PowerPoint プレゼンテーション

86 MS MS GC LC GC LC Fig. 1.MS 3. 質 量 分 析 計 の 構 成 1 試 料 導 入 部 2イオン 化 部 3イオン 分 離 部 4イオン 検 出 部 5データ 処 理 部 10 4 10 6 Pa Fig. 2.

Bulletin of Osaka University of Pharmaceutical Sciences 6 (2012) 85 有 機 化 学 実 験 のための 易 しいマススペクトロメトリー Concise Mass Spectrometry for Experiments of Organic Chemistry Note Mihoyo Fujitake Osaka University

橡ﾏﾆｭｱﾙv4c.PDF

LC/MS MS LC/MS LC LC (APCI) (ESI) FAB 2 LC (APCI) 4.1.1.1 LC LC/MS LC MS LC 3 ph APCI/MS LC (1) APCI ESI 100% 100% ESI 4.1.1-1 LC 1.00cp 100 34 a 4.1.1-1 LC b ( /mpas) n- 0.23 36 0.5 99 0.31 69 n- 0.92

C:CAD?????????w???W??KUT?????????4?N?????O???I??1?O_?I??1?i???jweb?p.IPO

Microsoft Word - 5MS.doc

5 5.1 mass spectrometer electron impact, EI 5.1 :;"< 789 =>? *!"#$%& '%&(),,,-./ 0.12%3456 :;"@AB CDEFG:;"HIJK@LMN :;"@HIOPQ0RST6 5.1. 70 ev molecular ion #"$%& M M e!"!"'() #" m/z ; m = z = 1 mass spectrum,

J. Mass Spectrom. Soc. Jpn.: 58(5), (2010)

J. Mass Spectrom. Soc. Jpn. Vol. 58, No. 5, 2010 REVIEW 9 Secondary Ion Mass Spectrometry (SIMS) SIMS SIMS Fundamentals of Mass Spectrometry Secondary Ion Mass Spectrometry (SIMS), Cluster SIMS, and Electrospray

Japanese Journal of Pesticide Science 42(1): (2017)

42(1), 203 203 215 (2017) DOI: 10.1584/jpestics.W17-54 1, * 2, ** 3, *** 4, **** 4 1 2 3 4 2017 1 6 Recent data analysis technique in mass spectrometry Takaya Satoh, 1 Kentaro Takahara, 2 Tomoaki Kondo,

2 3

VISPO /表1-4

7 2005 1,132 5,249 362 13,666 311,809 1,359 3,723 1,669 538 3,737 17,418 39,036 75,694 5,281 1,169 161,502 7,463 11,408,436 500,000 13,263 192,052 41,391 49,706 136,232 61,102 12,402,182 11,573,898 273,042

2357

1

J. Mass Spectrom. Soc. Jpn. Vol. 50, No. 6, 2002 COMMUNICATION Hydrogen-Attachment Dissociation (HAD) The Characteristics of In-source Decay in Mass S

J. Mass Spectrom. Soc. Jpn. Vol. 50, No. 6, 2002 COMMUNICATION Hydrogen-Attachment Dissociation (HAD) The Characteristics of In-source Decay in Mass Spectrometric Degradation Methods Hydrogen-Attachment

yamato_2016_0915_色校_CS3.indd

４章　困難な課題への挑戦　核酸結晶学

4-2-6. I. a. DNA DNA RNA Watson & Crick 1953 b. DNA DNA DNA DNA RNA Cech et al. 1981 RNA in vitro selection DNA Breaker & Joyce 1994 2% 50% 30% International Human Genome Sequencing Consortium 2001 1 DNA

untitled

untitled

186 17 100160250 1 10.1 55 2 18.5 6.9 100 38 17 3.2 17 8.4 45 3.9 53 1.6 22 7.3 100 2.3 31 3.4 47 OR OR 3 1.20.76 63.4 2.16 4 38,937101,118 17 17 17 5 1,765 1,424 854 794 108 839 628 173 389 339 57 6 18613

untitled

1. 3 14 2. 1 12 9 7.1 3. 5 10 17 8 5500 4. 6 11 5. 1 12 101977 1 21 45.31982.9.4 79.71996 / 1997 89.21983 41.01902 6. 7 5 10 2004 30 16.8 37.5 3.3 2004 10.0 7.5 37.0 2004 8. 2 7 9. 6 11 46 37 25 55 10.

