Di(2-ethylhexyl) adipate C22H42O Dimethyl phthalate C10H10O Diethyl phthalate C12H14O D

Size: px
Start display at page:

Download "Di(2-ethylhexyl) adipate C22H42O Dimethyl phthalate C10H10O Diethyl phthalate C12H14O D"

Transcription

1 ) SVOC 1 Fluoranthene-d10 ( : C16D10 : : 99.3%) 2. SVOC m WHO 5.0 L/min 24 SVOC (Volatile Organic Compounds: VOC) (Semi Volatile Organic Compounds: SVOC) VOC SVOC 3. SVOC / (GC/MS) SVOC ( ) SVOC (Type 2500 QAT-UP) 3M Empore (High Performance Extraction Disks, 2215FF, C18) mg/ml 2 ( ) PropetamphosMGK-264Resmethrin EMO-47 MP-500 Hydramethylnon 5.0 mg/ml 400 4Thiabendazole2.0 mg/ml Empore 10 ml 10 5 SVOC 123g/ml Fluoranthene-d10 Acetone 5,000 ( PCB g/ml

2 Di(2-ethylhexyl) adipate C22H42O Dimethyl phthalate C10H10O Diethyl phthalate C12H14O Di-n-propyl phthalate C14H18O Di-iso-butyl phthalate C16H22O Di-n-butyl phthalate C16H22O Di-n-pentyl phthalate C18H26O Di-n-hexyl phthalate C20H30O Benzylbutyl phthlate C19H20O Di-n-heptyl phthalate C22H34O Dicyclohexyl phthalate C20H26O Di(2-ethylhexyl)phthalate C24H38O Triethyl phosphate C6H15O4P Tripropyl phosphate C9H21O4P Pfaltz&Bauer 97.0 Tributyl phosphate C12H27O4P Tris(2-chloroethyl) phosphate C6H12Cl3O4P Tris(1,3-dichloro-2-propyl) phosphate C9H15Cl6O4P Triphenyl phosphate C18H15O4P Tris(2-butoxyethyl) phosphate C18H39O7P Aldrich 94.0 Tris(2-ethylhexyl) phosphate C24H51O4P Tricresyl phosphate C21H21O4P # Dichlorvos C4H7Cl2O4P Diazinon C12H21N2O3PS Dichlofenthion C10H13Cl2O3PS Chlorpyrifosmethyl C7H7Cl3NO3PS Dr. Ehrenstorfer GmbH 99.5 Fenitrothion C9H12NO5PS Malathion C10H19O6PS Fenthion C10H15O3PS Dr. Ehrenstorfer GmbH 95.5 Chlorpyrifos C9H11Cl3NO3PS Tetrachlorvinphos C10H9Cl4O4P Pyridaphenthion C14H17N2O4PS Propetamphos C10H20NO4PS AccuStandard 97.8 Fenobucarb C12H17NO Carbaryl C12H11NO Propoxur C11H15NO Allethrin C19H26O Tetramethrin C19H25NO Dr. Ehrenstorfer GmbH 99.1 Phenothrin C23H26O Dr. Ehrenstorfer GmbH 94.5 Permethrin C21H20Cl2O Dr. Ehrenstorfer GmbH 97.5 Cyfluthrin C22H18Cl2FNO Dr. Ehrenstorfer GmbH 98.5 Deltamethrin C22H19Br2NO Dr. Ehrenstorfer GmbH 99.0 Empenthrin C18H26O Furamethrin C18H22O Prallethrin C19H24O Imiprothrin C17H22O4N Resmethrin C22H26O Bifenthrin C23H22ClF3O Cyphenothrin C24H25NO Riedel-de Haen 96.5 Ethofenprox C25H28O Silafluofen C25H29FO2Si Metoxadiazone C10H10N2O Fenoxycarb C17H19NO Methoprene C19H34O Dr. Ehrenstorfer GmbH 98.0 Pyriproxyfen C20H19NO Tripropyl isocyanurate C12H21N3O Hydramethylnon C25H24F6N AccuStandard ,3,3,3,2',3',3',3'-Octachlorodipropylether (S-421) C6H6Cl8O Riedel-de Haen 99.0 Piperonyl butoxide C19H30O MGK C17H25NO AccuStandard Chloronaphthalene C10H7Cl Chlorothalonil C8Cl4N Dichlofluanid C9H11Cl2FN2O2S Thiabendazole C10H7N3S (Thiocyanomethylthio)benzothiazole (TCMTB) C9H6N2S Supelco Iodo-2-propynyl-N-butylcarbamate (IPBC) C8H12INO Aldrich Bromo-3-ethoxycarbonyloxy-1,2-diiodo-1-propene () C6H7O3BrI p-chlorophenyl-3-iodopropargyl formal (IF-1000S) C10H8O2ClI Thiuram C6H12N2S Cyproconazole C15H18ClN3O Furmecyclox C14H21NO Riedel-de Haen 98.2 Difolatan C10H9Cl4NO2S Pentachlorophenol C6HCl5O N,N-Diethyl-m-toluamide (DEET) C12H17NO

