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1 Agilent SPE SPE

...3...4...5...6...7...8 OPT...10 SCX...12 SAX...14 DVB...16 PS-DVB...17...18 C18EC...18 C18 ODS...19 C8...20 C2...21...21...22 (CN)...23...23...24 Si-SCX.

2 OPT...10 SCX...12 SAX...14 DVB...16 PS-DVB C18EC...18 C18 ODS...19 C C (CN) Si-SCX...25 Si-SAX Florisil PR...27 A...28 B...29 N C8/Si-SCX...31 SPE...32 Evidex QuEChERS

3 SPE (SPE) HPLC SPE SPE Agilent SPE HPLC ISO-9001 SPE SPE 3

4 Agilent SPE < 2000 ( ) MeOH ( ) ACN () Et OAc ( ) THF ( ) CH 2 Cl 2 () Et 2 O () C5 (n-) C6 (n-) ic8 () CEX AEX n-bpc LSC RPC n-bpc LSC RPC SCX SAX OPT DVB PS-DVB OPT DVB PS-DVB Si-SCX C8/Si-SCX ( ) Si-SAX (WAX) C18 C18EC C8 C2 C18 C18EC C8 C2 Florisil PR A B N Florisil PR A B N EVIDEX 4

5 Agilent Bond-Elut Plexa Oasis HLB Strata-X Bond-Elut ENV Strata SDB-L Supelclean ENVI-Chrom P Bond-Elut Plexa PCX Oasis MCX Strata X-C Oasis MAX Bond-Elut C18 Discovery DSC-C18 Sep-Pak tc18 Strata C18-E Supelclean ENVI-18 Supelclean LC-18 Bond-Elut C18OH Sep-Pak C18 Strata C18-U InsertSep C18 Bond-Elut C8 Sep-Pak C8 Strata C8 InsertSep C8 Bond-Elut C2 Sep-Pak tc2 InsertSep C2 Discovery DSC-Ph Strata Phenyl (PH) Supelclean LC-Ph InsertSep PH Bond-Elut Certify-I Strata Screen-C () Bond-Elut SI Discovery DSC-Si Sep-Pak Silica Strata Si-1 Bond-Elut SI Discovery DSC-Si Sep-Pak Silica Strata Si-1 InsertSep SI Bond-Elut FL Sep-Pak Florisil Strata FL-PR Supelclean LC Florisil Supelclean ENVI Florisil InsertSep FL Bond-Elut NH2 Discovery DSC-NH2 Sep-Pak Amino Propyl Strata NH2 Supelclean LC-NH2 InsertSep NH2 Bond-Elut 2OH Discovery DSC-Diol Supelclean LC-Diol Bond-Elut CN-U Discovery DSC-CN Sep-Pak Cyano Propyl Strata CN Supelclean LC-CN InsertSep CN Bond-Elut AL-A,B,N Sep-Pak Alumina A, B, N Supelclean LC-Alumina A,B,N InsertSep AL A, B, N Bond-Elut SAX Discovery DSC-SAX LC-SAX Sep-Pak AccellPlus QMA Strata SAX InsertSep SAX Bond-Elut SCX Discovery DSC-SCX Sep-Pak AccellPlus SCX Strata SCX Supelclean LC-SCX InsertSep SCX Supelclean ENVI-Carb InsertSep GC Agilent OPT PS-DVB SCX SAX C18EC C18 C8 C2 Evidex Florisil PR A B N Si-SAX Si-SCX 5

6 Agilent HPLC LC/MS GC ( ) ( ) ( ) / GC 6

7 Agilent SPE Agilent SPE Agilent SPE ph 0 14 ph 7

8 A/N/B Log P < 1.5 / pka < 3 SAX Log P > 1.3 pka > 3 pka < 10 OPT Log P < 1.5 / pka > 10 SCX 0.1% 2% 1 ml/min (ph 7) mm (ph 7) 5% 5 10% 2% % 0.1% 3% NH 4 OH 8

9 1 () SCX OPT SAX SCX (A) (N) (B) * 1 ml 1 ml 1 ml 1 ml 1 ml 1 ml 3 ml 2 ml 2 ml 2 ml 2 ml 2 ml 6 ml 3 ml 3 ml 5 ml 4 ml 4 ml µl 200 µl µl 200 µl µl * 9