(1519) () 1 ( ) () 1 ( ) - 1 - - 2 - (1531) (25) 5 25,000 (25) 5 30,000 25,000 174 3 323 174 3 323 (1532) () 2 () 2-3 - - 4 - (1533) () 1 (2267)204 () (1)(2) () 1 (2267)204 () (1)(2) (3) (3) 840,000 680,000

スタイルシェルフ　〈クローク収納プラン〉

2

<31332D97708CEA89F090E02E6D6364>

1 2 http://www.japan-shop.jp/ 3 4 http://www.japan-shop.jp/ 5 6 http://www.japan-shop.jp/ 7 2,930mm 2,700 mm 2,950mm 2,930mm 2,950mm 2,700mm 2,930mm 2,950mm 2,700mm 8 http://www.japan-shop.jp/ 9 10 http://www.japan-shop.jp/

マイスタープロジェクト　推奨仕様

1

第18回海岸シンポジウム報告書

2011.6.25 2011.6.26 L1 2011.6.27 L2 2011.7.6 2011.12.7 2011.10-12 2011.9-10 2012.3.9 23 2012.4, 2013.8.30 2012.6.13 2013.9 2011.7-2011.12-2012.4 2011.12.27 2013.9 1m30 1 2 3 4 5 6 m 5.0m 2.0m -5.0m 1.0m

3

(718)

1 911 34/ 22 1012 2/ 20 69 3/ 22 69 1/ 22 69 3/ 22 69 1/ 22 68 3/ 22 68 1/ 3 8 D 0.0900.129mm 0.1300.179mm 0.1800.199mm 0.1000.139mm 0.1400.409mm 0.4101.199mm 0.0900.139mm 0.1400.269mm 0.2700.289mm

液晶ディスプレイ取説TD-E432/TD-E502/TD-E552/TD-E652/TD-E432D/TD-E502D

1 2 3 4 5 6 7 1 2 3 4 5 6 7 2 2 2 1 1 2 9 10 11 12 13 14 15 16 17 1 8 2 3 4 5 6 7 1 2 3 4 5 6 7 8 9 10 9 11 12 13 13 14 15 16 17 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 1 2 3 4 5 6 7 8 9 11 12

() () ()

1 1 36 223 42 14 92 4 3 2 1 4 3 4 3429 13536 5 6 7 8 9 2.4m/ (M) (M) (M) (M) (M) 6.67.3 6.57.2 6.97.6 7.27.8 8.4 5 6 5 6 5 5 74 1,239 0 30 21 ( ) 1,639 3,898 0 1,084 887 2 5 0 2 2 4 22 1 3 1 ( :) 426 1500

1 C 2 C 3 C 4 C 1 C 2 C 3 C

1 e N >. C 40 41 2 >. C 3 >.. C 26 >.. C .mm 4 C 106 e A 107 1 C 2 C 3 C 4 C 1 C 2 C 3 C 108 109 110 111 112 113 114 115 116 117 118 119 120 121 122 123 124

<967B95D2955C8E F4390B32E6169>

平成２４年財政投融資計画ＰＤＦ出後８／０１６‐０３０

24 23 28,707,866 2,317,737 26,390,129 29,289,794 2,899,665 24 23 19,084,525 21,036,598 1952,073 24 23 8,603,613 8,393,427 967,631 925,404 202,440 179,834 217,469 219,963 66,716 64,877 3,160,423 2,951,165

000-.\..

1 1 1 2 3 4 5 6 7 8 9 e e 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 10mm 150mm 60mm 25mm 40mm 30mm 25 26 27 1 28 29 30 31 32 e e e e e e 33 e 34 35 35 e e e e 36 37 38 38 e e 39 e 1 40 e 41 e 42 43

[mm] [mm] [mm] 70 60 50 40 30 20 10 1H 0 18 19 20 21 22 23 24 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 1 2 3 4 5 6 7 8 9 10 11 12 60 50 40 30 20 10 0 18 19 20 21 22 23 24 1 2 3 4

ochem2_30

第 30 回 有機化合物の構造決定 (2) NMR NMR NMR 質量分析法 赤外分光法 NMR 1. 質量分析法の原理 1913 Thomson (Proc. R. Soc. Lond. A 1913, 89, 1 26) Thomson Thomson 20 Ne 22 Ne Thomson mv/qb m q v B m/q Thomson 1 EI 法 ( electron ionization,

