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- みいか かやぬま
- 5 years ago
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1 I
2 Lagmur Freudlch DNA DNA
3 GCMS
4 .
5 : 4 5 : A A
6 2.8 a) b) a 2.9 A4
7 ) [ ][ ] Cp [Jmol K ], Cp =.98 Jmol K Excel
8 , A4 A 5 TK03500 B6 67
9 3. 3. C [mol] 3. m 3 40mol/ m 3 40m 3 60kg mol/ m 3 g mol/g g [mol/g] g + V[m 3 ] C 0 [mol/ m 3 ] : W () (C 0 -C)V (2) W(C 0 -C)V (3) C C V = 0 V = ( C C0 ) (4) W W
10 C kg : [mol/g] V (3) W V mol / g) = ( C C W 2 C 40 3 ( 0 40 ) = ( C 40) 60-2/3 C C 0 Lagmur KC = + KC V = ( C C0 ) W [mol/m 3 ] C 0 -V/W V C 0 W C mol/ 0.02 mol/ (4) C W= V=00cm 3 C mol/dm 3 dm 3 3 = 0.N 0. C=0.478mol/dm 3 [mol] (4)
11 V = ( C C0 ) W = () [mol] C 0 [mol/m 3 ] V[m 3 /hr] w[g] C C - [mol/m 3 ] [mol/g] C [mol/m3] [mol/g]lagmur K K EPS EPS Freudlch Lagmur Lagmur ml 500ml 500ml 5
12 52ml 25ml 20ml 00ml 50ml N/0N/00-NaOHN/0-HCl ml 000ml 000ml N2- N2-500ml 000ml N4N8N6N32 500ml 00ml g 00ml 20 2 N0-,N00-000ml N0- N2- N4-2mlN8- N6-5mlN32 5ml N32 N N2 N0- N0- N2- N4-2mlN8- N6-5mlN32-5ml N32 N00
13 28ml 000ml 000ml N2- N2-500ml 000ml N4-N8-N6- N32-500ml N0-,N v v' x = N f (3.3) x [mol/] v [m] NNaOH [N] fnaoh [-] v NaOH [m] mol/=n
14 (3.3) v 2 m, NaOH N = 0. N NaOH f = 0.998, NaOH v = 9.85 m (3.3) x[mol/] v v' x = N f v' x = N f v 9.85 = = mol/ ( x C C 0 ) 2 00m g 00ml g g 00ml 00ml 00ml 20 2
15 2 Lagmur Freudlch C0 C 00 = w 000 (3.4) [mol/g] C [mol/] C [mol/] w [g] 3.5 vs C C vs C l vs l C 3 Excel
16 g w[g] Table Table w [g] 23 2 Table 6 Fg. g [mol/g] C 0 C b w w [mol/] ( C C ) = 0 b [mol/] [g] [mol/g] Fg. C b =0.462C 0 =0.4894w= = ( ) = Table Table 6 Fg. C b C b =
17 3.6 WdowsXP OSWdows98, 2000, NT C Excel Excel A A B A A Eter 5 Excel 6 Excel B5 C A B C fx =A+B Eter C 6 Excel C Excel AA3 Delete
![A5A9 C 0 mol/dm 3 B5B9 C mol/dm 3 E5E9 W[g] C5 fx (A5 B5)0.](/docs-images/97/131171868/images/18-0.jpg "E5 8 Excel [mol](4) C 5C9 V = ( C C0 ) W Excel C 5 fx (A5 B5)0.E5 Eter C 6C9 00cm 3 C mol/dm 3 00cm 3 0.dm 3 V=0.")
18 A5A9 C 0 mol/dm 3 B5B9 C mol/dm 3 E5E9 W[g] C5 fx (A5 B5)0.E5 8 Excel [mol](4) C 5C9 V = ( C C0 ) W Excel C 5 fx (A5 B5)0.E5 Eter C 6C9 00cm 3 C mol/dm 3 00cm 3 0.dm 3 V=0. dm 3 Excel ad_gra.xls Excel ad_gra.xls 3.6 Lagmur Lagmur
19 Lagmur Lagmur Excel ad_gra.xls Excel ad_gra.xls USB
20 3.5 FD ad_gra.xls ad_gra.xls ad_gra.xls ad_gra.xls Excel
21 4 0 Excel ad_gra.xls ad_gra.xls C b [mol/l] C [mol/g]b,c 4 C b / Excel D5 =B5/C5 D6D9
![C b [mol/l] [mol/g] C b [mol/l] C b /[g/l] Excel Excel sheet Graph2 Graph Graph2 Graph C b [mol/l] [mol/g] Graph2 C b [mol/l] C b](/docs-images/97/131171868/images/22-0.jpg "/[g/l] Graph2Lagmur C b [mol/l] C b [mol/l] [mol/g] C b /[g/l] Lagmur Lagmur K Excel Excel ad_gra.")
