スライド 1

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1 API Gas API

2 Topics API Gas Gas Heater Gas Temparature Gas

3 Topics API Gas

4 API Gas Curtain Gas 60PSI

5 API Gas Neblizer Gas Gas1 TurboIonSpray

6 API Gas Heater Gas Gas1 Gas2 Gas2

7 API Gas Exhaust Gas Exhaust Flow

8 Gas

9 Gas API4000 Curtain Gas 60 PSI Gas / Gas2 105 PSI Exhaust Gas PSI

10 API4000 Gas1/Gas2 : N 2 or Air Max 105 PSIG =0.72MPa=7.4kgf/cm2 CUR : N 2 Max 60 PSIG =0.41MPa=4.2kgf/cm2 Exhaust supply PSIG = MPa= kgf/cm2

11 Gas Supply Requirements <PSIG>

12 Topics Gas

13 Gas (1) Source Exhaust Pump Bad Event Viewer

14 on Analyst: View/Event Log... Event Viewer on PC: Start /Settings/ Control Panels/ Administrator Tools Event Viewer

15 Event Viewer <Application Log> Warning Error [ Fault Set: Source Exhaust System Failure ] "Housing Pressure Too High "

16 Source Exhaust System Failure Housing Pressure Too High Exhaust ( Standby Ready Standby Error

17 Source Exhaust System Failure Housing Pressure Too High Exhaust 1) etc.. Exhaust Flow Control API 1 API3

18 Source Exhaust System Failure Housing Pressure Too High EXHAUST WASTE OUT Exhaust Out / Exhaust MS

19 Application Log Application Log.evt

20 Error Log ; MassChrom Mac DAD Instrument Status Mac DAD Console

21 Error Log ; MassChrom System Folder / Preferences/ PE SCIEX folder /LC2 Error Log

22 Gas ( ) Source Gas 1* Outlet Pressure Too Low (* Gas 2)

23 Gas1/2 Outlet Pressure Too Low Gas1/2 Standby Ready

24 Gas1/2 Outlet Pressure Too Low Gas1,2 Gas1 80 Gas2 90 Error Gas1 60 Gas2 70 Ready

25 Gas ( ) Curtain Gas Outlet Pressure Too Low

26 Curtain Gas Outlet Pressure Too Curtain Gas Low etc.

27 Topics Heater Gas Temparature

28 Cycloprothrin H 2 C CH 3 O O C 26 H 21 C l2 NO 4 Monoisotopic Mass = O [ M+NH 4 ] + Cl Cl O H C N [ M+H ] +

29 Cycloprothrin [ M+H ] + : m/z 482 MRM Channel:482/165 [ M+NH 4 ] + : m/z 499 MRM Channel:499/257 50ppb 50ppb

30 GS Temparature GS2 Temp < > [ M+NH 4 ] + : m/z 499 MRM Channel:499/257 50ppb API mM AcONH4 / MeOH gradient Atlantis dc18 2x50mm 0.2mL/min TurboIonSpray

31 Pregnanediol / Pregnanetriol CH 3 C OH CH 3 C OH OH HO H HO H Pregnanediol C21H36O2 Monoisotopic Mass Pregnanetriol C21H36O3 Monoisotopic Mass

32 Pregnanediol / Pregnanetriol CH 3 C OH m/z 338 [ M+NH 4 ] + HO H Pregnanediol C21H36O2 Monoisotopic Mass m/z 321 [ M+H ] +

33 [ M+NH 4 ] + as Precursor ions API 4000 GS1:40 psi GS2:40 psi GS2 Temp: 0 (No heat) 10mM AcONH4 / MeOH gradient Unison UK C8 2x50mm 0.2mL/min TurboIonSpray Pregnanetriol 354/301 3pg / ul Pregnanediol 338/285 10pg / ul

34 CUR/CAD/GS1/GS2 Pressure / Temp. FIA

35 FIA Flow Injection Analysis HPLC Injection S/N =100

36 API 4000 / 5000 FIA Optimization; API 3000 API 2000

37 Topics Gas

38 TurboIonSpray for API 3000 Gas2 Heater Gas1 Neblizer

39 TurboIonSpray for API 3000 Gas2 Heater Gas1 Neblizer GAS1 90PSI

40 Heated Neblizer for API 3000 Gas2 Pressure 60-90psig Gas 1L/min

41 API TEL FAX;

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