3 MS EI 70eV 60A min SIM SVOC (Selective Ion Monitoring) g/ml 1.08 kv 0.2 sec (34.7 Auto Injector 20i 40.6 min 0.31 sec) 8 0.3ml (7.0 min l min) Empore 2 10ml 8 ml 10 SVOC SVOC 10 (2000 rpm10) SVOC (g/ml) / 5 ml (g/ml)(x) SVOC 3.0l / (y) SD905 ( 150 ml/min/ 30) 0.3 SVOC(ng) ml Auto Injector 20i SVOC(ng) {(SVOC GC/MS ) } (g/ml) GC/MS Auto 0.3(8/5)1000 Injector 20i GCMS-QP2010 Gas Chromatograph Mass Spectrometer SVOC SVOC (ng/m 3 ) GC J&W DB-1 ( 30 m SVOC (ng/m 3 ) 0.25 mm 0.25m) = { ( SVOC(ng) 68.4 kpa SVOC(ng))1000} 20.0 ml/min 1.14 (L/min) (h) ml/min ( 2.0) 60-5/min-300(10 ) l

4 1. 73 SVOC (15.0 Tetramethrin g/ml) (TIC) 1 SVOC 50 Imiprothrin Tricresyl phosphate Deltamethrin Hydramethylnon TIC SVOC (1 No ) SVOC (EmpenthrinFuramethrinAllethrin Prallethrin Imiprothrin Resmethrin PhenothrinCyphenothrin PermethrinCyfluthrinDeltamethrin) Tricresyl phosphate

5

6

7 MGK Chloronaphthalene Imiprothrin 90%50% SVOC 2. SVOC 3 adipate Tris (2-chloroethyl) phosphate SVOC030.0g/ml g/m 3 Thiuram IPBC EmpenthrinPentachlorophenol Chlorothalonil IF-1000S CarbarylFuramethrinFenitrothion SVOC DichlofluanidThiabendazoleAllethrin SVOC TCMTBPrallethrinCyproconazol ImiprothrinPiperonyl butoxidetris (2-butoxyethyl) phosphate SVOC PyridaphenthionFenoxycarbTris (2-ethylhexyl) phosphatepyriproxyfen Tricresyl phosphatecyphenothrin PermethrinCyfluthrinEthofenprox Deltamethrin Empore ( ) SVOC 120l ( 2058 ng/m 3 ) 4 (Control) 4 SVOC 5.0 L/min24 Empore ml Empore 2 SVOC ( Empore 4 Diethyl phthalate Di-iso-butyl phthalate Di-n-butyl phthalatedi (2-ethylhexyl) phthalate 2(Sample 1) Di (2-ethylhexyl) SVOC 8 Empore 3) 3 Empore (Sample 2) 4

8 24 Empore 1 (Blank) SVOC 6 5 (Sample) 6 (Control) 60l SVOC (%) ( 1029 ng/m 3 ) = { (Sample 1 SVOC8 ml * Blank SVOC 6 *) Control SVOC * } ml Blank Blank SVOC (%) SVOC = { Sample 2 SVOC * (Sample 1 SVOC *Blank SV OC *)}100 SVOC () Sample SVOC * * SVOC Control SVOC * 4Blank SVOC * 1-ChloronaphthaleneThiuram Blank SVOC * 100 Empenthrin Furmecyclox Furamethrin FenthionMGK-264 Allethrin Prallethrin * SVOC 6 MethopreneImiprothrinDifolatan ResmethrinTetramethrinPhenothrin 6.0l Cyphenothrin Hydramethylnon( 103 ng/m 3 ) 10% 6 SVOC Propetemphos 70% 100% SVOC Thiabendazole % 55 80% 24 1% L/min SVOC 2g/m 3 5. SVOC 5 SVOC

9

10 3 SVOC 0.12g/ml10 24 SVOC 7 Diethyl phthalate Di-iso-butyl phthalatedi-n-butyl phthalatedi (2-ethylhexyl) phthalate Di (2-ethylhexyl) adipate Tris (2-chloroethyl) phosphate6 4 Diethyl phthalatedi-n-butyl phthalate Di (2-ethylhexyl) phthalate 3 SVOC ng/m 3 SVOC0.5 ng/m 3 Di-n-butyl phthalate Di (2-ethylhexyl) phthalate SVOC IPBC PentachlorophenolChlorothalonil IF-1000S Carbaryl Fenitrothion DichlofluanidThiabendazoleTCMTB CyproconazolPiperonyl butoxidetris (2-butoxyethyl) phosphate PyridaphenthionFenoxycarbTris (2-ethylhexyl) phosphatepyriproxyfen Tricresyl phosphatepermethrin CyfluthrinEthofenprox Deltamethrin ( ) SVOC 60l ( 1029 ng/m 3 )

11 5.0 L/min24 Sample 3 Control Sample SVOC SVOC (ng/m 3 ) { (Sample SVOC(ng) Control SVOC(ng) *)1000} ( (L/min) (h) 60) *3 (n=5) 5.0L ( 86 ng/m 3 ) 8 60l 5.0l Cyfluthrin Deltamethrin SVOC 10% 2 SVOC 60l Pentachlorophenol Chlorothalonil Dichlofluanid ThiabendazoleDeltamethrin SVOC 10% 73 SVOC SVOC (Empenthrin 5.0l FuramethrinAllethrinPrallethrin SVOC 10% ImiprothrinResmethrinTetramethrin 13% PhenothrinCyphenothrin) SVOC 1-ChloronaphthaleneThiuram 2 FurmecycloxFenthionMGK-264 MethopreneDifolatanHydramethylnon Propetamphos18