22 C b [mol/l] [mol/g] C b [mol/l] C b /[g/l] Excel Excel sheet Graph2 Graph Graph2 Graph C b [mol/l] [mol/g] Graph2 C b [mol/l] C b /[g/l] Graph2Lagmur C b [mol/l] C b [mol/l] [mol/g] C b /[g/l] Lagmur Lagmur K Excel Excel ad_gra.xls Graph2 Graph2Excel Graph Graph2
![C b [mol/l] C b](/docs-images/97/131171868/images/23-2.jpg "/[g/l]excel R")
23 3.8 Lagmur Lagmur K Graph2 C b [mol/l] C b /[g/l]excel R ax+b OK OK
24 OK 22
![22 C8 D8 Graph2 C b [mol/l] C b /[g/l] Excel 438.6526.54 438.65 26.54 Lagmur K 3.](/docs-images/97/131171868/images/25-1.jpg "6 Lagmur C ( + KC ) C KC = K = C = C = =( K) C/ C = = K Excel Lagmur K C8D8 Graph2 26.54 438.")
25 22 C8 D8 Graph2 C b [mol/l] C b /[g/l] Excel Lagmur K 3.6 Lagmur C ( + KC ) C KC = K = C = C = =( K) C/ C = = K Excel Lagmur K C8D8 Graph D9 C9 D8 D8C8 C8D8 Graph D9 C9 D8 D8C8
26 Excel =/ =438.65, =/( K)=26.54 K =/D molg -, K =/ /=/D8/C86.5 D9 C9 K Lagmur Lagmur Excel F5F30 C b [mol/l] [mol/g]graph C b [mol/l] C b [mol/l] [mol/g] Lagmur KC = + KC (3.0) K =/D molg -, K =/ /=/D8/C86.5 D9 C9 K Graph G5G30 F5F30 C b [mol/l] [mol/g] G5 D9 C9 K $$D$9, $C$9 =$D$9*$C$9*F5/(+$C$9*F5) Lagmur G5 F5 D9 C9
27 G5 G5 G6G30 Sheet Graph Graph ( Freudlch BET ) Excel Excel Excel Excel C b [mol/l] [mol/g] C b / Excel C b [mol/l] [mol/g] C b [mol/l] C b /[g/l] 3.9 Freudlch C b Freudlch ab Freudlch Freudlch = ac b ab l = l a + l C b b l C b l /b l a C b ad_gra.xls b
![l C b [-] =l(b5) B5 Cb l [-]](/docs-images/97/131171868/images/28-3.jpg "=l(c5) C5 l C b [-]l [-] l C b")
28 l C b [-] =l(b5) B5 Cb l [-] =l(c5) C5 l C b [-]l [-] l C b [-]l [-]
29 y = 0.369x 5.93 l = lcb a/b 93 l a = 5.93 a = e 5. = = b a Excel =exp(-5.93) Ferudlch a/b Ferudlch a/b Ferudlch Ferudlch = ac b a /b C b Ferudlch b Lagmur Excel Ferudlch = ac b b a/b b = C Excel
30 =0.0027*G5^0.369 G5 C b 0 C b 0.5 C b Freudlch Graph C b [mol/l] [mol/g] Lagmur 3.0 Freudlch ac /b () C a b (Lagmur)
31 KC = + KC (2) K Freudlch Lagmur 3. (a) Hery KC (3) K 3- (a) C C p 0 (a) 0 (b) 0 0 (c) (d)bet 3-
32 (b)lagmur 3-2 [-] r [mols - ] a[mols - ] 3-2 Lagmur ra (6) r[mols - ](-)[-] C[mol m -3 ] r b(-)c (7) b[m 3 s - ] ab(-)c (8) b C θ = (9) a + b C [molkg - ] b/a K[m 3 mol - ](K )θ =