Microsoft Word - 14_LCMS_アクリルアミド

3--2-3-Iodo-2-propynyl butylcarbamate (IPBC) Carbamic acid, butyl-, 3-iodo-2-propynyl ester Iodocarb CAS 55406-53-6 C 8 H 12 NO 2 I C (g/cm 3 ) (mmhg) log P ow 281.09 (280.9910) 64 68 1.51 1.57 (20 C)

10 10 10095 95 100 108

25491231 21 21 114 10 10 10095 95 100 108 10 10 2510 079685 10 100 109 20 2015 110 134 e [ 350 350 145 18 111 112 16 18 16 18 1816 18 20 48 25 20315 28 113 114 25 05 03 01 20 100150 Q & A Q A 18 16 Q &

untitled

MALDI-TOF-MS : imaging X (MRI/MRS) (CT) (PET) 2009 8 8 ( ) 15:39 UTC Imaging mass spectrometry(ims) MALDI (Matrix-Assisted Laser Desorption Ionization ) SIMS (Secondary Ion Mass Spectrometry) DESI (desorption

1 WSV SIR m/z Analyte RT (Min) SIR m/z Cone voltage (V) Ascorbic Acid (C).91 177 2 Thiamine (B1) 1.1 265 5 Nicotinic Acid (B3) 1.27 124 15 Pyridoxal (

ACQUITY UPLC H-Class ACQUITY QDa Mark E. Benvenuti, Dimple Shah, and Jennifer A. Burgess Waters Corporation, Milford, MA, USA MS ACQUITY QDa UPLC HPLC UV ACQUITY QDa LC EC 1925/26 CFR 21 HPLC 1 LC-MS ACQUITY

平成23年度電気設備技術基準関係規格等調査役務請負報告書

1 V 3 L 150 100 V 6 I 10 1 V 3 L 2 1 I1 2 3 0 3 R R V R 3 10 X V X 3 10 R X 2 2 2 2 2 3 2 I 1 2 2 3 2 168 171-1

160mm OR16-34 ORB16-34 OR16-35 ORB16-35 OR16-43 ORB16-43 OR16-44 ORB16-44 OR16-45 ORB16-45 OR16-46 ORB16-46 OR16-47 ORB16-47 OR16-48 ORB16-48 OR16-53

IP44 120mm OR12-33 ORB12-33 OR12-34 ORB12-34 OR12-35 ORB12-35 OR12-36 ORB12-36 OR12-43 ORB12-43 OR12-44 ORB12-44 OR12-45 ORB12-45 OR12-46 ORB12-46 OR12-47 ORB12-47 OR12-48 ORB12-48 OR12-49 ORB12-49 OR12-53

untitled

27.2.9 TOF-SIMS SIMS TOF-SIMS SIMS Mass Spectrometer ABCDE + ABC+ DE + Primary Ions: 1 12 ions/cm 2 Molecular Fragmentation Region ABCDE ABCDE 1 15 atoms/cm 2 Molecular Desorption Region Why TOF-SIMS?

Microsoft PowerPoint - 藤田保険衛生大学

質量分析セミナー autoflex III LRF 韮澤崇 Bruker Daltonics K.K. MALDI Matrix Assisted Laser Desorption / Ionization マトリックス支援レーザー脱離イオン化 2 MALDI の基本原理 Matrix と Sample の混合結晶 LASER による Matrix の励起 脱離およびイオン化 ( プロトン化 ) LASER

I 2 ESI - Ion Trap

I 2 ESI - Ion Trap 2011 35 ESI 520l/min 35V V Taylor 20 R N- ESI) Intens. x10 8 1.0 14+ 15+ 883.9 825.1 Cytochrome c 12000 Da 09123cyto mass00003.d: +MS 0.8 0.6 0.4 0.2 0.0 17+ 728.1 16+ 773.6 13+ 951.8

- 1 - A T MC FDMS CADIN ATMC FDMS - 2 - - 3 - - 7 - - 8 - 16 4 53 :36 6 52 :71 53 52 () 53 52 () 1 41 02 9 39 02 2 32 02 10 40 01 3 29 00 11 38 01 4 38 01 12 38 01 5 41 01 13 39 02 6 7 8 34 00 14 39

Metabolomic Profiling_JA.qxp

LC/MS-TOF LC/Q-TOF GeneSpring MS BLB: Bacterial Leaf Blight Steven Fischer Senior Application Chemist Agilent Technologies Santa Clara, California U.S.A Theodore Sana Senior Research Scientist Agilent

27.\..