12

13 Empore Thiabendazole 2 SVOC g/m 3 IPBCPentachlorophenolChlorothalonil IF-1000SCarbaryl FenitrothionDichlofluanidTCMTB CyproconazolPiperonyl butoxidetris (2-butoxyethyl) phosphate PyridaphenthionFenoxycarbTris (2-ethylhexyl) phosphatepyriproxyfen Tricresyl phosphatepermethrin CyfluthrinEthofenprox Deltamethrin 2 SVOC 5.0 L/min24 SVOC

NAGINATA化合物データ4.xls

NAGINATA化合物データ4.xls 農薬 環境汚染物物質 MCR-NAD-1 28 年 3 月版 ID 化合物名 Formula Page 1 アセナフテン-d1 C12D1 1 2 アセナフテン C12H1 1 3 アセナフチレン C12H8 2 4 アセフェート C4H1NO3PS 2 5 アセタミフ リト C1H11ClN4 3 6 アセトクロール C14H2ClNO2 3 7 アセトフェノン C8H8O 4 8 2-アセチルアミノフルオレン

More information

Microsoft Word - 14_LCMS_アクリルアミド

Microsoft Word - 14_LCMS_アクリルアミド 3--2-3-Iodo-2-propynyl butylcarbamate (IPBC) Carbamic acid, butyl-, 3-iodo-2-propynyl ester Iodocarb CAS 55406-53-6 C 8 H 12 NO 2 I C (g/cm 3 ) (mmhg) log P ow 281.09 (280.9910) 64 68 1.51 1.57 (20 C)

More information

<4D F736F F D F90858C6E5F C B B B838B>

<4D F736F F D F90858C6E5F C B B B838B> Isobutyl alcohol IUPAC 2-methylpropan-1-ol 2--1-2-Methyl-1-Propanol, Isobutanol CH 3 H 3 C OH CAS 78-83-1 C 4 H 10 O log P ow ( C) ( C) (kpa) (g/l) 74.12 74.14 1) -108 2) 108 2) 1.2 2) 87 2) 0.8 2) (74.1214)

More information

平成26年度 化学物質分析法開発報告書

平成26年度 化学物質分析法開発報告書 N,N- N,N-Dimethylacetamide Acethyldimethylamine CAS 127-19-5 C 4 H 9 NO 87.12 ~ 87.14 87.68413 163-165 C 1) - 18.59 C 2) 1 mg/l 25 C 3) 3.3 hpa 2 C 4) log P ow -.77 2).9429 2/4 C 1) 3.1 4) 1.31E - 8 atm-m

More information

まえがき

まえがき JAAS0012006 1 -------------------------------------------------------------------------------------------------------- 1 2 --------------------------------------------------------------------------------------------------------

More information

3 夢を実現した加熱脱着導入システム GERSTEL TDS A2, /3C, CIS 4 -GC VVOC SVOC GERSTEL TDS A2 /3C CIS 4 Agilent 7890GC 5977MSD 1バルブレス流路を実現したオートサンプラー SVOC C 20 TDS A2 CIS

3 夢を実現した加熱脱着導入システム GERSTEL TDS A2, /3C, CIS 4 -GC VVOC SVOC GERSTEL TDS A2 /3C CIS 4 Agilent 7890GC 5977MSD 1バルブレス流路を実現したオートサンプラー SVOC C 20 TDS A2 CIS GERSTEL /3C 加熱脱着導入システム C www.gerstel.co.jp 3 夢を実現した加熱脱着導入システム GERSTEL TDS A2, /3C, CIS 4 -GC VVOC SVOC GERSTEL TDS A2 /3C CIS 4 Agilent 7890GC 5977MSD 1バルブレス流路を実現したオートサンプラー SVOC C 20 TDS A2 CIS 4 Agilent

More information

Group A (2,5-Dimethoxyphenyl type) 25D-NBMe (1) 25B-NBMe (2) 25I-NBMe (3) 25C-NBF () 25B-NBF (5) Group B (Benzofuran-2-yl type) Group C (-Alkoxy-3,5-d

Group A (2,5-Dimethoxyphenyl type) 25D-NBMe (1) 25B-NBMe (2) 25I-NBMe (3) 25C-NBF () 25B-NBF (5) Group B (Benzofuran-2-yl type) Group C (-Alkoxy-3,5-d 3 * * * * * Analytical data of designer drugs of synthetic phenethylamines Ryosuke SASAKI*, Miho KAT*, Tsuyoshi MATSUMT*, Akira UDAGAWA* and Ryuichi MATSUZAKI* *Tokyo Customs Laboratory 2-7-11, Aomi, Koto-ku,

More information

57 Isofenphos-methyl イソフェンホス-メチル C14H22NO4PS Isoprocarb イソフ ロカルフ C11H15NO Isoprothiolane イソフ ロチオラン C12H18O4S2 290

57 Isofenphos-methyl イソフェンホス-メチル C14H22NO4PS Isoprocarb イソフ ロカルフ C11H15NO Isoprothiolane イソフ ロチオラン C12H18O4S2 290 1 1,3,5-Trinitrobenzene 1,3,5-トリニトロヘ ンセ ン C6H3N3O6 213 99-35-4 2 2-(1-naphtyl)acetamide 2-(1-ナフチル ) アセタミト C12H11NO 185 86-86-2 3 2,6-Dichlorobenzamide 2,6-シ クロロヘ ンス アミト C7H5Cl2NO 189 2008-58-4 4 a-bhc