33 KC = + KC (0) (c)(freudlch) 3-(c) ac /b () [molkg - ] a b [-] (d)bet(bruauer-emmett-teller) BET 3-(d) BET 3-3 q = q K C ( C) ( + KC C) 3-3 Lagmur 2 3- K K
34 3-, C, C/ C [molm -3 ] [molkg - ] C/ [kgm -3 ] (3.0) K C = + KC (3.3) C C ( + KC ) C KC = K = C = C (3.4) = =( K)(3.4) C/ C = = K 3- C/ C =/ =438.65, =/( K)=26.54 K =/D molg -, K =/ /=/D8/C86.5 K = / [ molkg - ] Lagmur : C [ molm -3 ] C
35 Freudlch C b C b [mol/l] [mol/g] log 0 C b log Freudlch ab b = ac b () ab l = l( ac b b = l a + lc ) b b = l a + lc b b l C b l x=l C b y=l l = l a + lc b (3) b y=a 0 +a x a a 0 = l a( ) a = e = ( ) b a 0 a 0 a a = a 0 = a= b= =ac /b b c b =00.5 (2) (4)
36 BET BET KC = ( C)( C + KC) 7 BET KC ( C) = ( C + KC) 8 8 ( C) ( C + KC) = KC + ( K ) C = KC 9 9 C C ( C) C( + ( K ) C) = KC C ( C) = K K + C K 2 C K C (- C) K K
37 3.2 Hb HcCbCa Hd Oa ObHa Ob Ca 2.9 Oa 3.6 [m 2 ] 3-6 Ca Oa.32 Ca Ob.206 OaCaOb 2.9 C 0.77 O 0.62 S s' = ( ) ( ) = m 2 2 S[m 2 /g] 23 S = s' S [m 2 /g] [mol/g] s [m 2 ] [/mol] S[m 2 /g] = mol/g 20 s ' = m S = = 28.5 m 2 /g
38 [] [] 25 0,20,40,50,60,80,00 wt% vs [] dt / w = (4.) d t w w : [g/cms] : g/cms [g/cms]25 d : [g/cm ] d : g/cm 3 [g/cm ]25 t : [s] t : [s] W: dt = w (4.2) d w t w /d [cm /s] (4.3)
39 [] ) b 20m f a b 5 4- bd m [wt.%] d[g/cm 3 ] / w [-]
40 4.3 [] 4-2 w'g w g 25 d g/cm g/cm 3 V w w = (4.4) d w' w
41 V wg w w' d = (4.5) V d w [g] w w [g] V[cm 3 ] w[g] d[g/cm 3 ] [wt.%] [wt.%] w [g] w w [g] V[cm 3 ] w[g] d[g/cm 3 ]
42 4.4 [] [ ] PVA; -CH 2 CHOH- 0.5g00cc 2/3, /2, /3, /5 l( / w ) [] C - w C w vs [] 4-3 [g/00cc] d[g/cm 3 ] / w [-] 0.5(/5) 0.5(/3) 0.5(/2) 0.5(2/3) 0.5
43 [] PVA M - w w l( / w ) C w = g/cms [] M []KM (4.6) K= [] - [ ] = lm (4.7) w C 0 C w l( / w ) [ ] = lm (4.8) C C 0 - w l( / ) C C w C C w [] - w C w C l( / w ) C w C w C PVA M 4.6 PVA M M=/K / / /
44 [] w c w - w K PVA C C w [] l( / w ) c l( / w ) K PVA C C
45 5. DNA 5. DNA 5.2 DNA DNA DNA TE ph 5.3 ) 30ml ) ) 3) 2) 4) 5) DNA DNA DNA DNA 6).5ml 70% 8 5) DNA 70% DNA DNA DNA TE ml DNA 5.4 DNA ) DNA DNA
46 A 0 H Buffer 2µ DNA 5 B Eco RI 0 H Buffer 2µ DNA 5 2 2) ) A B 20 00V DNA 3) ) DNA bp DNA 2 DNA 3 DNA 4 -DNA 5 -DNA DNA 5.5 DNA DNA
47 DNA DNA DNA DNA (A,T,G,C) DNA DNA(dNTPs) (EtBr) (DNA) UV =302m EtBr () DNA 5.3 DNA 5.6 DNA 4 GATC DNA Eco RIGAATTC Eco RI GAATTC CTTAAG H diii AAGCTT TTCGAA 5.4 DNA. 2.
