*1 *2 *1 JIS A X TEM 950 TEM JIS Development and Research of the Equipment for Conversion to Harmless Substances and Recycle of Asbe

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1 *1 *2 *1 JIS A X TEM 950 TEM JIS Development and Research of the Equipment for Conversion to Harmless Substances and Recycle of Asbestos with Superheated Steam Part 3 An evaluation with the TEM of the processing material and the cement raw materials Kouya SAWADA *1 Isao MIURA *1 Masatoshi HANDA *2 As means to confirm that there was not asbestos fiber to a detoxification disposal of construction materials containing asbestos, it has been performed by X-ray diffraction and the dispersion staining using the phase contrast microscope until now in conformity with JIS A 1481 (2008). However, it was notified that we confirmed it with a transmission electron microscope (TEM) to raise official approval sensitivity from Ministry of the Environment. In this report, We describe the result that the non-asbestos produces the cement which assumed the result that confirmed becoming it and a processing thing raw materials in TEM, and confirmed the compatibility as cement raw materials in overheat steam of 950 degrees Celsius atmosphere. The following results are obtained in this development. (1) The harmless treatment process was made clear by the scientific consideration related to the atmosphere of superheated steam. (2) The adequate conditions of the maximum temperature and the holding time of maximum temperature for the harmless treatment were evaluated by the fundamental experiments under the atmosphere of superheated steam. (3) The experiment using large size equipment developed for the harmless treatment of construction materials containing asbestos in large quantity was performed on the adequate conditions obtained above and the transformation to non-asbestos was sufficiently verified. (4) The non-asbestos construction materials obtained by the experiment described above were evaluated to be able to be used as the raw material of cement by the strength test based on Japanese Industrial Standards. *1 *2 *1 Technical Research Institute *2 Department of Research Planning and Management 4-1 4

2 *1 *1 *2 JIS A X TEM 950TEM μmOH 1, ADVANTEC [FUT542FB] W560 D360 H380 D D950 *1 *2 4-2

3 4 X CaSiO TEM kW TEM CASE AE 5 AC D JISA TEM 0.5μm 0.05μm 3μm 3 EDS 4.0mm cm cm EDS CASE A CASE B CASE C CASE D CASE E 4-3

4 5 TEM 900CASE A C CASE D CASE A CASE B CASE C CASE D CASE E t TEM kg/h 4m 3 /min 179kW 6 TEM kg/h 210kg/ 1 52kW 1 SEM kg

5 8 1 1 JIS R AB TEM A 150Mf/g BC A B 10 A JIS ALL PCM ALL PCM A B C ALL 0.5μm 0.05μm 3μm PCMPCM 5μm 0.2μm 3μm A49Mf/g B2Mf/g C150Mf/g SiO 2 Al 2O 3 Fe 2O 3 CaO MgO SO 3 Cl A B JIS 5 5 g/cm 3 cm 2 /g min N/mm 2 h A JIS

6 1mg2mg 2mg Wistar HO JIS PJ NEDO / TEM T. Kozawa, A. Onda, K. Yanagisawa, O. Chiba, H. Ishiwata and T. Takanami, J. Ceram. Soc. Japan, 118, (2010) 4-6

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