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1 2006 [ No ]19-24 Charge and discharge cycle performance of negative electrode film of lithium ion battery made of natural graphite particles of different tapping densities Katsutomo Ohzeki", Yoshie Ohsaki*, Boris Golman** and Kunio Shinohara** The relationship was experimentally investigated between the cycle performance and the packing structure of a negative electrode film made of natural graphite particles of different tapping densities. At the same packing density of the electrode film, the modal voiddiameter and volumetric resistance increased with the tapping density of graphite powder. It was considered due to the fact that contact areas among particles of massive one were smaller than these of flaky one. Though the discharge capacity of the electrodes made of high tapping density powder rapidly decreased at low packing density, these cycle performances were satisfactorily improved with small irreversible capacity at high packing density. KEYWORDS: Lithium ion battery, Natural graphite, Packing structure, Cycle performance, Tappingdensity **Division ofchemical Process Engineering, Graduate School of Engineering, Hokkaido University: West 8, North 13, Kita-ku, Sapporo, Hokkaido , Japan
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3 [No ] Fig. 3 Relationship between tapping density and modal void diameter by mercury penetration method. Fig. 1 Hg intrusion curve for sample A and F. Fig. 2 Void size distribution by mercury penetration method. :ƒïb=1.2g/cm3, œ:ƒïh=1.8g/cm3
4 Fig. 4 Relationship between tapping density and specific surface area of void space by mercury penetration method. Fig. 6 Specific charge and discharge curves for sample A and F. (a) Sample A, ĕb=1.2g/cm3 (b) Sample A, ĕb=1.8g/cm3 (c) Sample F, ĕb=1.2g/cm3 (d) Sample F, ĕb=1.8g/cm3 : first cycle -: second cycle Fig. 5 Relationship between tapping density and film resistance. Fig. 7 Effect of packing density on irreversible capacity at 1st cycle. Fig. 8 Relationship between modal void diameter and irreversible capacity with different samples.
5 [No ] Fig. 9 Relationship between tapping density and increasing ratio of film thickness after 1st cycle. Fig. 10 Relationship between tapping density and packing density after 1st cycle in comparison with green film. Fig. 11 Effect of packing density on cycle performance. (a) ĕb=1.2g/cm3, (b) ĕb=1.5g/cm3, (c) ĕb=1.8g/cm3
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Size Effect of Biomass on Carbonization Rate Treated in Superheated Steam Combined with Far Infrared Heating Akiko ISA Yoshio HAGURA and Kanichi Kit Graduate School of Biosphere Science, Hiroshima University,
Authors' Abstract It in known that the method of feeding powder into split cell affects the adhesion forces of powder beds, especially in fine particle powders. But the effect of the agglomeration phenomenon
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