Pittsburgh Conference for Analytical Chemistry and Applied Spectroscopy Pittcon2000 Pittcon Pittsburgh Conference for Analytical Chemistry and Applied
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1 N o JES-FR30 LEO 912AB JSX-3220Z NM-MB Dual View Camera PC ESR SpecInfo JEOL DATUM INFORMATION
2 Pittsburgh Conference for Analytical Chemistry and Applied Spectroscopy Pittcon2000 Pittcon Pittsburgh Conference for Analytical Chemistry and Applied Spectroscopy 1950 Spectroscopy of Pittsburgh "Science for the 21st Century" Morial Convention Center 8 67,000m 2 54,000m 2 1,280 27, , DNARNA JEOL40 LCMS JMS-LCmateFT NMR (Agilent 2100 BioAnalyzer) JNM-ECP400 JSM-5900LV3 Pittcon Best New Products: Gold Award Lab-on-a-Chip Lab-on-a-Chip 21 MS 2 ANALYTICAL NEWS
3 ESR ESR JES-FR30 - O2 Fenton OH OH ESR ESR ESR C 1 - O2 HPX XOD DMPO [1] - DMPOO2 2(a) 12 2(b) (d) - O2 - O2 DMPO - O2 1-2O2 - O2 1 - O2 - O2 1 (10 6 M -1 s -1 ) () UC 1 R1=OH, R2=H R1=H, R2=OH ESR 20,000/ [1]. M. Hiramatsu and M. Kohno, JEOL NEWS 23A, 7 (1987) TEL ANALYTICAL NEWS 3
4 EO LEO 912AB TEM TEM TEM X EDS TEM LEO912AB TEM TEM 1 4 LEO912AB LEO912AB TEM LEO912AB LEO912AB E=887eV 1. LEO 912AB 2. H2O2 4 ANALYTICAL NEWS EO
5 EO X JSX-3220Z X X EDS EDXRF NaC U ppm X-Y 15mm CCD 1mm CCD 0.3mm FP JSX-3220Z JSX-3220Z 1 X 2 4. CCD 1. 10mm 5 1mm mm 0.3mm 2. CCD X-Y 3 CCD X-Y kV X AgCdInSn K 2IC 1. JSX-3220Z 6. IC CCD8. IC Au IC 0.3mm EO ANALYTICAL NEWS 5
6 NMR AI (SPE) 4.5mL(48) ( ) Lead Discovery (1 4mL(48)8mL(24)16mL(12)32mL(6) 5mL) Lead Optimization (525mL) 48 2 SPE Mettler-Toledo Bohdan Bristol-Myers Squibb20801 PP Neptune TM ) Neptune 2 (96 ), ( 64) Dry Down Vial (48) Dry Down Vial Deep Well Plate Neptune ANALYTICAL NEWS 2 4.5mL(PP) (300) (5) (50)
7 NM-MB 1) 1 2 2) 3) ) 48 ( 3 4 5) PP 6) SPE 2 SPE ) 48 8) mm2.5mL mm5 ml ml/ 48 5 ml/ mL/ SPE MiniBlock Reactions Alkylation Reduction Acylation Saponification Biaryl Coupling Sulfonylation Enolate Formation SnAr 24 ( 8mL Grignard SPE Purlfication 12 (16mL Heterocycle Formation TFA Cleavage 6 (32mL 4mL ( ) Reductive Amination ,800,000 Mettler Toledo Bohdan Neptune) AI TEL FAX ANALYTICAL NEWS 7
8 NMR EM Dual View Camera CCD Dual View Macintosh-PCWindows-PC 360 (Digital Micrograph) CCD 1,0301, m6.7m 15 / 12-Bit 4, , MHz /60Hz 80W 478mm (W )44mm (D)88mm () Dual View CCD GATAN 1 TEM ,0301,300 CCD 12 4 Digital Micrograph TEM Industry standard 5MacWindows Dual View Mac Windows 13,000,000 3 TEL FAX ANALYTICAL NEWS
9 PC ESR SpecInfo Internet ESR SpecInfo ESR PC ESR HP EWS HP EWS EWS g IBM PC17 AD Mn g OS Windows SpecInfoNMRMSIR & 200, C-NMRMSIR 660,000 SpecInfo SpecInfo (JCAMP) 1 NMR 2 30 Wiley 5,000( 13 C- 1 H-Hetero-NMRIRMS) 13 C-NMR2,000 Chemical Shift 1, URLe- 2, e- 3, Windows Internet Explorer 4.01 SPI5.0, IRIX Netscape Navigator4.05 Netscape Navigator4.07Java Macintosh 1) ESR STATUS REFRESHESR 2) 3) AUTO SAVE SAMPLE001 4) 5) 6) 3 2 RESULT 7) PRINT PREVIEW C-NMR PC 2 ESR ES-IPRIT RDA-03W JES-FE ESR JES-RE, TE JES-RE, TE ES-IPRITRDA-03W ES-IPRIT 3,350,000 RDA-03W 4,000,000 AITEL SpecInfo v3.2basic version(32,000) 1,800,000840,000 SpecInfo v3.2 Chemical Concepts/Wiley AI1 ;specinfo@jeol.co.jp ANALYTICAL NEWS 9