More information

☆H23 13-農薬一斉分析(大垣).doc

☆H23 13-農薬一斉分析(大垣).doc 13 56 2011 Examination of Determination of Residual Pesticides in Agricultural Products Yuki OHGAKI, Katsuhiro HAYASHI, Hiroyuki KAWAI, and Kyoko SHIMURA GC/MS 92 LC/MS/MS 60 150 n- 5 GC/MS 92 79 70% LC/MS/MS

More information

<4D F736F F D C6E30385F A B B83932E444F43>

<4D F736F F D C6E30385F A B B83932E444F43> 1,2,4-1,2,4-Trimethylbenzene Pseudocumene 1,3,5-1,3,5-Trimethylbenzene Mesitylene CH 3 CH 3 CH 3 CH 3 CH 3 CH 3 1,2,4-trimethylbenzene 1,3,5-trimethylbenzene CAS 95-63-6 CAS 108-67-8 C 9 H 12 C 9 H 12

More information

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物)

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物) N- 1) 2) 1) GC/MS HPLC GC/MS 2) 0.01~0.05µg/l 0.5~50µg/kg GC/MS SIM GC/MS SIM GC/MS SIM a) b) -d 10 -d 10 -d 12 -d 12 c) d) 600 C 4 e) 1 99.999% f) a) b) - IX-1 - c) (ODS) 200-1,000mg 5ml 5ml 5ml d) e)

More information

取扱説明書 [F-12C]

取扱説明書 [F-12C] F-12C 11.7 1 2 3 4 5 6 7 8 9 10 11 12 13 14 a bc b c d d a 15 a b cd e a b c d e 16 17 18 de a b 19 c d 20 a b a b c a d e k l m e b c d f g h i j p q r c d e f g h i j n o s 21 k l m n o p q r s a X

More information

LC/TOF-MS MS ( )

LC/TOF-MS MS ( ) LC/TOF-MS MS () (TOF-MS) MS) LC/MS 1. 2. Agilent 1100 LC/TOF-MS MS ~0.25ppm / C ambient Compound Exact mass Positive Negative Purine 121.050873 TFA 112.985587 Hexakis(1H, 1H, 3H 922.009798 966.000725 1)

More information

untitled

untitled 18 HNS HNS HNS HNS HNS HNS HNS 19 3 18 HNS 18 6 14 OPRCHNS 18 68 19 4 1 20 4 1 OPRCHNS 18 6 14 15 19 6 14 17 HNS 19 2 1 1 3 4 5 5 5 7 8 10 13 13 15 15 10 16 HNS 17 HNS 18 HNS 19 HNS 20 21 22 23 39 61 61

More information

ッ ー ー ー() () 2.5 () () 21 1) -1 2) -2 10 m 5 7 23 6 1)2) 3) -1-2 H23.4.25 -15-20 4 75 5 1) -1 (5) (3) (3) (2) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) 1) ( 23 6 8 ) 2) 22 3)

More information

食糧 その科学と技術 No.46( )

食糧 その科学と技術 No.46( ) , IARC A ppb ppm, WHOµg/L GC GC GCMS GC MS, d O O O NH 2 Br 2 NEt 3 Br NH 2 NH 2 Br Br GC, [C H NO Br] + m/z [C H NO Br] m/z SIM [C H D NO Br] m/z [C H D NO Br] + m/z Br Br HBr [C H NO Br] + m/z GC -d

More information

Ⅱ6.3界面活性剤

Ⅱ6.3界面活性剤 6.3 6.3.1 6.3.1 6.3.1.1 (1) (2) a) JIS K 0557 A3 b) JIS K 8891 c) (5g/L) d) (10g/L)JIS K 8576 1g 100mL e) (7+993)JIS K 8951 f) JIS K 8322 g) 0.1g 100mL 30mL 1L 500mL6.8mL 50g 1L h) 1L 500mL6.8mL 50g 1L

More information

-------------------------------------------------------------------------------------------------- 1 ----------------------------------------- 3 --------------------------------------------------------------------------------

More information

取扱説明書 [F-02F]

取扱説明書 [F-02F] F-02F 4. 2 3 4 5 6 7 8 9 0 2 3 4 5 6 7 8 a b c d a b c d a b cd 9 e a b c d e 20 2 22 ab a b 23 a b 24 c d e 25 26 o a b c p q r s t u v w d h i j k l e f g d m n a b c d e f g h i j k l m n x 27 o

More information

広大な敷地に多数のケミストが在籍 ラボスケールからバルクスケールまで対応 医薬品原料 中間体として 製品を世界的に供給 Bicyclo[1.1.1]pentanes PB05031 bicyclo[1.1.1]pentane-1,3- dicarboxylic acid C7H

広大な敷地に多数のケミストが在籍 ラボスケールからバルクスケールまで対応 医薬品原料 中間体として 製品を世界的に供給 Bicyclo[1.1.1]pentanes PB05031 bicyclo[1.1.1]pentane-1,3- dicarboxylic acid C7H Bicyclo[1.1.1]pentanes PB05031 bicyclo[1.1.1]pentane-1,3- di 56842-95-6 C7H8O4 156.14 PB05032 1,3-dimethyl bicyclo[1.1.1]pentane -1,3-dicarboxylate 115913-32-1 PB05524 methyl 3-aminobicyclo[1.1.1] 758684-88-7

