48ASMS Conference 48ASMS (American Society for Mass Spectorometry) Conference , JEOL USA JEOL USA NanoESI LC-MS/ N
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1 N o JSM-6500F JSPM SNOM 17- JMS-700 MStation JEOL DATUM INFORMATION
2 48ASMS Conference 48ASMS (American Society for Mass Spectorometry) Conference , JEOL USA JEOL USA NanoESI LC-MS/ NMR Costello HX MS Michel Bertrand MAB (Metastable Atom Bombardment)/MS 2 ANALYTICAL NEWS MAB EI ASMS LC-MS/NMR Conference FinalHyatt Hotel Rainbow Langoon 49 ASMS5
3 SEM FE SEM JSM-6500F JSM-6500FFEG( ) FEG EBSPWDSCL EDS EBSP WDS 3.0nm 200nA 150mm X-Y3 (5 ) 1,280 1, nm15kV 5.0nm1kV 10500, kV A210 7 A 200mm 150mm 200mm I II X-Y 70mm50mm 110mm80mm mm41mm 3mm41mm XYR5 OS Windows NTH ,2801, Pa WindowsHMicrosoft ANALYTICAL NEWS 3
4 SPM SPM JSPM-4210 SPM 20 STMAFMSNOM SPM JSPM-4210 SPM STMAFM SPM 130K AFS PFM SEMSEM Basic Mode Advanced Mode AC Mode AFE / Contact Mode AFM Phase Image / MFM / FFM STM / STS / CITS LM-FFM / VE-AFM / PFM / SKPMF / / 4 ANALYTICAL NEWS
5 SPM AFMSNOM -SNOM -SNOM SPM WITec Confocal SNOM AFMOM AFM/SNOM SNOM AFM 650 nm 22 K counts/s 240mm 20mm( ) PFM 2 0 nm 7 K counts/s AFM AFM AFM 540nm570nm DIC18 514nm 5nW ANALYTICAL NEWS 5
6 NMR MS 17- QMSMSMS JSM-Automass Sun, JMS-GCmate, JMS EDL 17EDL 3 GC/MS 17EDL tbdms BSA TMS JMS-Automass Sun, JMS- GCmateJMS EDL JMS-Automass Sun 1m R500SIM GCmate R=3,000 SIM JMS- 700 R=10,000 SIM TMS Automass Sun, GCmateJMS S/N ODS HPLC 3 JMS-700 > GCmate > Automass Sun S/N Automass Sun m/z = EDL DiTMS Q-MS 17EDL ODS HPLC GCmate Automass Sun S/N 17EDL DiTMS JMS EDL ODS HPLC 17EDL S/N GC/MS g/l GC/MS 17EDL 17EDL 6 ANALYTICAL NEWS
7 SEM/TEM NMR Image Analysis Software for Windows9598NT2000 / DOCUAUTOPRO3 DOCU EFI MIA AUTODOCU PROAUTO EFI MIA EFI PRO BMPTIFFPhotoCDJPEG 8-16Bit (24Bit) (PC-SEM) SemAfore Fastscan IF MIALaw EFI ANSI Image C (ANSI C DOCU 800,000 AUTO 2,300,000 PRO 3,400,000 EFI DOCUAUTO MIA LAN SEM PC : Windows95/98/NT Image Analysis Software SEM ANALYTICAL NEWS 7
8 8 ANALYTICAL NEWS NMR CHROMPACK 0.2m TEL FAX ˇ 3 TEL FAX TeCDDs/TeCDFs/PeCCDs/PeCDFs/HxCDDs/HxCDFs P/M CP-SIL88 FOR DIOXINS 100%Cyanoproply Poliysiloxane 0.25mm 0.25mm 0.32mm 0.1m 0.1m 0.13m 60m 30m 60m 128,000 69, , ,000 62, ,000 P/M CP-SIL8CB-MS 5%Phenyl 95%Dimetylpolys ilo-xane 0.32mm 0.32mm 0.25m 0.25m 60m 30m 138,900 81, ,000 73,000 HpCDDs/HpCDFs/OCDD/OCDF/TeCBs/PeCBs/HxCBs/HpCBs NEW 0.5mm 1.0mm 2.0mm 2.5mm 3.0mm 0.5mm 1.0mm 2.0mm 1.0mm 2.0mm 3.0mm 76, , , , ,000 76, , , , ,000 85,000 73, , , , ,000 73, , , , ,000 85, XAC
9 NMR MS FAB MSESIMS High Resolution Mass Spectrometry 3 FABESI LC/MSFAB ESI LC/MS UV JMS-700 JMS-700XMS FABESILC/MS 1 10ppm B 1 PEG 2000 PEG MH R=2000 PEG m/z mmu 3B MH 4B R=4000 CsI CsI MH MCs CsI BCsI /z ppm 35mmu 7.2mmu (2ppm) FABESILC/MS FAB TEL: FAB FAB FAB B FAB ESI LC/MS LC/MS PEG300 PEG CsI 1621 PEG300 PEG300 (m/z) (m/z) (ppm/mmu) / / / / / / /-2.5 PEG MH MH PEG PEG 3 B (a) (a) ppm/0.9mmu (b (b 2 a PEGb 4 B CsI b B ANALYTICAL NEWS 9