10 Agilent OPT SPE Agilent Optimized Polymer Technology (OPT) OPT ( ) ph 0 14 OPT GC LC OPT ph pka 0.1% OPT OPT R N R O R 30 mg 1 ml mg 3 ml mg 6 ml mg

11 OPT (%) OPT ( RSD) OPT ( EN) 11

12 Agilent SCX (SCX) SCX (log P) ph 0 14 SCX R 1 R 2 SO 3-30 mg 1 ml mg 3 ml mg 6 ml SCX 25 12

13 3% (%) () 2 () (3% ) ph SAX ( EN) 8 13

14 Agilent SAX Agilent (SAX) 3 SAX (log P) SAX ph 0 14 SAX N R 3 R 1 R 2 30 mg 1 ml mg 3 ml mg 6 ml SAX 26 14

15 2 SAX SAX (%) % (2% ) SAX / / / / / /- 1.3 (%) ph SAX ( EN) 8 15

16 Agilent DVB DVB SPE C18 PS-DVB 100% DVB SPE ph 0 14 SPE DVB 30 mg 1 ml mg 3 ml mg 6 ml

17 Agilent PS-DVB PS-DVB (PS-DVB) (600 m2/g) C18 C8 ( µm) PS-DVB [-CH - CH 2 - CH - CH 2 - CH - CH 2 -] n 500 mg 6 ml mg 6 ml [-CH - CH 2 C - CH 2 - CH - CH 2 -] n - 17

18 Agilent SPE SPE 45 µm 60 Å SPE 3 Agilent () SPE () C18EC Si O Si (CH 2 ) 17 CH 3 O Si O Si(CH 3 ) 3 C18 C18EC (ODS) (EC) C18 C18EC 25% C18EC 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

C18 C18 ODS ( ) ( ) SPE C18 24% Si O Si (CH 2 ) 17 CH 3 O Si OH (C18) C18 100 mg 1 ml 100 5982-1111 200 mg 3

19 C18 C18 ODS ( ) ( ) SPE C18 24% Si O Si (CH 2 ) 17 CH 3 O Si OH (C18) C mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

Si O Si (CH 2 ) 7 CH 3 O Si OH C8 C8 ( ) () SPE SPE (C8) C8 100 mg 1 ml 100 5982-1011

20 Si O Si (CH 2 ) 7 CH 3 O Si OH C8 C8 ( ) () SPE SPE (C8) C8 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml g

21 C2 C2 SPE () 3 C8 C18 O Si Si O OH Si CH 2 CH 3 C2 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml SPE () (pi-pi) O Si Si O OH Si 100 mg 1 ml mg 3 ml mg 3 ml g

Agilent () SPE () O Si Si OH OH SPE () 1 () ph 100 mg 1 ml 100 5982-2211 200 mg 3 ml 50

22 Agilent () SPE () O Si Si OH OH SPE () 1 () ph 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

23 (CN) (CN) SPE () Si O Si O OH Si (CH 2 ) 3 CN (CN) 100 mg 1 ml mg 6 ml mg 6 ml SPE () Si O Si O OH Si (CH 2 ) 3 OCH 2 CH CH 2 OH OH 500 mg 3 ml

24 (NH 2 ) Si O Si (CH 2 ) 3 NH 2 O Si OH (NH 2 ) (NH 2 ) SPE () 2 -OH -NH -SH ph 7.8 (NH 2 ) 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

25 Agilent ph (Si-SCX) Si-SCX SPE () 0.3 meq/g Si O Si O Si OH (CH 2 ) 2 SO 2 - H + (Si-SCX) SCX 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml

26 Si O Si (CH N + (CH 3 ) 3 CI 2 ) 3 O Si OH SAX (Si-SAX) Si-SAX SPE () pka ph 0.6 meq/g (Si-SAX) 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

Agilent SPE SPE / Florisil PR Florisil PR Florisil PR 200 mg 3 ml 50 5982-4332 500 mg