More information

橡19-25.PDF

橡19-25.PDF 1. ( ) (CR) VOC) VOC VOC CR (p&t) GC/MS VOC 2mm 50 100ml/min P&T 12mm 1,000 3,000m min P&T V( 2.CR 2-1CR Fig.1 12mmi.dx110mm 2.5g TenaxGR AL-410 AL-430 AC100V 1,000ml/min VOC 10 ( 3 ) VOC P&T-GC/MS JHS-100/100A

More information

要調査項目等調査マニュアル

要調査項目等調査マニュアル PBDEs TriBDE DeBDE 1 TriBDE 8 TeBDE 6 PeBDE 8 HxBDE 7 HpBDE 5 OcBDE 3 NoBDE 2 DeBDE 40 GC/MS 1 1 1 ng/l µg/kg, dry µg/kg TriBDE 0.1 0.01 0.01 TeBDE 0.1 0.01 0.01 PeBDE 0.1 0.01 0.01 HxBDE 0.1 0.01 0.01

More information

untitled

untitled 2017 5 26 350 Restek time time time increasing time μ = = k = t r t o t o = t r ' t o van Deemter Equation H A B H = height equivalent theoretical plate (HETP) A = Eddy diffusion term B = Molecular diffusion

More information

平成25年度 化学物質分析法開発報告書

平成25年度 化学物質分析法開発報告書 2,4-2,4-Dimethylaniline 2,4-2,4-Xylidine CH 3 CH 3 CAS 95-68-1 C 8 H 11 N 121.18 121.0892-14.3 C 2) 214 C 2) 0.9723 g/cm 3 2) 0.133 mmhg (25 C) 1) 1390 mg/l (25 C) 1) 3.710 3 mg/l 25 C WSKOWWIN 5) 6.0710

More information

48 13 13 13 38 21 13 3 13 3.1 l l l l l l 4.1.1 5mm 0.5mm 5mm 10 500mL 500mL 500mL 20 1 200 / 4 5 6 3000G 20 G1118 R N 2 10-8 GG Rcm Nrpm 1μm 2 3000G 1 /1 4.1.2PCB PCB 5mm 0.5mm 5mm 10 500mL 500mL 500mL

More information

橡A PDF

橡A PDF 2 1 MS 300 TRT MS JDI-800 2 g MS Py MS GC Py-GC Py GC 50 Py MS MS Py GC PY-GC 2 JDI-800 MS JDI-800 QP 2000 QP 1000 QP 2000 Fig 1 QP 1000 CI PEG 300 600 423 MS EI CI MS PEG 3 10 g Fig.1 300 600 MS 3 JDI-800

More information

154 CAT. NO. OP 2 EPA8141 71000 µg/ml 1mL 861283 13,300 Su B Bromacil Butachlor Metolachlor Prometon 9500 µg/ml 1mL 47728-U 12,300 Su -Chlordane -Chlo

154 CAT. NO. OP 2 EPA8141 71000 µg/ml 1mL 861283 13,300 Su B Bromacil Butachlor Metolachlor Prometon 9500 µg/ml 1mL 47728-U 12,300 Su -Chlordane -Chlo 153 CAT. NO. 7100 µg/ml 1mL CRM48392 10,100 Su CRM Ametryn Prometryn Terbutryn Propazine Prometon 31000 µg/ml 2mL 33417-2ML-R 5,400 F Cyfluthrin -Cypermethrin Flumethrin EPA8151 18 1mL 48996-U 17,600 Su

More information

ヒト血漿中オキシステロールの高感度分析法

ヒト血漿中オキシステロールの高感度分析法 High sensitive determination of oxysterols in human plasma using gas chromatography-mass spectrometry (GC-MS) Saori Nakagawa and Susumu Yamato Oxysterols, cholesterol oxidation products, have been important

More information

2 3

2 3 Sample 2 3 4 5 6 7 8 9 3 18 24 32 34 40 45 55 63 70 77 82 96 118 121 123 131 143 149 158 167 173 187 192 204 217 224 231 17 285 290 292 1 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38

More information

新潟県保健環境科学研究所年報第 24 巻 加工食品中の残留農薬分析法の検討 小林ゆかり, 土田由里子, 岩崎奈津美, 丹治敏英 Determination of Residual Pesticides in Processed Foods Yukari Kobayashi, Yuri

新潟県保健環境科学研究所年報第 24 巻 加工食品中の残留農薬分析法の検討 小林ゆかり, 土田由里子, 岩崎奈津美, 丹治敏英 Determination of Residual Pesticides in Processed Foods Yukari Kobayashi, Yuri 新潟県保健環境科学研究所年報第 24 巻 2009 73 加工食品中の残留農薬分析法の検討 小林ゆかり, 土田由里子, 岩崎奈津美, 丹治敏英 Determination of Residual Pesticides in Processed Foods Yukari Kobayashi, Yuriko Tsuchida, Natsumi Iwasaki and Toshihide Tanji Keywords:

More information

untitled

untitled Frank David Research Institute for Chromatography President Kennedy Park B- Kortrijk, Belgium Pat Sandra University of Gent Krijgslaan 281 S4, B-9000 Gent Belgium Allen K. Vickers Agilent Technologies,

