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1 溶媒工業溶媒 Column : Equity-, 0 m x 0. mm ID,.0 µm Cat. No. : 0- Column : SPELCOWAX 0, 0 m x 0. mm ID,.0 µm Cat. No. : Column : Equity-0, 0 m x 0. mm ID,.0 µm Cat. No. : - Oven : ( min), /min to 0 ( min) Inj.: 0 Det. : FID, 0 Carrier gas: Helium, Injection : 0. µl, split 00: Liner : Split, cup design Sample : 0. µl of a component neat solvent mixture Equity-. Methanol. Methyl formate. Ethanol. Acetone. -Propanol. Ethyl formate.,-dichloroethylene. Methylene chloride. Methyl acetate 0. -Propanol. trans-,-dichloroethylene.,-dichloroethane. -Butanone. sec-butanol. Hexane. Ethyl acetate. Chloroform. Tetrahydrofuran. Isobutanol 0. -Methoxyethanol.,-Dichloroethane.,,-Trichloroethane. Isopropyl acetate. n-butanol. Benzene. Carbon tetrachloride. -Nitropropane. Trichloroethylene.,-Dioxane 0. -Ethoxyethanol (cellosolve). n-propyl acetate. -Methyl--pentanone. Isoamyl alcohol. Dimethylformamide. Toluene. Isobutyl acetate. -Hexanone. Mesityl oxide. Tetrachloroethene 0. n-butyl acetate,,. Diacetone alcohol. Chlorobenzene. -Methyl--hexanone. Ethyl benzene. m-xylene. p-xylene. Isoamyl acetate. Cyclohexanol. Styrene 0. o-xylene.,,,-tetrachloroethane. -Ethoxyethyl acetate. Butyl cellosolve. n-amyl acetate. -Methylcyclohexanol.,-Dichlorobenzene. -Methylphenol. -Methylphenol. -Methylphenol,, 0,0 0,, 0,, ,, SPELCOWAX0 G00, 0 0,0,,,,, 0 0,,, G00 Equity-0,,,,,,, 0 0, 0 0 0,, G00 0

2 溶媒工業溶媒 Column : PTE -, 0 m x 0. mm ID,.0 µm film Cat. No. : Oven : 0 ( min.), /min to 0 Inj.: 00 Carrier gas: Helium, 0 Det. : FID Inj.: µl, split 00 : Sample : mixed solvents, 0, Column : SPELCOWAX 0, 0 m x 0. mm ID,.0 µm film Cat. No. : 0- Oven. : 0 ( min.), /min. to 00 Inj. : 0 Carrier gas: Helium, ml/min. Det. : FID Inj.: µl, split 0: Sample : mixed solvents 0 溶媒工業溶媒, 0 0,, 0. Hexane.,-Dichloroethylene. Acetone. Methyl acetate. trans-,-dichloroethylene. Tetrahydrofuran. Carbon tetrachloride.,,-trichloroethane.,-dichloroethane,, 0 0. Ethyl acetate. Methanol. Isopropyl acetate. Methyl ethyl ketone. Isopropanol. Methylene chloride. Benzene. Propyl acetate. Trichloroethylene. Methyl isobutyl ketone 0. Isobutyl acetate. Chloroform. Tetrachloroethylene. -Butanol. Toluene.,-Dioxane.,-Dichloroethane. n-butyl acetate. -Hexanone (MBK). Isobutanol 0. Isoamyl acetate. p-xylene. m-xylene. -Butanol. Methyl Cellosolve. Amyl acetate. o-xylene. Isoamyl alcohol. Chlorobenzene. Cellosolve 0. Styrene. Cyclohexanone. N,N-Dimethylformamide. Cyclohexanol. Butyl Cellosolve. -Methylcyclohexanol.,-Dichlorobenzene.,,,-Tetrachloroethane. o-cresol. p-cresol 0. m-cresol,,, 0,,, 0, 0,

Column : SPB-, 0 m x 0. mm ID,.0 µm film Cat. No. : 0- Oven : 0 ( min.) to at /min., ( min.) Inj. : 0 Carrier gas: Helium, cm/sec @ 0 Det. : FID, 0 Inj.: 0. µl, split 00 : Sample : approximately equal proportions of each component 0, 溶媒工業溶媒.

