JAAS0012006
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6.7 --------------------------------------------------------------------------------------------------------- 9 6.7.1 --------------------------------------------------------------------------------------------------------- 9 6.7.2 --------------------------------------------------------------------------------------------------- 9 6.7.3 --------------------------------------------------------------------------------------------------------- 10 6.7.4 --------------------------------------------------------------------------------------------------------- 10 6.7.5 ------------------------------------------------------------------------------------------------------ 10 6.8 --------------------------------------------------------------------------------------------------------- 10 6.8.1 --------------------------------------------------------------------------------------------------------- 10 6.8.2 --------------------------------------------------------------------------------------------------- 10 6.8.3 --------------------------------------------------------------------------------------------------------- 10 6.8.4 --------------------------------------------------------------------------------------------------------- 10 6.8.5 ------------------------------------------------------------------------------------------------------ 10 ------------------------------------------------------------------------------------------------------------------- 11 1 ----------------------------------------------------------------------------------- 11 2 ----------------------------------------------------------------------------------------------------- 11 3 -------------------------------------------------------------- 12 3.1 ------------------------------------------------------------------------------------------ 12 3.2 ------------------------------------------------------------------------------------------------------------ 12 3.3 --------------------------------------------------------------------------------------------------- 12 4 ----------------------------------------------------------------------- 12 5 ----------------------------- 12 5.1 ------------------------------------------------------------------------------------ 12 5.2 --------------------------------------------------------------------------------- 12 5.2.1 --------------------------------------------------------------------------------------------------------- 12 5.2.2 --------------------------------------------------------------------------------------------------- 12 5.2.3 --------------------------------------------------------------------------------------------------------- 13 5.2.4 --------------------------------------------------------------------------------------------------------- 13
25 FW : 46.07 JIS K 0114 JIS K 0512 JIS K 0557 JIS K 1107 JIS K 8034 JIS K 8085 JIS K 8101 (99.5) JIS K 8129 JIS K 8155 JIS K 8247 JIS K 8295 JIS K 8355 JIS K 8371 JIS K 8464 JIS K 8528 JIS K 8541 JIS K 8550 JIS K 8721 p- JIS K 8810 1- JIS K 8811 2--1- JIS K 8812 2- JIS K 8838 1- JIS K 8839 2- JIS K 8891 JIS K 8949 JIS K 8951 JIS R 3503 JIS Z 8301
