寄稿論文 有機合成から現代の錬金術へ | 東京化成工業
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- そうすけ やまがた
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1 FAMS MT FAMS S Formaldehyde Dimethyl Dithioacetal S-xide FAMS DMS α DMS SDMS
2 H 3 SH 3 S K 2 3 or Pyr. H 3 SH 2 l 3 Sa H 3 SH 2 S 4 Finkelstein FAMS FAMS FAMS FAMS H 2 2 H 2 + MeSH H+ H 2 1 (FAMS) 5 MT FAMS p p MT DMS p H 3 SH 3 Ac 2 [ H 3 SH 2 Ac ] 5 TolS 2 a 2 AcH (Aca) DMS p MT one-potmt
3 FAMS MT FAMS FAMS MT MT TMA MT FAMS MT
4 (H 2 ) n 1 2 H H 3 + ah 2 X hν 1 H H 2 (H 2 ) n 1 1 Me H H 2 2 SMe X 1 H H + /MeH ah (H 2 ) n 1 X ah X Ar ArH H H 2 2 H 2 abh 4 H + /MeH ArH 2 H Ar 1 H Me H 2 H BuLi/TMSl Me n n X ah 1 Si H H ArH 2 1 TolS X ah 1 3 TolS 2 H 2 MT X + H 2 2 TMA 50% ah-toluene 91-99% H H ah/dmf 'X rt / 0.5 h rt / h (50-60 / 3 h) ' H + /MeH reflux / 2-3 h ' H + : 4 Hl or H 2 S 4 PhH 2 Me n- 12 H 25 'X MeI n- 6 H 13 Br PhH 2 Br MeI 96 % 92 % 85 % 90 %
5 MTS,S S,S MT H K 2 3 /iprh H 2 2 H 2 X ah H 2BuLi/TMSl H 2 H 1) S 2 l 2 2) H 6 MT S,S α H 2 H H S 2 Me S,S p TolS 2 captodative Y Y H H 6 8
6 THF THF α THF α 6 hν Ph 2 'I ah ' 4 H 2 S 4 MeH ' =Ph, '=Me 85% aney i a-eth Me THF =Me 94% =Ph 98% =Ph 82% =Ph 80% S,S PS H H (Me) 2 Me 2 hν, Ph 2 PTS MeH 77% ()-(E)-9 81% H MeS (2S, 3) aney-i 90% hν (254 nm) ether-h 2 (19:1) 44% (Me) 2 Me 2 PTS H ah 3 75% H 1) a, a 2 HP 4, EtH, 2) PTS, MeH 81% H H H
7 S,S MPBA MPBA MPBA S 2 Me MPBA (2 equiv) MPBA S 2 Me S 2 Me 7 u or :uh S 2 Y u Y=Me or Tol u u α ω S 2 Me H '' or H 2 '' (A) Hl 3, rt H 2 '' '' '' '' or H H (A) α α
8 7 S 2 Me H 2 H 2 Hl 3, rt H H diamine (mol-equiv.) (h) (%) Et Ph S 2 Me H 2 H 2 Hl 3, rt H H H S 2 Me diamine (mol-equiv.) (h) (%) Et Ph π π π π MeS TolS 2 H S Ar 15 S H H + /ArH 2 S S S S 13 Ar 14 a: EWG H b: EWG H () c: EWG H () 2 S Ar S 16 EWG
9 π S,S EWG EL EL EWG S,S nm EWG ma EWG S,S EL DMF Y Y Y S S 17 (a) (b) (c) (a) 17 (Y=n-Pr) (b) 17 (Y=F) (c) 17 (Y= 14 H 29 )
10 THF λmaxnm ev nm π 17 (Y=F) p (a) (b) 17 (Y=Me) (a) (b)
11 p H H p p (a) (b) 17 (Y=n- 14 H 29 ) (a) (b) Y p Y S S 18
12 Y p (a) (c) (b) 17 (Y=H 3 ) πp π (a) Y (b) S (Y=H 3 ) 1) G. Tsuchihashi, K. gura, Bull. hem. Soc. Jpn. 1971, 44, ) K. gura, G. Tsuchihashi, J. hem. Soc., hem. ommun. 1970, ) K. gura, G. Tsuchihashi, Bull. hem. Soc. Jpn. 1972, 45, ) D. T. Gibson, J. hem. Soc. 1932, ) K. gura,. Yahata, J. Watanabe, K. Takahashi, H. Iida, Bull. hem. Soc. Jpn. 1983, 56, 3543.