More information

<4D F736F F D2089BB8A7795A88EBF82C68AC28BAB2E646F63>

<4D F736F F D2089BB8A7795A88EBF82C68AC28BAB2E646F63> ( 株 ) 島津テクノリサーチ 二硝酸プロピレン 1,2-propanediol,dinitrate 対象物質及び構造式 O O N O O N O O 分子式 C 3 H 6 N 2 O 6 CAS 番号 6423-43-4 物性 分子量沸点 ( ) 蒸気圧 (Pa) 水溶解度 (g/l) LogPow 166.11 121( 分解 ) 92(10 mmhg) 0.42 (3.16 10-3 mmhg

More information

3 DI 29 7 1 5 6 575 11 751, 13 1,1,25 6 1,251,5 2 1,51,75 1,752, 1 2,2,25 2,252,5 2,53, 3,3,5 3,5 5 1 15 2 25 3 5 6 575 12 751, 21 1,1,25 27 1,251,5 9 1,51,75 1,752, 1 2,2,25 2 2,252,5 2,53, 2 3,3,5

More information

% 32.3 DI DI

% 32.3 DI DI 2011 7 9 28.1 41.4 30.5 35.8 31.9% 32.3 DI 18.2 2.4 8.1 3.5 DI 9.4 32.2 0.0 25.9 2008 1 3 2 3 34.8 65.2 46.753.8 1 2 8.82.9 43.1 10 3 DI 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25

More information

31, 21% 24, 17% 8, 5% 23, 16% 24, 16% 91, 62% 19, 13% 39, 27% 33, 23% 73 48 57 51 31 1 9 13.0% 7.4% 5.3% 12.5% 17.1% 13.2% 17.9% 4.5% 36.4% 56.5% 40.7% 36.8% 50.0% 67.1% 56.3% 65.8% 75.0% 26.0% 37.0%

More information

2 DI 28 7 1 37 28 4 18 27 11 21 5 2 26 4 5 1 15 2 25 3 35 4 17 7 5 48 76 31 47 17 2 92 12 2 2 4 6 8 1 12 1 2 4 1 12 13 18 19 3 42 57 57 1 2 3 4 5 6 1 1 1 3 4 4 5 5 5.5 1 1.5 2 2.5 3 3.5 4 4.5 5

More information

37 27.0% 26 19.0% 74 54.0% 9 6.4% 13 9.2% 28 19.9% 26 18.4% 37 26.2%. 24 17.0% 99 69 75 59 39 1 6 4.5% 1.4% 7.7% 2.9% 25.0% 17.9% 20.8% 50.0% 41.7% 47.0% 51.4% 54.3% 61.5% 57.1% 55.6% 42.4% 50.0% 58.3%

More information

大型トランス等に係る現場解体作業について(抜油及び付属品取外し作業)

大型トランス等に係る現場解体作業について(抜油及び付属品取外し作業) 炁 PM2.5 DEP i 1 3 3 8 10 13 13 22 34 34 34 ii iii PCB PCB 15 4 16 4 PCB PCB 1 PCB 6 PCB 1 2 PCB ( ) 3 4 6kV 60kV 1m PCB 500kVA 1,300kg 3,300V 5 6 ( ) 2,000kW 5,750kg 2,200L 1.6 x 1.3 x 2.4m 3.1m 350kg

More information

2 / 102

2 / 102 1 / 102 2 / 102 ... 5... 21... 21... 21... 22... 23... 23... 23... 29... 29... 34... 39... 39... 40... 53... 59... 59... 59... 60... 60... 64... 65... 68... 74... 75... 78... 84... 84... 84... 85... 86...

More information

効率化計画冊子ファイナル.PDF

効率化計画冊子ファイナル.PDF - 1 - - 2 - - 3 - - 4 - - 5 - - 6 - - 7 - - 8 - - 9 - - 10 - - 11 - - 12 - - 13 - - 14 - - 15 - - 16 - - 17 - (77kV) (6kV) (77kV6kV 6kV - 18-77kV 10%20% - 19 - - 20 - - 21 - - 22 - - 23 - - 24 - DB( )

More information

取扱説明書 [F-08D]

取扱説明書 [F-08D] 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 a bc d a b c d 17 a b cd e a b c d e 18 19 20 21 22 a c b d 23 24 a b c a b c d e f g a b j k l m n o p q r s t u v h i c d e w 25 d e f g h i j k l m n o p q r s

More information

LCMS14003:UHPLC-Orbitrap質量分析計による環境汚染物質のターゲット分析、ノンターゲット分析

LCMS14003:UHPLC-Orbitrap質量分析計による環境汚染物質のターゲット分析、ノンターゲット分析 UHPLC Orbitrap Application Note LCMS14003 Orbitrap CEC CEC 61 CEC 312 CEC SPE UHPLCThermo Scientifi c Orbitrap Thermo Scientifi c TraceFinder WWTP S1 PS 5 ºC S2 TWAS 5 ºC 1 WWTP 1 2 WWTP 2 1 2 S1 1 S2

More information

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物)

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物) (PCB) 1 ng/l (µg/kg, wet) (µg/kg) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001)

More information

橡J0021-1.PDF

橡J0021-1.PDF 1 1950 60 PE PP PVD C PVC FT-lR DS C XRF GC LC 1 HS GC 2 2 1 2 1 GC GC 80 5 3 3 200 2 PVC 2 3 2 2 4 JHS 100 5 10ml GC 5 JHS-100 3 3 1 JHS 100A QP 5000 GC MS 6 1 1 TC-WAX 0.25mm 60m 40 180 5 /min--- 280