3 Column : SPB-, 0 m x 0. mm ID,.0 µm film Cat. No. : 0- Oven : 0 ( min.) to at /min., ( min.) Inj. : 0 Carrier gas: Helium, 0 Det. : FID, 0 Inj.: 0. µl, split 00 : Sample : approximately equal proportions of each component 0, 溶媒工業溶媒. Methanol. Methyl formate. Ethanol. Acetone. Isopropyl alcohol. Ethyl formate. Methylene chloride. n-propyl alcohol. Methyl ethyl keton 0. sec-butyl alcohol. Ethyl acetate. Chloroform. Tetrahydrofuran. Methyl Cellosolve. Isobutyl alcohol.,,-trichloroethane. Isopropyl acetate. n-butyl alcohol. -Nitropropane 0.,-Dioxane. Ethyl Cellosolve nknown. Methyl isobutyl ketone. Toluene. Isobutyl acetate. Mesityl oxide. n-butyl acetate. Diacetone alcohol. -Methyl--hexanone. Ethylbenzene 0. m-xylene. p-xylene. Cyclohexanone nknown. o-xylene. Cellosolve acetate. Butyl Cellosolve. Isoamyl acetate 0,,, 溶媒工業溶媒 -0 Column : PAG, 0 m x 0. mm ID, 0. µm film Cat. No. : Oven : 0 (min.), /min. to 00 Inj.: 0 Det. : FID, 0 Carrier Gas : Helium, 0 Injection : 0.µL, split 00 : Sample : neat solvents mix 0. Acetone. Methanol. Pentane. Tetrahydrofuran. Ethanol. Chloroform. Toluene.,-Dioxane. Butyl acetate 0. Isobutanol. Ethylbenzene. o-xylene. Ethyl Cellosolve. Cyclohexanone. Diacetone alcohol

4 溶媒残留溶媒 Column : Equity-, 0 m x 0. mm ID,.0 µm Cat. No. : - Oven : 0 ( min), /min to 00 Inj.: Det. : FID, 0 Carrier gas: Helium, 0 Injection :.0 µl, split 0: Liner : Split, cup design Sample : ng on-column of a component solvent standard in DMSO. Methanol. Ethanol. Acetonitrile. Acetone. -Propanol. Ethyl ether.,-dichloroethylene. Freon. Methylene chloride 0. Methyl-t-butyl ether. -Butanone. Hexane. Ethyl acetate. Chloroform. Tetrahydrofuran.,,-Trichloroethane.,-Dichloroethane. Carbon tetrachloride. Benzene 0. Trichloroethylene.,-Dioxane. -Methyl--pentanone. Toluene. Dimethylformamide 0,, G00 溶媒医薬品残留溶媒 (SP 規定 ) Column : OVI-G, 0 m x 0. mm ID,.0 µm (SP code G) Cat. No. : Oven : 0 Inj.: 0 Det. : FID, 0 Carrier gas: Helium, cc/min. Injection :.0 µl, direct. Methylene chloride. Chloroform. Benzene. Trichloroethylene.,-Dioxane -00

5 溶媒医薬品残留溶媒 Column : SPB-, 0 m x 0. mm ID,.0 µm Cat. No. : Column : OVI-G, 0 m x 0. mm ID,.0 µm Cat. No. : Column : SPELCOWAX 0, 0 m x 0. mm ID,.0 µm Cat. No. : 0- Oven : 0 ( min.), /min. to 00 ( min.) Inj.: 0 Det. : FID, 00 Carrier gas: Helium, cc/min. Injection : 0. µl, split 00 : SPB- (SP code G),,. Methanol. Methyl formate. Ethanol. Acetonitrile. Acetone. -Propanol. Ethyl ether. Pentane. Ethyl formate 0. Methylene chloride. t-butanol. -Butanol. n-propanol. Methyl t-butyl ether(mtbe),. Methyl ethyl ketone(mek). Isopropyl ether. Hexane. Ethyl acetae. Chloroform 0. Isobutanol. Tetrahydrofuran(THF). -Butanol. Benzene.Carbon tetrachloride. Cyclohexane. Diethoxymethane. Trichloroethylene. Dioxane. Heptane 0. Isopentanol. Methyl isobutyl ketone(mibk). Pyridine. Toluene. Dimethylformamide. Isobutyl acetate. n-butyl acetate. Dimethylsulfoxide(DMSO). Methyl isoamyl ketone(miak). Dimethylacetamide(DMA) 0. p-xylene. m-xylene. o-xylene 0, 0,,, 0,, 0, -0 0, OVI-G (SP code G) 0,,, 0 0, SPELCOWAX 0 (SP code G) -0,,,,, 0,

6 溶媒医薬品残留溶媒, Class Oven : ( min), /min to 00 Inj.: Det. : FID, 0 Carrier gas: Helium, 0cm/sec, constant Injection : µl, split : Liner : mm ID single taper Sample : Class I: ppm in DMSO (Cat. No. ) Class I Concentration Retention Time Identification (µg/ml) Equity- SPELCOWAX 0 OVI-G.,-Dichloroethylene ,,-Trichloroethane ,-Dichloroethane Carbon tetrachloride Benzene Class Solvents on Equity- Column: 0 m x 0. mm ID,.0 µm w/ m intermediate polarity guard Cat. No.: -, G00 Class Solvents on SPELCOWAX 0 Column: 0 m x 0. mm ID,.0 µm Cat. No.: 0-, Class Solvents on OVI-G Column: 0 m x 0. mm ID x.0 µm w/ m intermediate polarity guard Cat. No.: G G00