10 MS JMS-700 MStation Persistent Organic PollutantsPOPs JMS-700 MStationfg g 2 I MStation 2 II 4 I II TMP520L PFK HP HP () 10 ANALYTICAL NEWS
11 JEOL DATUM INFORMATION CS 1 44NMR 2 NOE NMRNMR 1 H 13 CNMR , , ,000 NMR MS MSNMR HP MODEL HP Laserjet Model:33449A MS-LPR449 NM-LPR33449A/NM-LPR33481A JMS-700 JNM-ALPHA HP LaserJet4050 HP HP Laserjet III TEL FAX TEL MS DIOK 6 1DIOK DIOK HP Laserjet4050 MS2 NMR 45NMR NMR NMR 12 LCMS 4PFGNMR ANALYTICAL NEWS 11
12 INFORMATION (1)TEM 1 T E M (2)2010TEM (3)1230TEM (4)1010TEM (5) 1A S I D (6) 1 9:3017: (1) 2 (2)TEM 1 (3) (4) (5) 2 (6) 2 (7) 2 (8) 2 (9) 2 (1)5000 SEM S E M (2)5800SEM S E M (3)SEM 3 S E M (4)FE-SEM 3 F E - S E M (5)LV-SEM 1L V - S E M (6) SEM 2 S E M (7)EDS 2 J E D E D S (1)SEM 1 S E M (2)SEM 2 S E M (3) 2 (1) / 8900 E P M A (2) / (3) / (1)EPMA 2 E P M A (1)LA4 1 D / 2 D 1 H 1 3 C (2)AL 1 2 A L (3)AL 2 21 D / 2 D 1 H 1 3 C (4)ECP4 1 D / 2 D 1 H 1 3 C Phase Sensitive 2D N O E H O H A H A 31 1 R O E S Y 1 1 H M Q C / H M B C 26 (12) 1 28 (1) 3 M S S I M2325 (2) 3 D i o k 2325 (3)DIOK 3 D I O K (4)MStation 3 M S1113 (5)GCmate 3 M S G C / M 2930 (6) FT-IR E S R (5)ECP 2 ECP (6) 2D-NMR (7)NOE & NOESY (8)HOHAHA (9)ROESY (10)HMBC/HMQC (11) NMR (13)FG-NMR 2 1 F G - N M R (14)DPFGSE1 D P F G S E N O E 2425 (7)Automass2 M S (8)Automass CI/DI 1 (9)Automass (P&T) 2 P & T V O C (10)Automass (H.S.) 2 H. S. V O C JIR WINSPEC 2 FT-IR WINSPEC JES-FA FIR50/60/702 FT-IR 50/60/ [NMR] E C P A l p h a L a m b d a N M R D P F G S E T E L (042) FAX (042) ANALYTICAL NEWS achiba@jeol.co.jp FAX usersmt@jeol.co.jp FAX e - m a i l usersmt@jeol.co.jp e - m a i l F a x No F TEL FAX TEL( FAX ( 042 ) ( 011 ) ( 022 ) ( 0298 ) ( 045 ) ( 052 ) ( 06 ) ( 082 ) ( 087 ) ( 092 )
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2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
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平成26年度 化学物質分析法開発報告書
2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
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(a) (a) 1010 LC/MS JIS K 04501010 JIS K 04502010 JIS K 04503010 JIS K 04504010 (2) ( JIS K 04505010 JIS K 04506010 JIS K 0128 No 1 PCBPCB 2 αhchβhchγhchδhchp,p DDTp,p DDEp,p DDD I IItranscis transcis HCB
J. Mass Spectrom. Soc. Jpn.: 58(5), (2010)
J. Mass Spectrom. Soc. Jpn. Vol. 58, No. 5, 2010 REVIEW 9 Secondary Ion Mass Spectrometry (SIMS) SIMS SIMS Fundamentals of Mass Spectrometry Secondary Ion Mass Spectrometry (SIMS), Cluster SIMS, and Electrospray
要調査項目等調査マニュアル
PBDEs TriBDE DeBDE 1 TriBDE 8 TeBDE 6 PeBDE 8 HxBDE 7 HpBDE 5 OcBDE 3 NoBDE 2 DeBDE 40 GC/MS 1 1 1 ng/l µg/kg, dry µg/kg TriBDE 0.1 0.01 0.01 TeBDE 0.1 0.01 0.01 PeBDE 0.1 0.01 0.01 HxBDE 0.1 0.01 0.01