More information

理解のための教材開発と授業 (宮内).PDF

理解のための教材開発と授業 (宮内).PDF - 25 - Y ( ) () () Y - 26 - CD Y Y Y Y Y Y Y - 27-10 11 12 Y Y - 28 - Y 100 6 2 4 Y PTA Y Y Y - 29 - 1 Y Y Y Y - 32 - T Y Y Y T Y Y T Y T Y T Y T T Y Y T db Y Y T Y B T - 34 - T Y Y T Y T Y T Y Y T

More information

服用者向け_資料28_0623

服用者向け_資料28_0623 1 2 3 1. 2. 4 3. 4. 1. 5 2. 3. 4. 5. 6 6. 7. 8. 7 9. 10. 11. 8 12. 9 10 11 12 Q-1 : OC Q-2 : OC Q-3 : 21 OC 28 OC 13 Q-4 : OC Q-5 : OC Q-6 : OC 14 Q-7 : Q-8 : OC Q-9 : OC Q-10 : OC Q-11 : OC 15 Q-12 :

More information

環境調査(水系)対象物質の分析法

環境調査(水系)対象物質の分析法 環境調査 ( 水系 ) 対象物質 物質名 分析法フローチャート 備考 水質 (1) ニトロベンゼン GC/MS(SIM) 試料 500ml 連続水蒸気蒸留抽出脱水カラム :DB-17 (2) p -クロロカラム長 :30m ニトロベンゼン NaCl 15g 内径 :0.25mm 精油定量装置無水 Na2SO4 サロゲート溶液膜厚 :0.5μm ヘキサン5ml 検出限界 : 底質 1ml 内標準溶液

More information

< F836F A815B934B8D87955C E706466>

< F836F A815B934B8D87955C E706466> 92897 92893 10,000 92894 10,600 92895 11,300 92896 11,900 92897 11,900 92898 15,200 2 92888 92873 4,200 92874 4,200 92875 7,000 92876 7,000 92877 7,000 92878 8,800 92879 8,800 92880 13,300 92881 8,800

More information

Metabolomic Profiling_JA.qxp

Metabolomic Profiling_JA.qxp LC/MS-TOF LC/Q-TOF GeneSpring MS BLB: Bacterial Leaf Blight Steven Fischer Senior Application Chemist Agilent Technologies Santa Clara, California U.S.A Theodore Sana Senior Research Scientist Agilent

More information

2

2 1 2 3 4 5 6 7 2007 30,870 2008 32,426 2009 34,971 13,000 8 9 http://www.hokkaido-marathon.com/volunteer/ http://www.hokkaido-marathon.com/volunteer/leader.html 2009 / http://www.shonan-kokusai.jp/archives/volunteer/

More information

untitled

untitled NO. 2007 10 10 34 10 10 0570-058-669 http://www.i-nouryoku.com/index.html (40 ) () 1 NO. 2007 10 10 2.2 2.2 130 70 20 80 30 () () 9 10 () 78 8 9 () 2 NO. 2007 10 10 4 7 3 NO. 2007 10 10 40 20 50 2 4 NO.

More information

untitled

untitled -- -- -3- % % % 6% % % 9 66 95 96 35 9 6 6 9 9 5 77 6 6 5 3 9 5 9 9 55 6 5 9 5 59 () 3 5 6 7 5 7 5 5 6 6 7 77 69 39 3 6 3 7 % % % 6% % % (: ) 6 65 79 7 3 36 33 9 9 5 6 7 3 5 3 -- 3 5 6 76 7 77 3 9 6 5

More information

N N 1,, N 2 N N N N N 1,, N 2 N N N N N 1,, N 2 N N N 8 1 6 3 5 7 4 9 2 1 12 13 8 15 6 3 10 4 9 16 5 14 7 2 11 7 11 23 5 19 3 20 9 12 21 14 22 1 18 10 16 8 15 24 2 25 4 17 6 13 8 1 6 3 5 7 4 9 2 1 12 13

More information

CFASDM004

CFASDM004 CFASDM CFASDM CFASDM CFASDM JIS T 8001:1992 JIS T 8001 1 CFASDM 5. a) 2 CFASDM b) c) a) b) c) a) b) c) 24V 1) 2) 3) 1) 2) 3) 3 CFASDM 1) 2) 7.1.1 a) b) c) 7.1.2 d)7.1.3 a) b) c) 7.1.4 30N 7.1.4 30N 7.1.4

More information

平成26年度 化学物質分析法開発報告書

平成26年度 化学物質分析法開発報告書 2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)

More information

平成26年度 化学物質分析法開発報告書

平成26年度 化学物質分析法開発報告書 2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)

More information

100km/h COMAND * 250 i

100km/h COMAND * 250 i CL-Class 100km/h COMAND * 250 i http://www.mercedes-benz.co.jp/ G! i H 3 4 13 19 29 COMAND 57 69 253 295 369 4 252 52 48 285 13 16 13 14 15 17 14 103 104 88 89 88 356 21 21 22 126 126 126 127 127 279 378

