODS T 7(s-7) 250 x 20mm 20 Fig.4 13CNMR 24 CMP(38) 25 Re- 24 DHB Si Physalis preuviana CMP DHB [2 13CD3]Acetate 20 HPLC CHP DHB 13CD 1H {2H} 13CNMR CMP 40 DHB 13CNMR 13CD DHB 2 13CD3 Acetate CMP CD3 Acetate 4 CMP DHB CMP DHB CMP 13C DHB 13CD CMP 2 CHP DHB 13C
7
8 DHB CMP HPLC 20 Isotope effect retention time HPLC CMP DHB HBD {1H} {2H} 13CNMR 13CD C CMP C 27 DHB C 26 13CD2H CMP C 26 DHB C 27 13CD3 13CD ergostero(33 25 D methyl-d3]methionine CMP DHB 21 HPLC Fig 5 3 a-c,d-f Fig.6 a f 2 CMP DHB (a,d) D2 M+2(m/z402) D HP LC Isotope effect CMP DHB cycloartenol (9 (36 ergosterol CMP DHB methylenecholesterol 7 24 methylenecycloartanol 3 Physalis peruviana Dioscorea tokoro D Re sitosterol 24 sitosterol C2 Acetate 2 13CD3 Acetate ( D. tokoro Bupleurum falcatum ( sitosterol C-26 C-27 13C [26-D]-(25R9-and(25S)-sitosterol 9 sitosterol (45) (46)
9
10 3 25 D methyl-d3]methionine P peruviana sitoste rol 4 D sitosterol cycloarte- nol isofucosterol sitosterol isofucosterol 48 P.preyviana Fig 7
11 Trichosanthes Kirilowii C2 Acetate 2 13CD3 Acetate 22 dihydrochondrillasterol Fig C Sitosterol Re D MVA C 6 C 27 D 2 D dihydro 25 dehydrochondrillasterol 54
12
13
14 cycloartenol D6 56 DeveloSil ODS T-5 250xlO mm 18 Fig 9 D 2 MS d6 cycloartenol 56 HPLC Deuterium Isotope Effect HPLC 13CNMR chole sterol dihydrobrassicasterol Si Re HPLC 1 2
15
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12 2004.9.3. no.234 2004.9.3. no.234 13 14 2004.9.3. no.234 2004.9.3. no.234 15 16 2004.9.3. no.234 2004.9.3. no.234 17 18 2004.9.3. no.234 19 2004.9.3. no.234 20 2004.9.3. no.234 21 2004.9.3. no.234 22
取扱説明書 ［F-12C］
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1 2 3 4 5 0% 20% 40% 60% 80% 100% 6 7 8 0% 20% 40% 60% 80% 100% 9 0% 20% 40% 60% 80% 100% 10 100% 90% 80% 70% 60% 50% 40% 30% 20% 10% 0% 2529 (n=17) 3034 35 (n=21) (n=17) 2529 (n=19) 3034 35 (n=34) (n=64)
Coarse Standard ISO 190/ /21.0 ISO 160/ /22.0 ISO 173/ /21.8 ISO 198/ /21.8 ISO 197/ /20.0 ISO 068/ /19.1 FO-54C
Coarse Standard 190/019 9.5/21.0 160/017 10.1/22.0 173/019 10.1/21.8 198/019 9.1/21.8 197/018 7.1/20.0 068/043 1.9/19.1 FO-54C TC-11C TF-13C TR-13C TR-62C WR-13C Standard 002/018 2.4/19.0 002/016 3.5/19.0
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第18回海岸シンポジウム報告書
2011.6.25 2011.6.26 L1 2011.6.27 L2 2011.7.6 2011.12.7 2011.10-12 2011.9-10 2012.3.9 23 2012.4, 2013.8.30 2012.6.13 2013.9 2011.7-2011.12-2012.4 2011.12.27 2013.9 1m30 1 2 3 4 5 6 m 5.0m 2.0m -5.0m 1.0m
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1 1 36 223 42 14 92 4 3 2 1 4 3 4 3429 13536 5 6 7 8 9 2.4m/ (M) (M) (M) (M) (M) 6.67.3 6.57.2 6.97.6 7.27.8 8.4 5 6 5 6 5 5 74 1,239 0 30 21 ( ) 1,639 3,898 0 1,084 887 2 5 0 2 2 4 22 1 3 1 ( :) 426 1500
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平成２４年財政投融資計画ＰＤＦ出後８／０１６‐０３０
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[mm] [mm] [mm] 70 60 50 40 30 20 10 1H 0 18 19 20 21 22 23 24 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 1 2 3 4 5 6 7 8 9 10 11 12 60 50 40 30 20 10 0 18 19 20 21 22 23 24 1 2 3 4
平成１６年度外務省事後評価実施計画策定について
2005 1 HP http://www.mofa.go.jp/mofaj/area/n_korea/index.html http://www.mofa.go.jp/mofaj/area/n_korea/abd/rachi_mondai.html HP http://www.mofa.go.jp/mofaj/area/n_korea/abd/6kaigo3_gh.html http://www.mofa.go.jp/mofaj/press/danwa/17/dga_0414b.html
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YOKOHAMA 1 1 2 YOKOHAMA 2 21 22 23 24 3 3 31 32 4 YOKOHAMA 33 34 5 4 1 2 6 YOKOHAMA 3 4 7 8 5 No.1 CACE STUDY 9 No.2 10 No.3 CACE STUDY 11 No.4 No.5 12 CACE STUDY 13 No.6 No.7 14 CACE STUDY 15 No.8 16
取扱説明書 ［F-01F］
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COSMOSIL.indd
Column: 5C 18 -MS-II Column size: 4.6mmI.D.-150mm Mobile phase: Methanol/ H 2 = 60/40 Detection: UV254nm Sample: 1; Acetophenone (0.05μg) 2; Methyl Benzoate (0.5μg) 3; Benzene (2.0μg) 4; Toluene (2.0μg)
取扱説明書 ［F-02F］
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Taro10-名張１審無罪判決.PDF
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取扱説明書 ［F-06E］
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BS18summer_H1_H4.indd
Book Selection 2018 Summer http://www.sbcr.jp/ CONTENTS P3 P3 IoT P4 P4 Excel Windows P5 Web P5 P5 Photoshop Illustrator P6 iphone Android P6 P6 P7 P8 SB P10 P10 P11 P11 Pepper http://www.softbank.jp/robot/special/pepper/
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ACQUITY UPLC H-Class ACQUITY QDa Mark E. Benvenuti, Dimple Shah, and Jennifer A. Burgess Waters Corporation, Milford, MA, USA MS ACQUITY QDa UPLC HPLC UV ACQUITY QDa LC EC 1925/26 CFR 21 HPLC 1 LC-MS ACQUITY
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