外因性内分泌攪乱化学物質調査暫定マニュアル（水質、底質、水生生物）
(PCB) 1 ng/l (µg/kg, wet) (µg/kg) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001)
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MH MH 9.50 8.50 9.40 8.40 9.30 9.20 8.30 9.10 9.00 8.20 8.90 8.80 8.10 8.70 8.60 8.00 8.50 7.90 8.40 8.30 7.80 8.20 8.10 7.70 8.00 7.60 7.90 7.80 7.50 7.70 7.60 7.40 1 7.50 7.40 7.30 2 7.30 7.20 7.20
MAbPac RPカラム
CHROMATOGRAPHY CONSUMABLES MAbPac RP Product Specifications Thermo Scientific MAbPac RP LC HCFc Fab scfc F ab LC/ UV LC/MS ph DTT ph 14 11 ºC mab QC mab mab Fc Fab scfc F ab mab QC LC/UV mab MAbPac RP
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14 4 12 10 8 6 3 2 4 2 1 0 0 100200300400500600 100200300400500600700 0 0 100200300400500600 100200300400500600700 (ppm) (ppm) 7 4 6 5 4 3 3 2 2 1 1 0 0 100200300400500600 100200300400500600700 0 0 100200300400500600
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税関分析25 年の進歩
25 1 25 40 27 25 27 32 25 CeEDTA 10) 11 1) Fe Al Zn EDTA 2) 12) n IR400 2N BT EDTA 14) e 15) 16) 17) 18) 3) Zn Cu 4) Mn 5) 6) 7) 8) 9 13) 2 24) X 56),57) 58) 25) 59) 60) X 61) X X 26) X 27),28),29) 62)
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[] 03084 [Pieters et al. 1993] m 21 600-1600 nm 8 nm 8 nm9 km 20 km SN 200 [ MT-300 F5.5 150 cm][ ] [600-1000 nm][1000-1600 nm] CCD [SBIG ST-7E Si-CCD ][SU IncSU320-1.7RT-DInGaAs-CCD ] PC [Phillips co.
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1 1 1 2 1 3 1 4 2 5 5 6 6 1 6 2 7 3 7 4 7 5 7 7 8 8 10 1 10 2 10 3 10 12 1 12 2 12 3 12 4 13 5 14 14 1 14 1 2 3 4 5 1 2 3 4 16 5 16 6 16 7 17 6 17 18 19~23-19- 1 0.5 1 43.25 2.20 3.60 103.50 43.88 2.20
財務情報
50 Financial Information >> 52 54 66 68 69 71 72 51 2004 4,625,151 2,605,343 2,019,807 N/A 373,435 139,401 234,034 (7,603) 2005 2006 2007 2008 2008 4,664,514 4,637,657 4,769,387 6,409,727 $ 63,976 2,650,586
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SEC (SEC) SEC SEC SEC 2
SEC (SEC) SEC SEC SEC 2 SEC ( 1) 1: SEC www.agilent.com/chem/jp 3 ( ) ( 2) ICH (Q6B) 3 lgg 8 7 6 5 4 1. 2. 3. 4. 5. Agilent AdvanceBio SEC 3 Å 7.8 x 3 mm 2.7 µm (p/n PL118-531) Agilent 126 Infinity LC
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名称未設定-2
Contents 1 2 3 4 5 6 7 8 9 1 11 12 13 14 15 16 17 18 19 2 21 22 i 23 24 25 26 27 28 29 3 31 32 33 34 35 36 37 38 39 4 41 42 43 44 45 46 47 48 49 5 51 52 53 54 55 56 57 ii 58 59 6 61 62 63 64 65 66 67 68
Microsoft Word - 第302回プログラム最終版（H ）.pdf
HP 24 10 15 24 10 24 302 374 24 11 10 9 00 16 30 20 A 1-2-27 TEL 06-6949-5151 602-8566 465 TEL 075-251-5620 FAX 075-251-5840 E-mail rad@koto.kpu-m.ac.jp http://www.jrs-kansai.jp/ PC 1 Macintosh PC Windows
Microsoft PowerPoint - 201409_秀英体の取組み素材（予稿集）.ppt
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