More information

<352E8B5A8F7095F18D90328AEC91BD2E696E6464>

<352E8B5A8F7095F18D90328AEC91BD2E696E6464> No.29, 2015 13 Development of Cat Repellent Using Excrement of Fierce Animals Koji Kita Reiko Yamashita Yoshitaka Ota Hidenobu Hoshi (2015 6 30 ) 1. ( ) 2011 83,000 1) ( ) ( ) ( ) 2) (GC/MS) ( ) 4 2. 2.1

More information

O157 6/23 7/4 6 25 1000 117,050 6 14:00~15:30 1 2 22 22 14:30~15:30 8 12 1 5 20 6 20 10 11 30 9 10 6 1 30 6 6 0 30 6 19 0 3 27 6 20 0 50 1 2 6 4 61 1 6 5 1 2 1 2 6 19 6 4 15 6 1 6 30 6 24 30 59

More information

untitled

untitled 2001 4 26 2003 5 22 2004 7 12 2004 7 15 54 2004 7 21 14 2004 9 16 62 IUPAC4--2--N,N --5-p --1-2 17.07 mg/kg / 100 0.17 mg/kg /ADI cyazofamidiso IUPAC 4--2--N,N- -5-p --1-4-chloro-2-cyano-N,N -dimethyl-5-p

More information

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物)

外因性内分泌攪乱化学物質調査暫定マニュアル(水質、底質、水生生物) p,p -DDT p,p -DDE p,p -DDD trans- cis- trans- cis- (PBB) (BaP) 25ng/L 5µg/kg GC/MS-SIM GC/MS-SIM GC/MS-SIM GC/MS-SIM (2-, 3-, 4- ) (4,4'- ) p,p'-ddt- 13 C 12 HCB- 13 C 6 BaP-d 12 -d10 -d 10 p- -d 14 1000

More information

PALL NEWS vol.126 November 2017

PALL NEWS vol.126 November 2017 PALL NEWS November 2017 Vol.126 PALL NEWS vol.126 November 2017 NEW =2000 9660 41.4 MPa 24 MPa NFPA T2.06.01 R2-2001 CAT C/90/* (1x10 6 0-28 MPa 1x10 6 29 120 C 60 C 450 Pa 340 Pa 1 MPa JIS B 8356-3/ISO

More information

Japanese Journal of Pesticide Science 42(1): (2017)

Japanese Journal of Pesticide Science 42(1): (2017) 42(1), 203 203 215 (2017) DOI: 10.1584/jpestics.W17-54 1, * 2, ** 3, *** 4, **** 4 1 2 3 4 2017 1 6 Recent data analysis technique in mass spectrometry Takaya Satoh, 1 Kentaro Takahara, 2 Tomoaki Kondo,

More information

untitled

untitled (1972 UNEP(1972 (1989 UNCED(1992 WSSD(2002 19 Strategic Approach to International Chemicals Management) PCB 2001 80/1107/EEC1980 1994 Restriction of the Use of Hazardous Substances in Electrical and Electronic

More information

Microsoft Word - 5MS.doc

Microsoft Word - 5MS.doc 5 5.1 mass spectrometer electron impact, EI 5.1 :;"< 789 =>? *!"#$%& '%&(),,,-./ 0.12%3456 :;"@AB CDEFG:;"HIJK@LMN :;"@HIOPQ0RST6 5.1. 70 ev molecular ion #"$%& M M e!"!"'() #" m/z ; m = z = 1 mass spectrum,

More information

2章.doc

2章.doc C 2 H 4 N 2 O 2 LPG LIF 13 2.1 2.1.1 2.1 2.2 115mm70mm 727cm 3 Hand Pump Injector Driver Computer Constant Volume Chamber Injector Piezo-electronic transducer Fan Spark Plug Temperature Indicator C 2 H

More information

17. (1) 18. (1) 19. (1) 20. (1) 21. (1) (3) 22. (1) (3) 23. (1) (3) (1) (3) 25. (1) (3) 26. (1) 27. (1) (3) 28. (1) 29. (1) 2

17. (1) 18. (1) 19. (1) 20. (1) 21. (1) (3) 22. (1) (3) 23. (1) (3) (1) (3) 25. (1) (3) 26. (1) 27. (1) (3) 28. (1) 29. (1) 2 1. (1) 2. 2 (1) 4. (1) 5. (1) 6. (1) 7. (1) 8. (1) 9. (1) 10. (1) 11. (1) 12. (1) 13. (1) 14. (1) 15. (1) (3) 16. (1) 1 17. (1) 18. (1) 19. (1) 20. (1) 21. (1) (3) 22. (1) (3) 23. (1) (3) 24. 1 (1) (3)

More information

untitled

untitled CL-Class * * G H! i 100km/h COMAND i http://www.mercedes-benz.co.jp/ 3 4 15 23 33 COMAND 67 79 293 341 409 4 254 255 255 257 291 61 58 247 248 248 328 15 19 15 16 15 18 20 16 116 116 99 99 99 395 24 24

More information

橡マニュアルv4c.PDF

橡マニュアルv4c.PDF LC/MS MS LC/MS LC LC (APCI) (ESI) FAB 2 LC (APCI) 4.1.1.1 LC LC/MS LC MS LC 3 ph APCI/MS LC (1) APCI ESI 100% 100% ESI 4.1.1-1 LC 1.00cp 100 34 a 4.1.1-1 LC b ( /mpas) n- 0.23 36 0.5 99 0.31 69 n- 0.92

More information