14 : : : : : : 00 LC/MS/MS 1, : : 00 Novel strategies and applications of enhanced shotgun lipidomics for

1 9 6 1 [ 講堂 ]2F 8 : 45-8 : 55 8 : 55-11 : 00 1 S1-1 1,2 1 2 S1-2 1 1 2 3 1 2 3 S1-3 1,2 1,2 1 2 S1-4 MALDI 1 2 1 2 S1-5 12 : 00-13 : 00 1 LS1 12 14 : 00-14 : 40 14 : 40-15 : 10 15 : 10-16 : 00 LC/MS/MS

Report Template

1 1 1 2 3 3 1 2 4 2 1 2 3 4 5 6 7 2 1 2 3 4 5 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 6 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 7 8 3 9 10 3 11 12 13 14 4 15 16 17 18 19 2 1 1 1 4

Taro9-111化兵条約法令集（和文）

:The Legal Texts 3. / 8. 6 8.1 8.1.1 C-I/DEC.35 8.1.2 6 C-II/DEC.6 8.1.3 C-I/DEC.38 8.1.4 C-I/DEC.33 8.1.5 C-I/DEC.40 8.1.6 C-I/DEC.34 8.1.7 C-I/DEC.36 8.1.8 EC-XIX/DEC.5 8.2 1 8.2.1 1 1 C-I/DEC.43 8.2.2

Japanese Journal of Pesticide Science 41(2): (2016)

Vol. 41, No. 2, 223 235 (2016) 41(2), 223 223 235 (2016) DOI: 10.1584/jpestics.W16-21 1, * 2, ** 3 3 3, *** 4, **** 1 2 3 4 2016 7 8 New ionization techniques in mass spectrometry Nobutake Sato, 1 Masaaki

(Hz) (kvar) (mm) A B C (kg) (L) 470 110 885 1995 1 0 700 895 5 120 2 300 990 0 130 400 1035 2095 6 0 1080 700 1 0 1120 710 800 190 7 1210 8 0 1255 2195 9 220 10 1 2300 1300 300 1195 0 1190 2400 10 3 470

12-7 12-7 12-7 12-7 12-8 12-10 12-10 12-10 12-11 12-12 12-12 12-14 12-15 12-17 12-18 10 12-19 12-20 12-20 12-21 12-22 12-22 12-23 12-25 12-26 12-26 12-29 12-30 12-30 12-31 12-33 12-34 12-3 12-35 12-36

☆H23 13－農薬一斉分析（大垣）.doc

13 56 2011 Examination of Determination of Residual Pesticides in Agricultural Products Yuki OHGAKI, Katsuhiro HAYASHI, Hiroyuki KAWAI, and Kyoko SHIMURA GC/MS 92 LC/MS/MS 60 150 n- 5 GC/MS 92 79 70% LC/MS/MS

Ⅱ6.3界面活性剤

6.3 6.3.1 6.3.1 6.3.1.1 (1) (2) a) JIS K 0557 A3 b) JIS K 8891 c) (5g/L) d) (10g/L)JIS K 8576 1g 100mL e) (7+993)JIS K 8951 f) JIS K 8322 g) 0.1g 100mL 30mL 1L 500mL6.8mL 50g 1L h) 1L 500mL6.8mL 50g 1L

<4D F736F F D F90858C6E5F C B B B838B>

Isobutyl alcohol IUPAC 2-methylpropan-1-ol 2--1-2-Methyl-1-Propanol, Isobutanol CH 3 H 3 C OH CAS 78-83-1 C 4 H 10 O log P ow ( C) ( C) (kpa) (g/l) 74.12 74.14 1) -108 2) 108 2) 1.2 2) 87 2) 0.8 2) (74.1214)