48 6. 0
49 () (S Fe) NH 3 Cl NH 2 NaOH + N 2 Cl O N C0H7ONa ( 2)
50 7. 7. GCMS GCMS 7. Gas ChromatographGC Mass Spectrometer MS 7. GABA GCMS GCMS 405MPa GCMS Web Wkpedacaffee.3.7-(C 8 H 0 N 4 O 2 ) () C 8 H 0 N 4 O 2 H 2 O,C 8 H 0 N 4 O Wkpedahttp:// GCMShttp://
51 GABA A4 GCMS A4 g 7.2 GCMS GCMS
52 GCMS 6 GC7 MS 3 GCMS GCMS GCMS 7.6 M.W.= m GABA GCMS
53 7.3 GCMS GCMS 7.3 g 50cc 405MPa0 GCMS ON GCMS ON GCMS GCMS GCMS GCMS 7.3 ON GCMS ON GCMS GCMS OK OK 7.7 GCMD GCMS GC-MS
54 2 GCMS 7.8 GCMS 3GCMS 7.9 GCMS 4)
55 GC-MS RR
56
57 (x y )(=2) y= a 0 + a x y y = a + bx ) ( ε = y y ( a 0 a ) ) f (x) = a 0 + a x (A-) (A-) y e (A-2) e = y f (x ) = y ( a 0 + a x ) (A-2) (A-2) S S = = e 2 = = 2 { y ( a + a x )} (A-3) 0 S a 0 a (A-3) a 0 a S a 0 = = a 0 2 { y ( a0 + ax )} = 2 { y ( a0 + ax )} (A-4) = a S a = 2 [{ y ( a + a x )} x ] (A-5) = 0 S S a 0 S = 0 = 0 a (A-6) a 0 a (A-6) = y = = a0 + a x (A-7) = = y x = = a0 x + a x (A-8) = 2 (A-7)(A-8) a 0 a
58 = = = = = = = x x x x y y x a ) ( ) )( ( ) )( ( (A-9) = = = = = = x x y x x y a 2 2 ) ( ) )( ( ) ( (A-0) (A-9)(A-0) y = a 0 + a x y=a x+a 0 e x y y=a x+a 0 S S a 0 a y=a x+a 0 S=e ={y -(a x +a 0 )} S (S a 0 )=0 (S a )=0 2a 0,a S
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2011 ( ) ph H3O + H + H3O + HCl H3O + HCl + H2O H3O + + Cl HCl H + + Cl OH OH NaOH OH NaOH Na + + OH NH3 OH NH3 + H2O NH4 + + OH 1 H + OH H + H + * 1 NH3 HCl NH4Cl NH4Cl NH3 + Cl NH3 + HCl NH4 + + Cl.
[1.1] r 1 =10e j(ωt+π/4), r 2 =5e j(ωt+π/3), r 3 =3e j(ωt+π/6) ~r = ~r 1 + ~r 2 + ~r 3 = re j(ωt+φ) =(10e π 4 j +5e π 3 j +3e π 6 j )e jωt
![[1.1] r 1 =10e j(ωt+π/4), r 2 =5e j(ωt+π/3), r 3 =3e j(ωt+π/6) ~r = ~r 1 + ~r 2 + ~r 3 = re j(ωt+φ) =(10e π 4 j +5e π 3 j +3e π 6 j )e jωt](/thumbs/101/152334931.jpg "[1.1] r 1 =10e j(ωt+π/4), r 2 =5e j(ωt+π/3), r 3 =3e j(ωt+π/6) ~r = ~r 1 + ~r 2 + ~r 3 = re j(ωt+φ) =(10e π 4 j +5e π 3 j +3e π 6 j )e jωt")
3.4.7 [.] =e j(t+/4), =5e j(t+/3), 3 =3e j(t+/6) ~ = ~ + ~ + ~ 3 = e j(t+φ) =(e 4 j +5e 3 j +3e 6 j )e jt = e jφ e jt cos φ =cos 4 +5cos 3 +3cos 6 =.69 sin φ =sin 4 +5sin 3 +3sin 6 =.9 =.69 +.9 =7.74 [.]
欧州特許庁米国特許商標庁との共通特許分類 CPC (Cooperative Patent Classification) 日本パテントデータサービス ( 株 ) 国際部 2019 年 7 月 31 日 CPC 版が発効します 原文及び詳細はCPCホームページのCPC Revision
欧州特許庁米国特許商標庁との共通特許分類 CPC (Cooperative Patent Classification) 日本パテントデータサービス ( 株 ) 国際部 2019 年 7 月 31 日 CPC 2019.08 版が発効します 原文及び詳細はCPCホームページのCPC Revisions(CPCの改訂 ) をご覧ください https://www.cooperativepatentclassification.org/cpcrevisions/noticeofchanges.html
36 th IChO : - 3 ( ) , G O O D L U C K final 1
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