13 6) Encyclopedia of eagent for rganic Synthesis, vol. 4, pp (Wiley, 1995). 7) Encyclopedia of eagent for rganic Synthesis, vol. 5, pp (Wiley, 1995). 8) K. gura, G. Tsuchihashi, Tetrahedron Lett. 1971, 12, ) K. gura and G. Tsuchihashi, Tetrahedron Lett. 1972, 13, ; K. gura, Y. Ito and G. Tsuchihashi, Bull. hem. Soc. Jpn. 1979, 52, ) K. gura, K. htsuki, M. akamura,. Yahata, K. Takahashi, H. Iida, Tetrahedron Lett. 1985, 26, ) K. gura, K. htsuki, K. Takahashi, H. Iida, hem. Lett. 1986, ) K. gura,. Sumitani, A. Kayano, H. Iguchi, M. Fujita, hem. Lett. 1992, ) K. gura, A. Yanagisawa, T. Fujino, K. Takahashi, Tetrahedron Lett. 1988, 29, ) K. gura, A. Kayano,. Sumitani, M. Akazome and M. Fujita, J. rg. hem. 1995, 60, ) A. Kayano, M. Akazome, M. Fujita, K. gura, Tetrahedron 1997, 53, ) K. gura, T. Arai, A. Kayano, M. Akazome, Phosphorus, Sulfur and Silicon 1999, , ) S. Matsumoto, M. Ishii, K. Kimura, K. gura, Bull. hem. Soc. Jpn. 2004, 77, ) Y. Sugiyama, Y. Suzuki, S. Mitamura, Y. Kawamoto, M. Fujita, K. gura, Bull. hem. Soc. Jpn. 1994, 67, ) K. gura, H. Yanai, M. Miokawa, M. Akazome, Tetrahedron Lett. 1999, 40, ) K. gura, M. Miokawa, M. Fujita, H. Ashidaka, A. Mito, onlinear ptics 1995, 13, ) H. Yanai, D. Yoshizawa, S. Tanaka, T. Fukuda, M. Akazome, K. gura, hemisty Lett. 2000, ) K. gura,. Zhao, H. Yanai, K. Maeda,. Tozawa, S. Matsumoto, M. Akazome, Bull. hem. Soc. Jpn. 2002, 75, ). Zhao, S. Matsumoto, M. Akazome, K. gura, Tetrahedron 2002, 58, ) K. gura,. Zhao, M. Jiang, M. Akazome, S. Matsumoto, K. Yamaguchi, Tetrahedron Lett. 2003, 44, ). Zhao, M. Akazome, S. Matsumoto, K. gura, Tetrahedron 2002, 58, (eceived ct. 2005) Katsuyuki gura BSJ SH 3 H 2 SH 3 SH 3 H 2 S 2 H 3
寄稿論文 ボロンアルドール反応の新展開 | 東京化成工業
substrate control reagent control Tf Tf amine H n-u Tf Et 3 3 n-u Tf Et syn Tf anti n Tf, Amine (1.3eq) (1.5eq) CH Cl, -78 C n n Z E CH -78 C, 1h; 0 C, 1h n H Triflate Et Tf n-u Tf c-pen Tf Tf Amine Yield
寄稿論文 新光延試薬 | 東京化成工業
DEAD TPP A Et C C Et Et C C Et 2 A A ex. ucleophiles (A) P 3 P 3 1 xygen itrogen Carbon Sulfur C 3 S Ts Tf Scheme 1. TPP DEAD TPP DEAD redox condensation Walden Bz Tf DEAD-TPP 87% Tf Bz Scheme 2. pk a
寄稿論文 規則性無機ナノ空間が創り出す新しい触媒能 | 東京化成工業
MCM-41 M41 MCM-41 M41 2 3 m 2 /g nm nm Mn Ti Ti H N 2 S Ti-MCM-41, H H N H H 2 2 -Urea, CH 2 Cl 2, H 2 S + S 1b 2b 3b 54%, 58% ee Ti M41 H 2 As 4 ZP 4 ZP ZS ZS 5 Me Me Me Me M41 / 15 mg MeH 1.0 mmol 89%
a b b c a c Ally anion type Propargyl/allenyl anion type a b c a b c a b c a b c a b c a b c b =,, or C a b c a b c b = Gothelf, K. V.; Jørgensen, K.
