Oxidation Characteristics of Carbon Materials Hideaki Sane and Yasuo Uchiyama Corresponding Author, Nagasaki Universi
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1 Oxidation Characteristics of Carbon Materials Hideaki Sane and Yasuo Uchiyama Corresponding Author, Nagasaki University: 1-14 Bunkyo-machi, Nagasaki , Japan
2 Table 1 Standard free energy of C-O system gaseous species.
3 (a) y axis: normal (b) y axis : logarithmic Fig. 1 Equilibrium amount of species of C-O system with temperature calculated by ChemSage8). Calculating condition; Pressure: 1atm, Volume: variable displacement, initial species; C: 1mol, O2(g): 0.1mol. Fig. 2 Ellingham diagram of C, B4C and SiC.
4
5 a) Apparatus for oxidation Fig. 3 Schematic diagram of (a) apparatus for oxidation furnace and (b) sample holder. Fig. 4 Morphological change of C/B4C/SiC composite after oxidation at 1200 Ž for 1, 2 and 5h in dry air.
6 a) TGA apparatus b) TG-DTA apparatus Fig. 5 Schematic diagram of (a) TGA apparatus and (b) TG DTA apparatus.
7 Fig. 6 TG-DTA curve of 2150 Ž heat-treated petroleum coke. Fig. 7 DTA curves for carbonized furfural-resin heat-treated at different temperatures20).
8 (c): Reaction rate (V3) vs oxidation burn-off (a): mass% vs oxidation time (b): Reaction rate (V2) vs oxidation burn-off Fig. 8 TG curve and oxidation rate V2 and V3 of carbonized saran char with and without 1.0mass%-boron loaded at 800t in dry air24).
9 1) H. Imai, TANSO 1981 [No.107] [in Japanese]. 4) M. W. Chase, J. L. Curnutt, H. H. Prohet, A. N. Syverud and L. C. Walker, J. Phys. Chem. Ref Data 3 [No.2] (1974) ) D. D. Wagman, W. H. Evans, V. B. Parker, R. H. Schumm, I. Halow, S. M. Bailey, K. L. Churney and R. L. Nuttall, J. Phys. Chem. Ref. Data 11 [No.2] Suppl. 2 (1982). 7) M. Hillert, B. Jansson, B. Sundman and J. Agren, Met. Trans. A 16A [No.2] (1985) ) G. Eriksson and K. Hack, Met. Trans. B 21B [No.12] (1990) ) H. Sano, H. M. Cheng, Y. Uchiyama and K. Kobayashi, J. Ceram. Soc. Japan 102 [No.10](1994) [injapanese]. 10) Y. Watanabe, T. Matsuzaki, H. Itagaki, K. Yudate, T. Takiguchi, Y. Shouda and S. Hasegawa, Journal of the Japan Society for Aeronautical and Space Sciences 42 [No.482] (1994) [in Japanese]. 12) J. Okada and T. Ikegawa, J. Appl. Phys. 24 (1953) ) H. Kawakami, TANSO 1986 [No.124] [in Japanese]. 15) H. Hatori, TANSO 2000 [No.195] [in Japanese]. 16) T. Ozawa, J. Thermal Anal. Calori. 59 (2000) ) H. E. Kissinger, Journal of the National Bureau of Standards 57 [No.4] (1956) ) T. Honda, T. Saito and Y. Horiguchi, TANSO 1973 [No.72] [in Japanese]. 21) G. L. Montet and G. E. Myers, Carbon 6 [No.5] (1968) ) H. Imai. et al.. JAERI-M 9153 (1980). 24) Y. Uchiyama, L. R. Radovic and C. G. Pntano, International Symposium of Carbon, Science and Technology for New Carbons, Tokyo, , ) M. R. Everett, D. V. Kinsey and E. Romberg, Chemistry and Physics of Carbon, (Philip L. Walker, Jr., ed. ) Vol.3 (1968) pp , Marcel Dekker, New York. 26) E. E. G. Hughes and J. M. Thomas, Nature 193 (1962) ) J. M. Thomas and E. E. Hughes, Carbon 1 [No.2] (1964) ) R. T. K. Baker and P. S. Harris, J. Phys. E 5 (1972) ) R. T. K. Baker and P. S. Harris, Carbon 11 [No.1] (1973) ) A. A. Gewirth and A. J. Bard, J. Phys. Chem. 92 [No.20] (1988) ) A. Miyazaki, M. Okamoto and I. Tomizuka, Journal of the Materials Science Society of Japan 31 [No.2] (1994) [in Japanese]. 32) H. Sano, E. Hayakawa, J. Eshima, Y. Uchiyama and K. Kobayashi, TANSO 1996 [No.175] [in Japanese]. 33) N. R. Laine, F. J. Vastola and P. L. Walker, Jr., J. Phys. Chem. 58 [No.20] (1963) ) J. N. Ong, Jr., Carbon 2 [No.3] (1964) ) A. C. Collins, H. G. Masterson and P. P. Jennings, J. Nucl. Mater. 15 [No.2] (1965) ) J. L. Wood, R. C. Bradt and P. L. Walker, Jr., Carbon 18 [No.3] (1980)
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9) H. SCHMCLZRIED: Z. Elektrochem. 66 (l%1) p ) W. D. KINGERY et al.: J. Am. Chem. Soc., 42 (1959), p ) F. HUND: Z. Phys. Chem., 199 (195
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