7 溶媒医薬品残留溶媒, Class Oven : ( min), /min to 00 Inj.: Det. : FID, 0 Carrier gas: Helium, 0 cm/sec, constant Injection: µl, split : Liner : mm ID single taper Sample : Class II: (Cat. No. ) + n-methylpyrrolidone, 0-000ppm in DMSO Class II Concentration Retention Time Class II Concentration Retention Time Identification (µg/ml) Equity- SPELCOWAX 0 OVI-G Identification (µg/ml) Equity- SPELCOWAX 0 OVI-G. Methanol Ethoxyethanol Acetonitrile Methylcyclohexane Methylene chloride Pyridine Nitromethane 0.. NI. Toluene Hexane Dimethylformamide cis-,-dichloroethylene Methyl butyl ketone Chloroform Chlorobenzene Methoxyethanol Dimethylacetamide *.,-Dimethoxyethane m-xylene Cyclohexane p-xylene...0. Ethylene glycol o-xylene.... Formamide n-methylpyrrolidone Trichloroethylene Tetralin ,-Dioxane Sulfolane NI = not integrated *coelutes w/solvent Class Solvents on Equity- Column: 0 m x 0. mm ID,.0 µm w/ m intermediate polarity guard Cat. No.: - 0, 0, Class Solvents on SPELCOWAX 0 Column: 0 m x 0. mm ID,.0 µm Cat. No.: 0- G00 0,, G00 Class Solvents on OVI-G Column: 0 m x 0. mm ID,.0 µm w/ m intermediate polarity guard Cat. No.: 0, 0, G00

8 溶媒 - 医薬品残留溶媒, Class Oven : ( min), /min to 00 Inj.: Det. : FID, 0 Carrier gas: Helium, 0 cm/sec, constant Injection : µl, split : Liner : mm ID single taper Sample : Class III: custom mix, approx. 000 ppm in MeOH Class III Concentration Retention Time Class III Concentration Retention Time Identification (µg/ml) Equity- SPELCOWAX 0 OVI-G Identification (µg/ml) Equity- SPELCOWAX 0 OVI-G. Ethanol Iso-Butanol Acetone n-butanol Propanol Isopropyl acetate Pentane Heptane Ethyl ether Propyl acetate Ethyl formate Isoamyl alcohol Methyl acetate Methyl--pentanone Propanol n-amyl alcohol Methyl-t-butyl ether Isobutyl acetate Acetic acid 000 NI.0.. Butyl acetate Butanone Dimethyl sulfoxide sec-butanol Anisole Ethyl acetate Cumene Tetrahydrofuran NI = not integrated Class Solvents on Equity- Column: 0 m x 0. mm ID,.0 µm w/ m intermediate polarity guard Cat. No.: -,,, Class Solvents on SPELCOWAX 0 Column: 0 m x 0. mm ID,.0 µm Cat. No.: 0- G00,, G00 Class Solvents on OVI-G Column: 0 m x 0. mm ID,.0 µm w/ m intermediate polarity guard Cat. No.: 0,, G00

9 溶媒メチルイソブチルケトン (MIBK) 中の不純物 Column : SPELCOWAX 0, 0 m x 0. mm ID, 0. µm film Cat. No. : 00- Oven : 0 Carrier gas: Helium, cm/sec Det. : FID Inj.: 0. µl MIBK, split 00 : Coumn : SPELCO WAX0, m x 0.mm ID,.0 µm film Cat.: 00- Oven : 0 (min), /min to 0 (min) Contamnants, 0.0%each Carrier gas : helium,ml/min Det. : FID Inj. : 0.µlL MIBK,direct 内径 0.mm カラムによる分離 Contaminants, 0.0% each. Acetone. -Propanol. -Pentanone. -Pentanone. α-mesityl oxide. β-mesityl oxide. Methyl isobutyl carbinol 内径 0.mm カラムによる迅速分離 Methyl Isobutyl Ketone Methyl Isobutyl Ketone,, 溶媒メチルエチルケトン (MEK) 中の不純物 -00 Column : SPELCOWAX 0, 0 m x 0. mm ID, 0. µm film Cat. No. : 0 Oven : 0 ( min.), /min. to 00 Carrier : Helium, cm/sec Det. : FID, 0 Inj.: 0. µl MEK, split 00 : Spiked 0.0% each compound in MEK (sec-butyl ether is contaminant in MEK, not spiked) Contaminants, 0.0% each. Diisopropyl ether. Dipropyl ether. sec-butyl ether*. Acetone. -Octene. Ethyl acetate. Methanol. Isopropanol. Ethanol 0. tert-butanol. sec-butanol. n-propanol 0 0-0

10 溶媒メチルエチルケトン中の不純物 Column : Equity-0, 0 m x 0. mm ID,. µm Cat. No. : - Oven : (0 min), /min to 00 Inj.: 0 Det. : FID, 0 Carrier gas: Helium, Injection : µl, 0: split Liner : mm ID cup style Sample : Methyl ethyl ketone of various purity levels ACS Reagent Grade 0. Methanol. Ethanol. Acetone. Isopropanol. t-butanol. n-propanol. n-butanol. Ethyl acetate. Diethoxymethane 0. sec-butanol. Methyl isobutyl ketone. Isopropyl acetate. Isobutanol. Toluene. -Methyl--pentanone. -Octene 0 0 G00000 Commercial Grade G0000 Laboratory Standard G0000

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