27 Agilent SPE SPE / Florisil PR Florisil PR Florisil PR 200 mg 3 ml mg 3 ml mg 6 ml mg 6 ml g

A () A 50 200 µm A 500 mg 3 ml 50 5982-4035

28 A () A µm A 500 mg 3 ml mg 6 ml g

B () B 50 200 µm B 500 mg 3 ml 50 5982-4135

29 B () B µm B 500 mg 3 ml mg 6 ml g N () N µm (N O P S ) N 500 mg 3 ml mg 6 ml g

100 mg 1 ml 100 5982-4411 250 mg 3 ml 50

30 100 mg 1 ml mg 3 ml mg 6 ml g

31 C8/Si-SCX SPE SPE (C8) (Si- SCX) C8 Si-SCX UV LC/MS 3 C8/Si-SCX 100 mg 1 ml mg 3 ml mg 3 ml mg 6 ml mg 6 ml

Agilent SPE Evidex SPE Evidex SPE SAMHSA ( ) / PCP () () / THC-COOH ( ) (RSD 5% ) Evidex SPE 200 mg 3 ml 50 5982-2332

32 Agilent SPE Evidex SPE Evidex SPE SAMHSA ( ) / PCP () () / THC-COOH ( ) (RSD 5% ) Evidex SPE 200 mg 3 ml mg 6 ml GC EDDP DB-5ms EVDX (5% )- GC (mm) (m) (µm) ( ) DB-5ms EVDX /

SPE Agilent SPE 35 QuEChERS C18EC 25 g 5982-1382 C18 25 g 5982-1182 C8 25 g 5982-1082 25 g 5982-4482 25 g 5982-1582 25 g 5982-2282

33 SPE Agilent SPE 35 QuEChERS C18EC 25 g C18 25 g C8 25 g g g g (NH 2 ) 25 g Si-SAX 25 g A () 25 g B () 25 g N () 25 g Florisil PR 25 g

SPE Agilent SPE 1 ml 50 5982-9301 SPE 3 ml 50 5982-9302 SPE

5982-9305 SPE 1 ml 100 5982-9306 SPE 3 ml 100 5982-9307 SPE

34 SPE Agilent SPE 1 ml SPE 3 ml SPE 6 ml SPE 35 ml SPE 70 ml SPE 1 ml SPE 3 ml SPE 6 ml SPE 35 ml SPE 75 ml

Effective, Rugged and Safe" www.quechers.

35 SPE QuEChERS QuEChERS Steven J. Lehotay CVUA Michelangelo Anastassiades QuEChERS "Quick, Easy, Cheap, Effective, Rugged and Safe" QuEChERS 100 g PSA ( 1 2 ) 25 g g C18 25 g Si-SAX 25 g

12 16 x 100 mm 20 16 x 100 mm 5982-9110 5982-9120 20

36 12 16 x 100 mm x 100 mm Luer

/ 5982-9106 5982-9107 5982-9108 12 12 5982-9111 12

100 mm 12 5982-9115 16 x 75 mm 12 5982-9116 16 x 100

5982-9123 13 x 75 mm 20 5982-9124 13 x 100 mm 20

37 / x 75 mm x 100 mm x 75 mm x 100 mm x 75 mm x 100 mm x 75 mm x 100 mm

12 20 20 5982-9100 20 5982-9101 20 5982-9102 20 5982-9103 25 5982-9104 5982-9105 12 5982-9109 96 96 96

96 96 50 5042-1389 96 0.5 ml 120 5042-1385 96 0.5 ml 10 5042-1386 96 5065-4402 0.

5 ml 29 mm 5185-5780 2 mm 96 25 5185-5782 96 5185-5798 96 5185-5799 96 5185-5778 96 Luer 25

39 ml ml ml 96 O /96 Agilent 1 ml 12 mm Agilent 0.5 ml 29 mm mm Luer Luer () / O

40 Agilent SPE GC/LC Agilent J&W GC Über One GC Agilent ZORBAX Eclipse Plus LC 40 (LOD) (LOQ) Agilent Technologies, Inc Printed in Japan August 7, JAJP

Bond Elut 25%OFF Bond Elut 25 %OFF Bond Elut, Mega Bond Elut Bond Elut AL-A Bio Bond Elut Bond Elut AccuCAT Bond Elut Carbon Bond Elut Atrazine Bond E

2016 Bond Elut : 2 GC/MSD IDP-3 : 9 Captiva : 3-4 : 10-11 ZORBAX / Poroshell120 LC : 5-6 J&W DB-WAX GC : 7-8 ICP-OES MP-AES ICP-MS : 12 Bond Elut 25%OFF Bond Elut 25 %OFF Bond Elut, Mega Bond Elut Bond