2 99 1 95 95 99 95 5 6 1 2 1 99 1 95 95 1 99.5 95.0 95.0 mg/100 ml 1.0 0.5 1.0 ( mg/l () 30 70 ) 1- mg/l () () 60 n- 2- mg/l 40 30 40 1- mg/l () () () n- mg/l 5 3 5 mg/l 1 n- mg/l mg/l 20 10 20 8 1,4-
3 99 95 99.5 95.0 mg/100 ml 1.0 1.0 mg/l 20 () 1-- mg/l 2- mg/l 70 70 1-- mg/l 50 50 mg/l 7 7 mg/l - mg/l 1 mg/l 20 20, a) b) c) d) e)
30 ml a) 100 ml b) 50 ml c) 4 d) JIS K 0557 A3 A4 2 30 ml 25 % 99 1 95 1 95 250300 ml a) 90100 1/10 b) 0500.1 c) 1020 mm 250300 ml 15 100 ml a) 100 ml b) c) d) 100 ml 105110 mg/100 ml
5 JIS K 0114 1 µl a) b) A B 2 3 A B mm 0.53 0.53 m 25 30 µm 20 1 2- n- 1- n- 1- n- 2-2- 2--1-2--1- A Pora PLOT Q HT 0.53 mm 25 m 20 µm B J&W DB-WAX 0.53 mm 30 m 1 µm c) d) 10 µl
6 a) JIS K 8891 b) 2- JIS K 8839 c) 99% d) JIS K 8464 e) n- 98% f) 1-n- JIS K 8838 g) 1-n- JIS K 8810 h) 2-2- JIS K 8812 i) 2--1- JIS K 8811 j) 2--1-98% k) JIS K 8034 l) JIS K 8101 m) JIS K 1107 n) 99.99 % o) JIS K 0512 p) a) 10 mg/l 4 A B 2- n- 1-n- 1-n- 2-2- 2--1-2--1-4 1 99.5 100 ml 10,000 mg/l 10 ml 99.5 100 ml 10 ml 99.5 100 ml 10 ml 99.5 100 ml 10 mg/l A 10 mg/l
7 b) 5 A B ml/min 15 15 3050 3050 min 0 5 /min 5 5 200 200 200 200 200 200 µl 1 1 c) d) (10 mg/l) 1 µl e) JIS K 0114 11.4 JIS K 0114 6.4.4 e) 0.1 mg/l 1 10 ml a) 18 mm 180 mm b) c) 2 ml5 ml10 ml25 ml50 ml d) 100 ml e) 100 ml200 ml1 L f) 25 ± 0.5 g) 20 W h) i) JIS R 3503 4 j)
8 a) A 1.5 g 95 ml 10 10 mm 511 nm 0.310 ± 0.005 B p- 1.20 g 100 ml 2.72 g 100 ml 1:3 p- 0.025 g 85 ml 10 mm 10 mm 400 nm 0.600 ± 0.010 ph 5.1 B 10:8 1 A B 1 b) 0.02 mol/l (N/10) 3.160 g 1 L 1 JIS R 3503 4 0.05 mol/l (N/10) 0.02 mol/l (N/10)0.1 ± 0.001N 0.02 mol/l (N/10) 1 0.02 mol/l (N/10) 1 c) 0.05 mol/l (N/10) 10 g 110 2 6.76.8 g 0.1 mg 1 L d) 0.02 mol/l (N/10) 0.05 mol/l (N/10) 25 ml 10 ml 6070 5 0.02 mol/l (N/10)30 0.05 mol/l (N/10) 1 ml 0.00316 g e) JIS K 8247 f) JIS K 8528 g) JIS K 8129 h) p- JIS K 8721 i) JIS K 8355 j) JIS K 8371 k) JIS K 8951 15 ml 2 25 ± 0.5 10 ml 2 0.0002 mol/l (N/1000) 5 ml 1 m 0.0002 mol/l (N/1000) a)
9 b) c) d) e) 0.002 mol/l (N/1000) 0.02 mol/l (N/10) 0.0002 mol/l (N/1000) 5 f) 0.0002 mol/l (N/1000) 5 ml a) b) 50 ml c) 5 ml d) 1 ml10 ml e) f) a) 5 g 10 ml 30 ml 3 b) JIS K 8949 c) JIS K 8295 d) JIS K 8085 90 % 5 ml 3 2 1 []0.4 mg/l[]0.7 mg/l 1) 2) 10 ml a) b) 100 ml c) 0.5 ml1 ml10 ml
10 d) a) 1.7 g 100 ml b) JIS K 8541 65% 1.40 g/ml c) JIS K 8550 10 ml 0.5 ml 1 ml 10 []0.3 mg/l 1) 2) 5 ml a) b) 100 ml c) 5 ml d) 1 ml10 ml e) a) 12 g 100 ml b) JIS K 8155 90 % 5 ml 5 ml 2 5 []2 mg/l 1) 2)
11 13 NEDO NEDO 13 4 18 4 NEDO 15 11 18 16 1,4-1,4-18 1 18 NEDO 13 4 NEDO 10 1 13 4 NEDO, 18 4 NEDO NEDO ISO ISO1388:1981
12 JIS Z 8301:2005 IUPAC SI 1,4-16 1,4- NEDO 1,4-1 1,4-0.05 mg/l 1,4-1,4-1,4-15 101 15 5 30 16 4 1 0.05 mg/l JIS K 0123 0.15.0 µl a) SIM b) 70 V c) 0.250.53 mm 3060 m 0.51.0 µm 1.05.0 µm d) 1 ml/min e) 406010 540 / 150200 110 f) 150200 g) 150200 h) 150200 i) 0.12 j) 110 µl
13 a) JIS K 8101 b) JIS K 0123 c) 99.99 a) 1,4-1 g 99.5 100 ml 10,000 mg/l 1 ml 99.5 100 ml 1 ml 99.5 100 ml 5 ml 99.5 100 ml 0.05 mg/l b) (0.05 mg/l) 88 58 c) 1,4-0.05 mg/l