Ⅱ6.3界面活性剤
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- あやか さかいざわ
- 5 years ago
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1 (1) (2) a) JIS K 0557 A3 b) JIS K 8891 c) (5g/L) d) (10g/L)JIS K g 100mL e) (7+993)JIS K 8951 f) JIS K 8322 g) 0.1g 100mL 30mL 1L 500mL6.8mL 50g 1L h) 1L 500mL6.8mL 50g 1L i) (0.001g NaO3SO(CH2)11CH3 /ml) 100% 1.00g 1,000mL j) (10g NaO3SO(CH2)11CH3 /ml) (0.001g NaO3SO(CH2)11CH3/mL) 10mL 1,000mL (3) (1) a) b) c) d) e) f) g) h) 15cm 5cm i) (1) (1+9) 100mL 10mL 25mL
2 (4) (4) a) 20g 100mL b) 30mL 300mL c) 10mL 300mL d) 300mL mL e) 60mL f) 200mL g) 30mL 30 h) 100mL i) a)h) (4).2 a) 20g (2) 100mL 40mL 10 b) 3,000rpm 5 200mL c) 40mL 1 d) 30mL 1 (3) 200mL e) 70mL GF/F (4) f) 50vol% 5mL 2 g) 100mL h) a)g) (2) (3) (4)70mL (5) a) 650nm b) 244
3 g/mL114mL 100mL (5)c) c) A 100mL (5g/L)3 (10g/L) (7+993) 10mL 25mL 1 23 (5) 10mL 2 50mL 30 50mL 5mL 2 50mL 650nm (4).1 i) (4).2 h) d) (g) 4.1 (%) (mg/kg) 100 ( mg / kg) = ( g) v 1 W(g) W (g) v (ml) (5) 245
4 6.3.1 (6) a) 20g 100mL mL 30mL 30 3,000rpm5 30mL 100mL b) mL 40mL 200mL 30mL 70mL GF/F 100mL 246
5 6.3.1 c) A 100mL (5g/L) (10g/L) (7+993) 25mL 10mL 10mL B 50mL 30 50mL 650nm 247
6 LAS (1) GCB / 65:35 1mL (HPLC) (2) a) JIS K 0557 A3 b) JIS K 8891 c) d) e) [0.1mol/L (50:50)] 12.3g 50:50 1L f) g)c12las (1mg/mL) 100mg / 65:35 (1) 100mL h)c12las (10g/mL)C12LAS (1mg/mL)10mL /65: mL i) LAS(C10C14 ) (1mg/mL) (2) 1100mg / 65:35 100mL j)las(c10c14 ) LASC10C14 (1mg/mL) 10mL / 65:35 100mL (1)HPLC/ LAS (2) 1 LAS HPLC (3) a) b) c) d) e) f) g) h) 15cm 5cm i) GCB j) 4.6mm25cm (ODS) 510m 248
7 nm 300nm k) 10500L (4) (4).1 a)i) (4).2a)h) (5) a) LCLC/MS LCLC/MS LC/ HPLC ODS2503.0mm5m 0.5mL/min 0.1M-NaClO4 / 65: L 225nm 300nm LC/MS HPLC C mm5m 0.5mL/min A 10mM B A / B35: L MS ESI negative N L/min 40psi 100V 4,000V b) LASC10C14 (3) 10L LC LC/MS C10C11C12C13 C14 LC C10C LC/MS C10C LAS (0.1mg/mL)0.25mL 1L 249
8 6.3.1 LAS (3) C10C14LAS C12-LAS LASC10C14 0.1mg/mL HPLC/ C12LAS 10g/mL C10C11C13C14LAS C10C14 LAS g/ml LASC10C14 C10 C11 C12 C13 C14 C12-LAS10g/mL LAS (0.1mg/mL) LAS mmol/l LAS g/ml c) 5mL 15mL (4) GCB (5) GCB 2 /70:307mL (6) 25M / 90:107mL (7) 10M / 90:10 7mL LAS /65:351mL LAS d) LAS 4.1 (%) 1g LAS (mg/kg) (mg / kg) = (ml) (ng) ( L) (ml) W(g) W (g) (4) 10mL 10mL 10L (5)GCB LAS 250
9 6.3.1 (6) (7) C11 C12 C10 C13 C LC/ C11 C12 C10 C13 C LC/MS 251
10 6.3.1 (6) 30mL/min (25vol%) 3mL 2 5mL 10mL 2mL HPLC 252
11 (1) 18 GC/MS (2) a) 2 b) c) d) e) f) g) h) i) (100g/mL)[ (CH3(CH2)11O(CH2CH2O)7H)] g 100mL j) (10g/mL) pd g 100mL 10mL 100mL k) SepPak Plus Accell CM Cartridges(360mg) 1 l) SepPak Plus Accell QMA Cartridges(360mg) 1 m)c18 SepPak Plus 18 Cartridges(360mg) 1 n) GF/FWhatman 1 (3) a) b) c) d) e) f) (5mL) g) 253
