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( 1) 100% (, Feringa, Nature, 1999) 1 (, Nature Commun. 2010) 2 (, Nature, 2007) 3 (, Nature, 2003) 4 ( 2) 3 1 C2- (9,9ʼ- ) ( 3)2 ( 4)3 (N-) () ( 5) 3. * ne-handed helix * ptically Active group Positional Switching * * Random helix Rational Design to Control Helical Polymers 4. (i)(ii)

C2-symmetric Cs-symmetric Coil-shaped Screw-shaped (1) C 2-9,9-2 / [Chem. Commun. 2015] (2) C 2-9,9 - [ACS Macro Lett. 2015] α CD [2] [3] α CD CD α CD [2][3] [3] CD head-to-head [Chem. Lett. 2012]

rg. Lett. 2012 Rotaxane-from method ACS macro Lett. 2013 Rotaxane-from method [2] rg. Lett. 2013 rg. Lett. 2013 - (BEK) (rg. Lett. 2013, Polym. J. 2014) ACS macro Lett. 2013

Polym. J. 2014 poly-(r)-1a NMe Through Space Chirality Transfer ne-handed Folded Helix poly-(r)-1a poly-(r)-1b TFA DBU ptically Active wheel (Far) (Close) NMe H Random Coil poly-(r)-1b poly-(r)-1a CF 3C poly-(r)-1b Angew. Chem., Int. Ed., 2015 Chem.Lett. 2015; ACS macro Lett. 2015 C. Wang, Y. Koyama, S. Uchida, T. Takata, Synthesis of Highly Reactive Polymer Nitrile N-xides for Effective Solvent-free Grafting, ACSMacro Lett. 2014, 3, 286-290, DI: 10.1021/ mz500069f K. Iijima, Y. Koyama, S. Uchida, T. Takata, Stimuli-Degradable Cross-Linked Polymers Synthesized by Radical Polymerization Using a Size-Complementary [3]Rotaxane Cross-Linker, Polym. J. 2014, 46, 67-72, DI:10.1038/ pj 2013.63 S. Suzuki, K. Matsuura, K. Nakazono, T. Takata, Effect of a Side Chain Rotaxane Structureon the Helix-Folding of Poly(m-phenylene diethynylene), Polym. J. 2014, 46, 355-365, DI:10.1038/ pj.2014.4 D. Aoki, S. Uchida, T. Takata, Mechanically linked Block/Graft Copolymers: Effective Synthesis via Functional Macromolecular[2]Rotaxanes, ACSMacro Lett. 2014, 3, 324-328, DI:10.1021/ mz5001306 D. Aoki, S. Uchida, T. Takata, Synthesis and Characterization of a Mechanically Linked Transformable Polymer, Polym. J. 2014, 46, 546-552, DI:10.1038/ pj 2014.22 Y. Abe, H. kamura, S.Uchida, T. Takata, Synthesis of main chain-type liquid crystalline polyrotaxanes: influoence of the wheel components and their mobility on liquid crystalline properties, Polym. J. 2014, 46, 553-558, DI: 10.1038/ pj.2014.23 K. Nakazono, T.Ishino, T.Takashima, D. Saeki, D. Natsui, N. Kihara, T. Takata, Directed ne-pot synthesis of Crown Ether Wheel-Containing Main Chain-type Polyrotaxanes with Controlled Rotaxanation ratio, Chem. Commun. 2014, 50, 15341-15344, DI:10.1039/C4CC06943A Y. Koyama, T. Yoshii, Y. Kohsaka, T. Takata, Photo-Degradable Cross-Linked Polymer Derived from a Vinylic Rotaxane Cross-Linker Possessing Aromatic Disulfide Axle, Pure & Appl. Chem. 2013, 85, 835-842, DI: 10.1351/PAC-CN-12-08-14 T. Arai, K. Jang, Y. Koyama, S. Asai, T. Takata, Versatile Supramolecular Cross-Linker: Rotaxane Cross-Linker that Directly Endows Vinyl Polymers with Movable Cross-Links, Chem. Eur. J. 2013, 19, 5917-5923, DI: 1-.1 2/chem201204402 R. Seto, Y. Koyama, K. Xu, S. Kawauchi, T. Takata, Exact Helical Polymer Synthesis by Directionally Fixed Connection of C 2 -Chiral 9,9 -Spirobifluorene Unit with C 2 - or C s -Symmetric Unit, Chem. Commun. 2013, 49, 5486-5488, DI:10.1039/C3CC41685B, D. Aoki, K. Nakazono, Y. Koyama, S.Uchida, T. Takata, Synthesis and Characterization of Macromolecular [2]Rotaxane Having Polymer Chain, ACSMacro Lett. 2013, 2, 461-465, DI:10.1021/mz400197d H. Iguchi, S. Uchida, Y. Koyama, T. Takata, Polyester-containing α-cyclodextrin-based Polyrotaxane: Synthesis by Living Ring-opening Polymerization, Polypseudorotaxanation, and End-capping Using Nitrile N-xide, ACSMacro Lett. 2013, 2, 527-530, DI: 10.1021/ mz4002518 H. kuda, Y. Koyama, T. Takata, 9,9-Diaryl-4,5-diazafluorene-based Cardo Polymer; Synthesis and Characteristic Properties, J. Polym. Sci. Polym. Chem. 2013, 51, 4541-4549, DI:10.1002/pola.26870S. Cheawchan, Y. Koyama, S. Uchida, T. Takata, Polymer, 2013, 54, 4501-4510, DI:10.1016/j.polymer 2013.06.020 T. Yuki, Y. Koyama, T. Matsumura, T. Takata, Click Annulation of Pseudo[2]rotaxane to [2]Catenane Exploiting Homoditopic Nitrile N-xide, rg. Lett. 2013, 15, 4438-4441, DI:10.1021/ol 401986u C. Wang, Y. Koyama, M. Yonekawa, S.