ニトロトルエン

4-115 116 4-3 2 117 4- g/kg/day mg/kg/day 25 125 30 40 50 100 250 300 ( ) ( ) ( ) ( ) F1 42 10 118 ER 10-11 M 1% 10-11 10-4 M ER 10-4 M 3% 10-11 10-4 M E-screen 10-9 10-4 M AR ( ) 10-6 10-4 M AR ( ) 10-6

low_ JAJP.qxd

LC/MS Chad Borges, Matthew Slawson, James Taccogno, and Dennis Crouch Center for uman Toxicology University of Utah Salt Lake City, UT USA John M. ughes Agilent Technologies, Inc. Pleasanton, CA USA (oa-tof)

Group A (2,5-Dimethoxyphenyl type) 25D-NBMe (1) 25B-NBMe (2) 25I-NBMe (3) 25C-NBF () 25B-NBF (5) Group B (Benzofuran-2-yl type) Group C (-Alkoxy-3,5-d

3 * * * * * Analytical data of designer drugs of synthetic phenethylamines Ryosuke SASAKI*, Miho KAT*, Tsuyoshi MATSUMT*, Akira UDAGAWA* and Ryuichi MATSUZAKI* *Tokyo Customs Laboratory 2-7-11, Aomi, Koto-ku,

J. Mass Spectrom. Soc. Jpn. Vol. 57, No. 2, 2009 Optimization of a Home-Built Desorption Electrospray Ionization Source and Its Application in Rapid A

脱離エレクトロスプレーイオン化質量分析用イオン源 Title の試作と迅速分析への応用 芳本, 有史, 元木, 翔一, 森脇, 悠介, 川崎, 英也, Author(s) 荒川, 隆一 Journal of the Mass Spectrometry Citation n, 57(2): 109-115 Issue Date 2009 URL http://hdl.handle.net/10112/6001

種々のイオン化法による質量分析法を用いる難溶性有 Title 機顔料の構造解析 浅井, 重博, 藤田, 憲一, 窪田, 雅之, 金井, みち子 Author(s), 川崎, 英也, 荒川, 隆一 Citation 分析化学, 57(4): Issue Date

種々のイオン化法による質量分析法を用いる難溶性有 Title 機顔料の構造解析 浅井, 重博, 藤田, 憲一, 窪田, 雅之, 金井, みち子 Author(s), 川崎, 英也, 荒川, 隆一 Citation 分析化学, 57(4): 265-271 Issue Date 2008-04-05 URL http://hdl.handle.net/10112/5918 Rights Type Journal

GPC/SEC

GPC/SEC Agilent GPC/SEC...3... 5...5...7...9...11...12... 13...13...14... 15...15...16... 18...18...19 /... 21...21... 23 GPC/SEC...24 Q Q Q Q Q 35 GPC/SEC 24 365 GPC/SEC GPC/SEC GPC 2 80 % 2006 - Polyplasdone

untitled

26 3 31 BDF BDF BDF FAME BDF BDF BDF BDF BDF BDF BDF BDF BDF FAME BDF BDF 80.0 97.0% BDF 120 330 0.8% 2.2% 1. 1 1-1 1 1-2 1 2. 2 2-1 2 2-2 5 2-3 6 3. BDF 7 3-1 7 3-2 7 3-3 14 3-4 JOY 21 3-5 32 3-6 39 3-7

スライド 1

API Gas API Topics API Gas Gas Heater Gas Temparature Gas Topics API Gas API Gas Curtain Gas 60PSI API Gas Neblizer Gas Gas1 TurboIonSpray API Gas Heater Gas Gas1 Gas2 Gas2 API Gas Exhaust Gas Exhaust

1 1 2 2 3 4 5 5 6 7 8 10 9 10 10 10 11 13 14 15 15 16 17 18 19 21 21 22 22 24 28 38 40 41 41 43 45 46 47 47 47 47 48 50 50 50 50 51 52 54 54 55 56 56 57 57 57 58 58 59 59 59 61 61 61 62 62 62 62 63 63

橡A PDF

2 1 MS 300 TRT MS JDI-800 2 g MS Py MS GC Py-GC Py GC 50 Py MS MS Py GC PY-GC 2 JDI-800 MS JDI-800 QP 2000 QP 1000 QP 2000 Fig 1 QP 1000 CI PEG 300 600 423 MS EI CI MS PEG 3 10 g Fig.1 300 600 MS 3 JDI-800

