Table 1 Concentration of stock solutions

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1 Table 1 Concentration of stock solutions

2 JAPAN ANALYST Vol. 8 (1959) Fig. 1 Absorption curves for azolitmin at different Fig. 2 Absorption curves for bromcresol green at different Fig. 3 Absorption curves for bromcresol purple at different Fig. 4 Absorption curves for bromphenol blue at different Fig. 5 Absorption curves for bromthymol blue at different Fig. 6 Absorption curves for chlorphenol red at different

3 Fig. 7 Absorption curves for omikuron Ē-cresol red at different Fig. 8 Absorption curves for Fig. 9 Absorption curves for lacmoid at different Fig. 10 Absorption curves for methyl red at different Fig. 11 Absorption curves for nile blue at different Fig. 12 Absorption curves for phenol red at different Fig. 13 Absorption curves for tetrabrom phenol blue at different Fig. 14 Absorption curves for thymol blue at different

4 JAPAN ANALYST Vol. 8 (1959) Fig. 15 Absorption curves for thymol blue at different Fig. 16 Absorption curves for thymol blue at different Fig. 17 Absorption curves for congo red at different Fig. 18 Absorption curves for dimethyl yellow at different Fig. 19 Absorption curves for methyl orange at different Fig. 20 Absorption curves for neutral red at different Fig. 21 Absorption curves for tropaeolin 00 at different

5 Fig. 22 Absorption curves for tropaeolin 000 at different Fig. 23 Absorption curves for bromcresol blue at different Fig. 24 Absorption curves for Fig. 25 Absorption curves for crystal violet at different phlvalues Fig. 26 Absorption curves for ć-dinitro phenol at different Fig. 27 Absorption curves for nitro thymol yellow at different Fig. 28 Absorption curves for phenol phthalein at different Fig. 29 Absorption curves for thymol phthalein at different

6 JAPAN ANALYST Vol. 8 (1959) Table 2 Type analysis and their isosbestic points, absorption maxima, pk values for investigated indicators (1) Indicators which acidic form more absorbs than alkaline form on long wave length side (2) Indicators which alkaline form more absorbs than acidic form on long wave length side

7 Fig. 30 Absorption curves of acidic form and alkaline form

8 JAPAN ANALYST Vol. 8 (1959) 1) W. R. Brode : J. Am. Chem. Soc., 46, 581 (1924). 4) W. B. Fortune, M. G. Mellon : J. Am. Chem. Soc., 60, 2607 (1938). 5) J. King : " Proceedings of the International Congress on Analytical Chemistry ", p. 186 (1952). 6) W. C. Holms : Ind. Eng. Chem., 16, 35 (1924). 7) A. W. Smith, C. E. Boord : J. Am. Chem. Soc., 44, 1449 (1922). Spectrophtometric study of acid-base indicators. SOichiro MUSHA and Ken'ichi SUGIMOTO (Department of Applied Chemistry, College of Engineering, University of Osaka Prefecture) Although some acid-base indicators have been investigated from a spectrophotometrical viewpoint, the systematic study of most indicators has been lacking. In the present paper the spectra of about 30 kinds of indicators commonly used were measured at various. As a result, indicators were divided into three types with regard to the variation of hue. Type A: Both the maximum and minimum appear in the absorption curve, and their positions are interchanged with each other at the extreme of transformation interval (See Fig. 2). Type B : The position of the absorption maximum changes as ph is varied (See Fig. 19). Type C : The position of the absorption maximum does not change, but the absorbancy changes as ph is varied (See Fig. 28). From an inspection of chemical structure, it was found that sulfonephthalein dye belongs to Type A, azo dye to Type B, and phthalein dye to Type C. And, in addition, theoretical consideration was given to the isosbestic point and to the position of the absorption maximum in absorption curves. (Received June 13, 1958)

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