1 a b b c a c Ally anion type Propargyl/allenyl anion type a b c a b c a b c a b c a b c a b c b =,, or C a b c a b c b = Gothelf, K. V.; Jørgensen, K. A. Chem. ev. 1998, 98, 863-909 2 itrogen in the middle
Activation and Control of Electron-Transfer Reactions by Noncovalent Bond
2 + 4e- + 4 + hν 2 2 1 2 20 J. Am. Chem. oc. Angew. Chem. Int. Ed. umber of Papers 15 10 5 0 1998 1999 2000 2001 2002 2003 Year : J. Am. Chem. oc. (Trost, B. M.; tanford University, UA) 3 π 1/2 k ET =
a L = Ψ éiγ c pa qaa mc ù êë ( - )- úû Ψ 1 Ψ 4 γ a a 0, 1,, 3 {γ a, γ b } η ab æi O ö æo ö β, σ = ço I α = è - ø çèσ O ø γ 0 x iβ γ i x iβα i
解説 4 matsuo.mamoru jaea.go.jp 4 eizi imr.tohoku.ac.jp 4 maekawa.sadamichi jaea.go.jp i ii iii i Gd Tb Dy g khz Pt ii iii Keywords vierbein 3 dreibein 4 vielbein torsion JST-ERATO 1 017 1. 1..1 a L = Ψ
p = mv p x > h/4π λ = h p m v Ψ 2 Ψ
II p = mv p x > h/4π λ = h p m v Ψ 2 Ψ Ψ Ψ 2 0 x P'(x) m d 2 x = mω 2 x = kx = F(x) dt 2 x = cos(ωt + φ) mω 2 = k ω = m k v = dx = -ωsin(ωt + φ) dt = d 2 x dt 2 0 y v θ P(x,y) θ = ωt + φ ν = ω [Hz] 2π
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... black body radiation black body black body radiation Gustav Kirchhoff 859 895 W. Wien O.R. Lummer cavity radiation ν ν +dν f T (ν) f T (ν)dν = 8πν2 c 3 kt dν (Rayleigh Jeans) (.) f T (ν) spectral energy
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. 4cm 6 cm 4cm cm 8 cm λ()=a [kg/m] A 4cm A 4cm cm h h Y a G.38h a b () y = h.38h G b h X () S() = π() a,b, h,π V = ρ M = ρv G = M h S() 3 d a,b, h 4 G = 5 h a b a b = 6 ω() s v m θ() m v () θ() ω() dθ()
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3 From Evans Application Notes http://www.eaglabs.com From Evans Application Notes http://www.eaglabs.com XPS AES ISS SSIMS ATR-IR 1-10keV µ 1 V() r = kx 2 = 2π µν x mm 1 2 µ= m + m 1 2 1 k ν = OSC 2
寄稿論文 オキシム誘導体を用いる新しいC-N結合生成法 | 東京化成工業
Gabriel Beckmann sp 2 displacement Beckmann earrangement of ximes 2 S 4 2 ' ' ' Displacement on itrogen Atom of ximes Y u Y u S 2 n-bu 4 e 4 p 33% 10 mol% (n-bu) 4 e 4 5 mol% Ts 2 C 2 Cl 2, rt, 5 min e
) a + b = i + 6 b c = 6i j ) a = 0 b = c = 0 ) â = i + j 0 ˆb = 4) a b = b c = j + ) cos α = cos β = 6) a ˆb = b ĉ = 0 7) a b = 6i j b c = i + 6j + 8)
4 4 ) a + b = i + 6 b c = 6i j ) a = 0 b = c = 0 ) â = i + j 0 ˆb = 4) a b = b c = j + ) cos α = cos β = 6) a ˆb = b ĉ = 0 7) a b = 6i j b c = i + 6j + 8) a b a b = 6i j 4 b c b c 9) a b = 4 a b) c = 7
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64 3 g=9.85 m/s 2 g=9.791 m/s 2 36, km ( ) 1 () 2 () m/s : : a) b) kg/m kg/m k
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平成27年度三菱重工グループ保険 フルガードくん（シニア）
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