門川町報4月号

LC/TOF-MS MS ( )

LC/TOF-MS MS () (TOF-MS) MS) LC/MS 1. 2. Agilent 1100 LC/TOF-MS MS ~0.25ppm / C ambient Compound Exact mass Positive Negative Purine 121.050873 TFA 112.985587 Hexakis(1H, 1H, 3H 922.009798 966.000725 1)

UPC 2 Baiba Cabovska, Michael D. Jones, and Andrew Aubin Waters Corporation, Milford, MA, USA UPC 2 ACQUITY UPC 2TM ACQUITY SQD Empower 3 UPC GC

UPC 2 Baiba Cabovska, Michael D. Jones, and Andrew Aubin Waters Corporation, Milford, MA, USA UPC 2 ACQUITY UPC 2TM ACQUITY SQD Empower 3 UPC 2 1-3 GC LC GC UltraPerformance Convergence Chromatography

Matrix Assisted Laser Desorption Ionization (MALDI) サンプル調製 サンプルとケミカルマトリクスの混合 (1,1 to 1,1) Major advantage= ease of sample prep!! 質量分析 レーザーによる固相中でのイオン化

合成高分子への質量分析法の応用 1. GPC/MALDI MS の応用例 2. GPC/ API MS の応用例 27 Nihon Waters K.K. GPC/MALDI MS Matrixassisted laser desorption/ionization (MALDI) 質量分析は 複雑な混合物の大規模分析のための最も強力なツールの 1 つであり bulk polymer の MS 分析に有用

02-量子力学の復習

4/17 No. 1 4/17 No. 2 4/17 No. 3 Particle of mass m moving in a potential V(r) V(r) m i ψ t = 2 2m 2 ψ(r,t)+v(r)ψ(r,t) ψ(r,t) Wave function ψ(r,t) = ϕ(r)e iωt steady state 2 2m 2 ϕ(r)+v(r)ϕ(r) = εϕ(r)

MALDI-TOF 1, # Quantitative Analysis of Cashmere and Other Animal Hair Fibers in Textiles Using MALDI-TOF Mass Spectrometry Shinichi Ohashi 1,#,

MALDI-TOF 1, # 1 1 2 Quantitative Analysis of Cashmere and Other Animal Hair Fibers in Textiles Using MALDI-TOF Mass Spectrometry Shinichi Ohashi 1,#, Yuka Demura 1, Motoaki Sano 1, and Yoichiro Yoshioka

バイオ解析チーム教育セミナーMS04

LTQ Orbitrap Shotgun proteomics Large scale proteomics by orbitrap technology. Thermo fisher scientific K.K SID C&MS Application OMICS Team TMT 2 Proteome Cell and Tissue Protein Peptide Extraction Protease

要調査項目等調査マニュアル

PBDEs TriBDE DeBDE 1 TriBDE 8 TeBDE 6 PeBDE 8 HxBDE 7 HpBDE 5 OcBDE 3 NoBDE 2 DeBDE 40 GC/MS 1 1 1 ng/l µg/kg, dry µg/kg TriBDE 0.1 0.01 0.01 TeBDE 0.1 0.01 0.01 PeBDE 0.1 0.01 0.01 HxBDE 0.1 0.01 0.01

食糧　その科学と技術　No.46( )

, IARC A ppb ppm, WHOµg/L GC GC GCMS GC MS, d O O O NH 2 Br 2 NEt 3 Br NH 2 NH 2 Br Br GC, [C H NO Br] + m/z [C H NO Br] m/z SIM [C H D NO Br] m/z [C H D NO Br] + m/z Br Br HBr [C H NO Br] + m/z GC -d

untitled

ACQUITY UPLC SYNAPT TM G2 HDMS TM 130 2010/3/29 13:00-13:20 2010 Nihon Waters K.K. LC/MS Monoclonal Antibody Aspirin Insulin EPO MW 180 MW 6,000 MW 34,000 MW 147,000 2010 Nihon Waters K.K. 2 1 LC/MS ACQUITY

10 117 5 1 121841 4 15 12 7 27 12 6 31856 8 21 1983-2 - 321899 12 21656 2 45 9 2 131816 4 91812 11 20 1887 461971 11 3 2 161703 11 13 98 3 16201700-3 - 2 35 6 7 8 9 12 13 12 481973 12 2 571982 161703 11

