橡紙（山添）
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1 Research on development and industrialization of the dental ceramics Masatoshi Yamazoe
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5 1889 Dr.C.H.Land 1
6 1954 NEY 1963 VITA Degussa 1), 2) ,
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11 1.4 Apply opaque Fired opaque Form dentine Form enamel Completion 1.4 7
12 1) ) BIO INDUSTRY2 (8) ) 92(4) ) Report of the Institute for Medical & Engineering ) P.J.Adair and D.G.GrossamInt.Periodont.Rest.Dent
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44 ) NaK
45 4SiO2Al2O3K 2O=KALSi2O
46
47 3.2 G67100 L L1 G
48 NaK
49 Na K 8 NaK
50
51 3) Ag2O Ce2O 3 2Ag0 2CeO2 CeO SiO2Al2O 3K 2O 47
52 CeO2 48
53 No SiO2 15.0Al2O310.7K2O 8.5Na2O0.3MgO1.2CaO0.6B2O 3(wt%) No SiO2 15.0Al2O311.8K2O 9.0Na2O0.3MgO1.2CaO0.6B2O 3(wt%) 55.1SiO2 23.3Al2O3 21.6K2O(wt%) No.1 No.2 SiO CeO2 75m m
54 CeO2 1 2 No.1 SiO2 CeO2 1 3 No.1 SiO2 1.5 CeO2 1 4 No.1 SiO2 2.0 CeO2 1 5 No.2 SiO2 4.0 CeO mm 2 JIS T
55 JIS T CeO CeO
56 4) CeO Tb4O SiO2Al2O 3K 2O 52
57
58 CeO2 Tb4O
59 No SiO2 15.0Al2O310.7K2O 8.5Na2O0.3MgO1.2CaO0.6B2O 3(wt%) No SiO2 15.0Al2O311.8K2O 9.0Na2O0.3MgO1.2CaO0.6B2O 3(wt%) 55.1SiO2 23.3Al2O3 21.6K2O(wt%) SiO2 CeO2 Tb4O7 CeO2 Tb4O7 75m m CeO2 Tb4O7 2 No.1 SiO CeO2 3 Tb4O7 1 No.1 SiO2 CeO2 55
60 0.05 Tb4O7 1 4 No.1 SiO2 1.5 CeO2 0.5 Tb4O7 1 75m JIS T JIS T nm 56
61 NaK CeO CeO2 4 57
62 NaK PCT/JP01/
63 ) 59
64 60
65 61
66 62
67 63
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69 65
70
71 Table Composition and coefficient of thermal expansion of noble metal for dental ceramics for tests used Au Pt Pd Ag
72 5.1.2 A, B C D E ) 784N80kgf/cm mm 1,2, mm TD5010S 5 /min 50~500 2) 2 2)-1 3mm mm 68
73 2 6mm 3mm 2 AGS-500 5mm/min 4 l 8 2 MPa Kgf/0.102dl 2) mm # mm 10.0mm 14.0mm 2 69
74 1.0mm 3) JIS T 6516 AGS-10KND 14mm 1.0mm/min 4) 588N60kgf/cm t 5.0mm #180#2000 3m1m HMV N 15 5) S-3500N 10 70
75 6) ) ,2,4 71
76 Thermal expansion curve of ZEO CE LIGHT and noble metal for dental ceramics. 72
77 of thermal expansion of translucent porcelain with the number of firing times (A, B, C, D and E are other companies products). 73
78 2)
79 Adhesive strength and compatibility with metals for each type of porcelain (A, B, C, D and E are other companies products). 75
80 (A, B, C and D are other companies products) 76
81 3)
82 (A, B, C, D and E are other companies products) 78
83 (A, B, C, D and E are other companies products) 79
84 (A, B, C, D and E are other companies products) 80
85 4) Figure Cracks in metal-ceramics made the metal of difference kinds. 81
86 Evaluation on tests of commercial dentine/enamel porcelain 82
87 ~
88 nm A, B C D E 1) 84
89 588N60kgf/cm t 5.0mm #180#2000 3m1 m mm 365nm UV 2) FP nm nm 3) X RIX2000 4) Au1.0Pt28.3Pd13.0Ag B1 85
90 365nm UV ) A,B,C,E D A 86
91 Figure Fluorescence of natural teeth under 365nm light. 87
92 Figure Fluorescence of porcelains under 365nm light (A, B, C, D and E are other company s products). 88
93 2) nm 89
94 Figure Fluorescent spectrum curve of natural tooth and porcelain under 365nm light (A, B, C, D and E are other company s products). 90
95 3) SiO2, Al2O3, K2O Na2O CeO2,Tb4O7 A B C Y2O 3 Ce Y2SiO5 Table Composition of porcelain (A, B, C, D and E are other company s products) Li, B Non-Aanalysis 91
96 4)
97 Figure Metal-ceramic restorations under 365nm light (A, B, C, D and E are other company s products). 93
98 Figure Fluorescence of a natural tooth and ZEO CE LIGHT. 94
99 Table Visual evaluation with the natural tooth in the fluorescence characteristic 95
100 ~
101 97
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103 Products name and producing country of commercial porcelains for tests used 99
104 Firing schedule of repairing and dentine/enamel porcelain light (A, B, C, D and E are other company s products) 100
105 Composition and coefficient of thermal expansion of noble metal for dental ceramics for tests used 101
106 Cu K N 80kgf/cm mm mm 0.025mm TD5010S 5/min N60kgf/cm t 5.0mm DE 102
107 930 D 770 E 890 #180#2000 2mm 11.5mm 2.5, t 1mm A, B, D, E A 740 B 870 C 760 D 780 #180#2000 3m1m S-3500N 16.0 t1.6mm A, B, D, E A 750 B 880 C 770 D
108 0.1mg JIS T vol% 16 7) 588N 60kgf/cm , t 2.0mm A, B, D, E A 740 B 870 C 760 D 780 V-550 E*ab 104
109 B, D, E B 870 D 745 E
110 X-ray patterns and leucite contents of repairing porcelain powder (A, B, C, D and E are other company s products). 106
111 107
112 The coefficient of thermal expansion of dentine/enamel and repairing porcelain (A, B, C, D and E are other company s products). 108
113 109
114 Particle size distribution of repairing porcelain (A, B, C, D and E are other company s products). 110
115 SEM micrographs of powder of repairing porcelain (A, B, C, D and E are other company s products). 111
116 112
117 SEM micrographs of the polished interface repairing and dentine/enamel porcelain (A, B, C, D and E are other company s products). 113
118 SEM micrographs of the etched interface repairing and dentine/enamel porcelain (A, B, C, D and E are other company s products). 114
119 Chemical solubility of repairing porcelain (A, B, C, D and E are other company s products). 115
120 116
121 Composition of repairing porcelain (A, B, C, D and E are other company s products) 117
122 Yellowish discolorations by silver of repairing porcelain (A, B, C, D and E are other company s products). 118
123 119
124 Metal-ceramic restorations (B and D are other company s products). 120
125 Evaluation on tests of commercial repairing porcelain
126 A wt B 3.8 C D B, C Sb2O
127 6) 123
128
129 6 5 0 A, B ~
130 5 m MPa HV 485 (2.45%) (84.1%) 126
131 Kg/
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133 2 129
134 130
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STRAUMANN CARES Straumann CARES Tooth-borne prosthetic CARES Scan CS2 13B1X10163000158 3M TM ESPE TM Lava TM Relyx TM Filtex TM Scotchbond TM 3M IPS e.max IPS Empress Ivoclar Vivadent VITA VITA Zahnfabrik
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