( ) ( ) ( ) ( ) ( ) ( ) ( ) 1
2
3
4
5
6
7
8
9
10
(2450 MHz, 4.9 kw, Oven: W7m x D7m x H15m) 11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
1 1 cms 26
1kgf 27
3kgf 1.5m/s 151030 28
2 29
30
31
0.25MPa 0.1MPa 0.17MPa 20 NaA NaY T 32
NaA NaY ZSM-5 NaA NaY 33
NaA Na2O/SiO21SiO2/Al2O32 H2O/Na2O60180 34
NaY Na2O/SiO20.88SiO2/Al2O325 H2O/Na2O 4560 12mm 9mm 800mm 1m 40 NaA NaY 6070 3 2451MHz 0.5kW4.9kW 4001000mm 40150mm 35130mm 200mm H2O/Na2O75 Na2O/SiO21 SiO2/Al2O32 0.6kW 30 SEM 10m 5m IPA (95) 9 12mm 800mm 600 0.1Mpa 20 0.17Mpa 20 10 1.5 H2O/Na2O75Na2O/SiO21SiO2/Al2O32 200 0.6KW NaA 35
36
37
38
39
40
41
42
4237(2000) 45446(2000) (20005) 2000 No.12109(2000) 43
66 E115(2001) H. Kita Continuous Synthesis of Zeolitic Membrane by Microwave Heating International Workshop on Zeolitic and Microporous Membranes 2001 H. Kita, T. Harada, T. Shibata, X. Lin, K. Okamoto Microwave vs.conventional Hydrothermal Synthesis of LTA, FAU and MFI Zeolite Membranes and Their Permeation Properties 222 nd American Chemical Society Meeting 2001 44