LC LC ACQUITY UPLC H-Class ACQUITY UPLC CSH C mm 1.7 µm : THF/ 2/8 A 1 mm / 4/6 THF 2 mg/ml THF/ 2 THF 2 ACQUITY UPLC CSH C 18

ACQUITY UPLC H-Class/QDa Nihon Waters K.K., Tokyo, Japan TAG 1 3 1 1 8 9 TAG TAG TAG TAG TAG UV UV APCI ESI MS TAG Sn-2 Sn-3 Sn-1 C18: ACQUITY UPLC CSH C 18 ACQUITY UPLC H-Class 1. ACQUITY QDa TAG ACQUITY

0.45m1.00m 1.00m 1.00m 0.33m 0.33m 0.33m 0.45m 1.00m 2

24 11 10 24 12 10 30 1 0.45m1.00m 1.00m 1.00m 0.33m 0.33m 0.33m 0.45m 1.00m 2 23% 29% 71% 67% 6% 4% n=1525 n=1137 6% +6% -4% -2% 21% 30% 5% 35% 6% 6% 11% 40% 37% 36 172 166 371 213 226 177 54 382 704 216

1 Q A 82% 89% 88% 82% 88% 82%

ブラジル産ジョロウグモから単離された新規アシルポリアミンの構造決定

J. School Sci. Eng. Kinki Univ. 41 (2005) 23-29 Structural Determination of Novel Acylpolyamines from the Venom of Nephila clavipes, a Brazilian Joro spider Takahiro NISHIMARU*, Terumi NAKAJIMA * *, Yasuhiro

10 44 1.2 5 4 5 3 6-1 - 1 2 3 4 5 1 2 3 4 5 6 7 8 1 2 3 4 5 6 7 8 9 10 TEL TEL 1 2 TEL FAX TEL FAX TEL FAX 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 1 2 3 4 5 6 ( ) ( ) 2

１

10 2 1990 5 1993 6 16 11 24 18 35 1960 41 1966 19 2 11 14 30 1955 10 41 1966 12 16 45 40 35 2004 2004 2004 30 25 20 15 10 5 0 1950 1960 1970 1980 1990 2000 6 10 1 6 46 10 2223 2 6 10 6 10 1 6 7 8 1011

() 2

1 () 2 2 4 3 6,500 4 5 2 6 A B A B A B A B - A B 7 8 A B A B A B 9 JR JR 10 11 6 5 12 17 6 13 14 B A A B A B A B 2 1 8 15 8 16 17 9 18 3 4 5 mm mm 19 2 20 3 6 7 11 12 13 14 18 4 3 2 1 21 3 12 13 14 16

05 agon Inaba 149

05 Inaba Office System Unit Line Unit 148 Inaba 05 agon Inaba 149 05 agon 150 Inaba 05 agon Inaba 151 152 Inaba 05 agon agon CO2 CO2 CO2 CO2 1/3 CO2 Inaba 153 05 agon agon 05 agon Check P.164 720 1770

報告書

1 2 3 4 5 6 7 or 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 2.65 2.45 2.31 2.30 2.29 1.95 1.79 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 60 55 60 75 25 23 6064 65 60 1015

効率化計画冊子ﾌｧｲﾅﾙ.PDF

- 1 - - 2 - - 3 - - 4 - - 5 - - 6 - - 7 - - 8 - - 9 - - 10 - - 11 - - 12 - - 13 - - 14 - - 15 - - 16 - - 17 - (77kV) (6kV) (77kV6kV 6kV - 18-77kV 10%20% - 19 - - 20 - - 21 - - 22 - - 23 - - 24 - DB( )

平成26年度 化学物質分析法開発報告書

2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)

Jean Le Rond d Alembert, ( ) 2005

5 5.1 5.2 5.3 1700 Jean Le Rond d Alembert, (1717-1783) 2005 5. 1 123 5.1 5.2 124 5. 5.3 lumped mass modeling) 5. 1 5.4 x x A l ρ 5.4 5. 1 125 x 10 x y(x, t) y M(x, t) Q(x, t) E I 2 y/ 2 M = EI 2 y 2 (5.1)