12 (4) a) (4).1 a)i) (4).2 a)h) b) 20mL (1) 18 3 c) 50vol% d)18 4mL (1) (5) a) GC/MS GC/MS VOCOL 0.32mm 60m 3.0m 50(2min)(10 min)200 2mL/min ( ) 150 (90sec) 200 (E1) 210 / b) p d10 /116 (100g/mL) g/mL (5) c) c) (4)d) (2) mL (3) mL 5mL 1mL 10g/mL 20L 1L GC/MS (4)a)d) d) 4.1 (%) 1g (mg/kg) 254
13 6.3.2 (ml) 1 (mg / kg) = (ng) ( L) W(g) W (g) (2) (3) 255
14 (6) mL 40mL 200mL 30mL 70mL GF/F C18 10mL C18 4mL (1:1) 0.5mL mL 34mL 5mL 1mL 20L 1L GC GC/MS 256
15 (1) 2 80:20 1mL HPLC/FLD (2) a) JIS K 0557 A3 b) JIS K 8891 c) JIS K 8161 d) e) (1) (1mg/mL) g 100mL f) (10g/mL) 1mL 100mL (1)NP1EONP2EO 1 NP3EONP6EO 1NP7EO (3) a) b) c) d) 50mL e) f) 3,000rpm g) h) i) 15cm 5cm j) 12mL 1g 5mL 10mL k) 100mL 200mL l) 200mL 500mL m) 1020mL n) o) 110L 257
16 p) mm 25cm (ODS) 510m 225nm 300nm (4) a) (4).1 a)i) (4).2 a)h) b) 50mL 100mL c) 100mL 50mL d) / 50:50 5mL 2mL 10 e) / 80:206mL f) 1mL g) a)f) (5) a) HPLC HPLC L NP1EONP10EO ShodexAsahipakGF310HQ7.6mm300mm (B):(A) 40 x 225nm, m 300nm 6.32 b) 6.32 Time solvent B flow rate (min) (%) (ml/min) (10g/mL) 00.11mL 10mL 0.11g/mL L HPLC 258
17 6.3.2 c) 10L HPLC d) (ng) (mg/kg) (ml) 100 (mg / kg) = (ng) ( L) 50 1 W(g) W (g) /min
18 6.3.2 (LC/MS) L L NP1EONP2EO NP3EO H + Na + K + Na LC/MS LC/MS L Asahipak GF310HQ B/ 0.1 A 40 10L electrospray(positive) mL/min 50psi 3,500V 6.33 Time solvent B flow rate (min) (%) (mlmin 1 ) LC/MS m/z [M+Na] + NP1EO NP2EO NP3EO NP4EO NP5EO NP6EO NP7EO NP8EO NP9EO NP10EO
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3--2-3-Iodo-2-propynyl butylcarbamate (IPBC) Carbamic acid, butyl-, 3-iodo-2-propynyl ester Iodocarb CAS 55406-53-6 C 8 H 12 NO 2 I C (g/cm 3 ) (mmhg) log P ow 281.09 (280.9910) 64 68 1.51 1.57 (20 C)
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13 56 2011 Examination of Determination of Residual Pesticides in Agricultural Products Yuki OHGAKI, Katsuhiro HAYASHI, Hiroyuki KAWAI, and Kyoko SHIMURA GC/MS 92 LC/MS/MS 60 150 n- 5 GC/MS 92 79 70% LC/MS/MS
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18 HNS HNS HNS HNS HNS HNS HNS 19 3 18 HNS 18 6 14 OPRCHNS 18 68 19 4 1 20 4 1 OPRCHNS 18 6 14 15 19 6 14 17 HNS 19 2 1 1 3 4 5 5 5 7 8 10 13 13 15 15 10 16 HNS 17 HNS 18 HNS 19 HNS 20 21 22 23 39 61 61
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10 12 A 12 C 12 13 13 13 13 16 16 18 18 18 23 23 23 23 23 A 24 25 25 26 28 28 30 32 38 38 41 42 43 10 43 11 45 48 48 120g 51 52 12 3 12 3 350g 120g 1 7 10 260g 90g 90g 30g 9 11 2 gg1 g 1 120g 10 1 12 6
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N,N- N,N-Dimethylacetamide Acethyldimethylamine CAS 127-19-5 C 4 H 9 NO 87.12 ~ 87.14 87.68413 163-165 C 1) - 18.59 C 2) 1 mg/l 25 C 3) 3.3 hpa 2 C 4) log P ow -.77 2).9429 2/4 C 1) 3.1 4) 1.31E - 8 atm-m
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2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
平成26年度 化学物質分析法開発報告書
2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
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