.1.2.3.4.5.6.7.8.9 1. 4s FT.1.2.3.4.5.6.7.8.9 1. 6 µ 65 µ µ µ µ -CHF- -CHF- 65 14 14
µ 13 C 1 H 19 F -8 19 F -21 ( NOE buildup ) -CHF-
23[] 27[] MPF7 MPF8 3[] 34[] 16 [] MPF9 MPF1 15[] µ
' & % $ # "!!$!!! & # % " ' $! 5. 4. 3. 2. 1. X : parts per Million : 1H 5. 4. 3. 2. 1. X : parts per Million : 1H 2D=IA Amplitude 13. 12. 11. 1. 9. 8. 7. 6. 5. 4. 3. 2. 1. 13. 12. 11. 1. 9. 8. 7. 6. 5. 4. 3. 2. 1. 3.6 4
19 F 13 C Gz E-BURP1 1/2J RE-BURP F/2 F/2 t 1 1/2J acquire 12. 11. 1. 9. 12. 11. 1. 9. X : parts per Million : 19F X : parts per Million : 19F