Uchida, T. Takata, Polymer Nitrile N-xide Directed toward Catalyst-and Solvent-Free Click Grafting, Chem. Commun. 2013, 49, 7723-7725, DI:10,1039/c3cc42992j Y. Koyama, T. Matsumura,. Ishitani, T. Takata, Fluorescence Control of Boron Enaminoketonate Using a Rotaxane Shuttle, rg. Lett. 2013, 15, 4686-4689, DI:10.1021/ ol 401984j Y. Akae, T. Arai, Y, Koyama, H, kamura, K. Johmoto, H. Uekusa, S. Kuwata, T. Takata, ne-pot Synthesis of Permethylated α CD-based Rotaxanes Having Alkylene Chain Axles and Their Structural Caracteristics, Chem. Lett. 2012, 41, 806-808. DI: 10.1246/cl.2012.806 Y. Abe, H. kamura, K. Nakazono, Y. Koyama, S. Uchida, T. Takata, Thermoresponsive Shuttling of Rotaxane Containing Trichloroacetate Ion, rg. Lett. 2012, 14, 4122-4125. DI: 10.1021/ol301771w M. Yonekawa, Y. Koyama, S. Kuwata, T. Takata, rg. Lett. 2012, 14, 1164-1167. DI: 10.1021/ol300125s 29 T. Takata, D. Aoki, S. Uchida, Transformable Polymer Architectures Functioned by Movable Linkages-Role of Rotaxane Linkage for Polymer Topology Change, 2014 7 1 7 4 High Tech Polymer Materials (HTPM)2014, Chinese Academy of Science (China) H. Sogawa, H. kuda, T. Takata, Structural Switch and Application of Exact Helical Foldamer Containing C 2 -chiral Spirobifluorene in the Main Chain, Chirality-2014, 2014 7 27 7 30 PragueCzech T. Takata, Y. Koyama, Macrocycle Catalyst for Highly Efficient Hydroaminatino via Cavity-Threading of Substrate as the Key Process, CRC International Symposium on Synthesis and Application of Functional Molecules and Materials Utilizing Biomolecules as a Motif, 2014 9 39 10 1, Hokkaido University (Sapporo) T. Takata, Chiral Rptaxane Catalysts for Asymmetric Reactions, MC Asia 2014, 2014 10 29 10 31, Beijing (China) T. Takata, T. Arai, K. Jang, Y. Koyama, Thermo-responsive Hydro Gels Networked by Rotaxane Cross-links, Polymer Network and Gel 2014 (PN&G2014), 2014 11 10 11 14 University of Tokyo (Tokyo) Toshikazu Takata, Intelligent Polymer Materials Characterized by Rotaxane Linkages, Yamagata University International Commemorative Symposium of GMAP Center, 2014 1 23 1 24, Yamagata University (Yamagata) T. Takata, Synthetic Protocol of Cyclic Polymer from Linear Polymer and Reversible Linear-Cyclic Polymer Topology Conversion, 245 th ACS Annual Meeting, 2013 4 7 4 11, New rleans (USA) T. Tkaata, Topological Chirality: Powerful Dynamic Chirality, 25 th International conference on Molecular chirality, 2013 7 7 7 10, Shanghai (China) T. Takata, Transformable Polymer Architectures Functioned by Movable Linkages, The 13th Pacific Polymer Conference 2013,2013 11 17 11 22, Kaohsiung (Taiwan)

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