10 DiATOME DiATOME ( ) DiATOME Du pont NACC DiaTech DDK DRUKKER JUMDI MicroStar TEL FAX ˇ 3 TEL FAX hist hist 1.5mm 2.0mm 2.5mm 3.0mm 3.5mm 4.0mm 35 /45 35 /45 35 /45 35 /45 35 /45 35 /45 200, , , , , , , , , , , ,250 ultra/cryo-dry/cryo-wet ultra/cryo-dry/cryo-wet ultra/cryo-dry/cryo-wet ultra/cryo-dry/cryo-wet ultra/cryo-dry/cryo-wet ultra/cryo-dry/cryo-wet 4.0mm 6.0mm 8.0mm 10.0mm , , , , , , , ,000 hist/hist-cryo hist/hist-cryo hist/hist-cryo hist 230, , , , , , , , , , , , , , , , , , , , ANALYTICAL NEWS
11 JEOL DATUM INFORMATION NMRMS NMR CRT NM-VT4207/NM-VT4211 JNM-EX90/270/ EXcalibur CRT EXcalibur NMRMS 5 NM-OD9200E/EII/EXE, JMO600 JNM-GX/GSX/EX/A JMA-DA5000/ JMO540 JMO MByte MO A3/A4 NM-PL7550SMS-PL7550 JNM-GX/GSX/EX/A JMA-DA5000/ DLP8000 DLP8000A3 MS 1. DIOK 2 3 DIOK SIM SIM GC GC VT4207 VT MS MSMS NMR NMR 1 H 13 C NMR NOE NMRNMR NMR 4NMR NMR 621 TEL FAX TEL , , , ,000 MS LCMS NMR ANALYTICAL NEWS 11
12 INFORMATION (1)SEM 1S E M (2)SEM 2S E M SEMEPMA (3) 2 (1) / 8900 E P M A (2) 28800/ (3) 28800/ (1)EPMA 2E P M A (1)TEM 1T E M (2)2010TEM (3)1230TEM (4)1010TEM (5) 1A S I D (6) 1 (1) 2 (2)TEM 1 (3) (5) 2 (6) 2 (7) 2 (8) 2 (9) 2 (1)5000 SEM S E M (2)5800SEM S E M (3)SEM 3S E M (4)FE-SEM 3F E - S E M (5)LV-SEM 1L V - S E M (6) SEM 2 S E M (7)EDS 2J E D E D S :3017: (4) (1)LA41 D / 2 D 1 H 1 3 C (2)AL 1 2A L (3)AL 2 21 D / 2 D 1 H 1 3 C (4)ECP41 D / 2 D 1 H 1 3 C [NMR] E C P A l p h a L a m b d a Phase Sensitive 2D N O E H O H A H A R O E S Y 26 1H M Q C / H M B C 27 (12) / (1) 3M S S I M (2) 3D i o k (3)MStation 3M S 1214 (4)GCmate 3M S G C / M 1315 (5)Automass2M S (6)Automass CI/DI 1 (7)Automass (P&T) 2P & T V O C (8)Automass (H.S.) 2H. S. V O C E S R (5)ECP 2ECP (6) 2D-NMR (7)NOE & NOESY (8)HOHAHA (9)ROESY (10)HMBC/HMQC (11) NMR (13)FG-NMR 2 1F G - N M R (14)DPFGSE1D P F G S E N O E JIR WINSPEC 2 FT-IR WINSPEC JES-FA N M R 6 3 TEL (042) FIR50/60/702 FT-IR 50/60/ E - m a i l usersmt@jeol.co.jp" " E - m a i l Fax ANALYTICAL NEWS achiba@jeol.co.jp FAX usersmt@jeol.co.jp FAX No F TEL FAX TEL FAX (042) (011) (022) (0298) (045) (052) (06) (082) (087) (092)
,000 21Dr. Kurunthachalam Kannan (MI,USA) Global Distribution of Perfluorooctane Sulfate in Wildlife2 PCB ANALYTICAL N
ANALYTICAL NEWS No.048 JSX-3600 Windows2000SEM FT-IR JES-EIRA1 2020 NMR 2 JEOL DATUM INFORMATION 10 10523 25 1,000 21Dr. Kurunthachalam Kannan (MI,USA) Global Distribution of Perfluorooctane Sulfate in
48ASMS Conference 48ASMS (American Society for Mass Spectorometry) Conference 61115 5 1 3,800 30 6 300400 4 250 611 JEOL USA JEOL USA NanoESI LC-MS/ N
N o.0 4 4 JSM-6500F JSPM-4210 -SNOM 17- JMS-700 MStation JEOL DATUM INFORMATION 48ASMS Conference 48ASMS (American Society for Mass Spectorometry) Conference 61115 5 1 3,800 30 6 300400 4 250 611 JEOL
A.N 61
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