ICP-AES (ppbppm ICP-AES, ICP-MS, AA, IC GC, LC, GC-MS, LC-MS,LC-MS-MS U=u ( k=)
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- いぶき すえがら
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1 006106
2 ICP-AES (ppbppm ICP-AES, ICP-MS, AA, IC GC, LC, GC-MS, LC-MS,LC-MS-MS U=u ( k=)
3 A B -a a u = a 3 -a a u = a 6 u ( x) = u( x ) + u ( x ) + u ( x ) + + u ( x n ) 1 3, EURACHEM/CITAC guide Second Edition;1999
4 1 ICP-AES (0.1mol/L) ICP-AES (ml) C = x (ml) x (mg/l) x (mg/l) ICP-AES [ ] ICP-AES
5 1 0mL ml 0.1mol/L 100mg/L 10mg/L 0.mg/L ICP-AES ICP-AES (Vp) u(p) u(p1) u(p) u(p3) Vf u(f) u(f1) u(f) u(f3). (x o ) u(x o ) 3. (Cs) u(s) 100mg/L (Cs1) u(s1) 10mg/L (Cs) u(s) 0.mg/L (Cs3) u(s3)
6 [ ] u(p) u(p1) JIS R 30 (B u(p) 10 A u(p3) / (B
7 u(p) u(f1) JIS R 30 (B ) u(f) 10 (A u(f3) / (B 1. (ml) 0 (ml) 1) ) (ml) ) = = ) JIS R 30 ) 6 3): =0.01/0 = u(p1)/vp1 (ml) 0 (ml) 4 ) ) ): =0.0/0 = u(p)/vp
8 1. (ml) () 6 7) 0 / / ) ) : =0 / /0 = u(p3)/vp u( p) u( p1) u( p) u( p3) = + + = + + = Vp Vp1 Vp Vp u( f ) u( f1) u( f ) u( f3) = + + = + + = Vf Vf 1 Vf Vf
9 3 (ICP-AES) (mg/l) x ICP-AES y (ICP-AES) 66 (mg/l) 0.3 s xo 3. s 1 1 = + + ( yo y) yo b n m b x i x { } sy = y ( ) /( ) O i bxi+ a m ( ) 1/ y= bx+ a s : xo yo : b : n : m : y o : y : J.N.Miller,J.C.Miller / xi : : x :, (004).
10 x = = y = = xi x ( xi x)( yi y) sxy ( ) sx = = m sxy b = = a = y bx = 3.3 s x = = m s y O { y ( )} i bxi + a = = 9.80 ( m ) ( xi x) =.13 yo = 66 m= n= 1 3. s xo s 1 1 = + + ( y o y) yo b n m b xi x ( ) 1/ ( ) = = 0.01 mg/l 1/ s xo u(xo) x o =(66+3.3)/99.04=0.30mg/L u( xo) 0.01 mg/l = = x 0.30 mg/l o
11 3 100mg/L 10mg/L 0..0mg/L (mg/l) (100mg/L) (10mg/L) (ml) (ml) mg/L 100mg/L 1 1mg/L 1 mg/l us ( 1) = = 0.77 mg/l 3 us ( 1) 0.77 mg/l Cs 1 = 100 mg/l = 100mg/L :0.0077
12 (Cs) u(p) u(p1) JIS R 30 (B ) u(p) 10 (A ) u(p3) / (B (Cs) u(p) u(f1) JIS R 30 (B ) u(f) 10 (A u(f3) / (B
13 (ml) (ml) (ml) = = (ml) (ml) (ml) () 10 / / ( s) ( p1) ( p) ( p3) ( f 1) ( f ) ( f 3) ( s1) u u u u u u u u = Cs Vp1 Vp Vp3 Vf1 Vf Vf 3 Cs1 = =
14 mg/L u = (ml) (ml) /6)/ /3 /( /3 / /100 /100 10/100 1/100 0/ mg/L 0.mg/L + ( s3) ( p1) ( p) ( p3) ( f1) ( f ) ( f 3) ( s) u u u u u u u u = Cs3 Vp1 Vp Vp3 Vf 1 Vf Vf 3 Cs = = = mg/L.0mg/L
15 4 Vp 0mL Vf ml 0.3mg/L u Cs3 0..0mg/L x o u( p) u( f ) ( xo) u( s3) ( c) ( p) ( f ) ( xo) ( s3) u u u u u = C Vp Vf xo Cs3 = = C = 0.3 = 0.88mg/L 0.9mg/L 0 u ( c) = mg/L 0.01mg/L 0.01mg/L 0.01mg/L=0.03mg/L k=) 0.9mg/L0.03mg/L (k=)
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