PERRY JOHNSON LABORATORY

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1 PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: Kobe Quarantine Station, Ministry of Health, Labour and Welfare 1-1 Toyahamacho Hyogo-ku Kobe-shi, Hyogo (Hereinafter called the Organization) and hereby declares that Organization is accredited in accordance with the recognized International Standard: ISO/IEC 17025:2005 This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (as outlined by the joint ISO-ILAC-IAF Communiqué dated January 2009): Analytical test of 5 items of sulfa drugs in chicken and shrimp using LC/MS/MS based on methods for simultaneous analysis of veterinary drugs, Identification inspection of Enterohaemorrhagic Escherichia coli in general foods using PCR and turbidity measuring device, Analytical test of pesticide residues (Isazophos and other four items) in agricultural produce using GC/MS/MS, Analytical test of cadmium and the chemical compound, and lead in rice using inductively coupled plasma atomic emission spectroscopy, detection of Insectresistance recombinant gene in rice using PCR (As detailed in the supplement) Accreditation claims for such testing and/or calibration services shall only be made from addresses referenced within this certificate. This Accreditation is granted subject to the system rules governing the Accreditation referred to above, and the Organization hereby covenants with the Accreditation body s duty to observe and comply with the said rules. For PJLA: Initial Accreditation Date: Issue Date: Expiration Date: February 14, 2014 February 23, 2016 April 30, 2018 Tracy Szerszen President/Operations Manager Perry Johnson Laboratory Accreditation, Inc. (PJLA) 755 W. Big Beaver, Suite 1325 Troy, Michigan Revision Date: Accreditation No.: Certificate No.: March 9, L16-61-R1 The validity of this certificate is maintained through ongoing assessments based on a continuous accreditation cycle. The validity of this certificate should be confirmed through the PJLA website: Page 1 of 3

2 Certificate of Accreditation: Supplement Kobe Quarantine Station, Ministry of Health, Labour and Welfare 1-1 Toyahamacho Hyogo-ku Kobe-shi, Hyogo Shunro Imura Phone: Accreditation is granted to the facility to perform the following testing: FIELD OF TEST Chemical F ITEMS, MATERIALS OR PRODUCTS TESTED Chicken Shrimp Vegetables Rice SPECIFIC TESTS OR PROPERTIES MEASURED Residual veterinary drugs Sulfadimidine (SDD) Sulfamerazine (SMR) Sulfamonomethoxine (SMM) Sulfadimethoxine (SDM) Sulfaquinoxaline (SQX) Pesticide residues Isazophos Isoprocarb Cyanophos Dichlofenthion Pyrimethanil Metal Cadmium and the chemical compound (As Cadmium) SPECIFICATION, STANDARD METHOD OR TECHNIQUE USED LC/MS/MS Simultaneous Analysis of Veterinary Drugs I-1 (Livestock and Marine Products) KCC/MT/138 Test method provided in Notification No , Ministry of Health, Labour and Welfare (January 24, 2005) GC/MS/MS Simultaneous Analysis of Pesticide Residues by GC/MS (Agricultural Produce) KCC/MT/291 Test method provided in Notification No , Ministry of Health, Labour and Welfare (January 24, 2005) Inductively coupled plasma atomic emission spectroscopy (ICP) Heavy metals in rice(cd and Pb) KCC/MT/053 RANGE (WHERE APPROPRIATE) AND DETECTION LIMIT SDD, SMR, SMM, SDM, SQX Quantitation Limit(Q.L.): 0.01 mg/kg (ppm) Quantitation Limit(Q.L.): 0.01 mg/kg (ppm) Maximum Level: 0.4 mg/kg (ppm) Lead Test method which changed a part of Specifications and Standards for foods and food additives, etc. (Ministry of Health, Labour and Welfare Notification No.370, 1959) and confirmed the validity Codex standard: 0.2 mg/kg (ppm) Issue: 2/2016 This supplement is in conjunction with certificate #L16-61-R1 Page 2 of 3

3 FIELD OF TEST ITEMS, MATERIALS OR PRODUCTS TESTED Certificate of Accreditation: Supplement Kobe Quarantine Station, Ministry of Health, Labour and Welfare 1-1 Toyahamacho Hyogo-ku Kobe-shi, Hyogo Shunro Imura Phone: Accreditation is granted to the facility to perform the following testing: SPECIFIC TESTS OR PROPERTIES MEASURED Biological F General foods Pathogenic microbe Enterohemorrhagic Escherichia coli O26, O103, O111, O121, O145 and O157 SPECIFICATION, STANDARD METHOD OR TECHNIQUE USED Real time PCR device Real time turbidity measuring device Inspection method of Enterohemorrhagic Escherichia coli O26, O103, O111, O121, O145 and O157 KCB/MT/072 Notification No.1120 Article 3, Ministry of Health, Labour and Welfare (November 20, 2014) RANGE (WHERE APPROPRIATE) AND DETECTION LIMIT Positive/Negative Rice Insect-resistance recombinant gene 63Bt, NNBt, CpTI Real time PCR device Detection of Insect-resistance recombinant gene rice DNA (63Bt, NNBt, CpTI) KCB/MT/417 Test method provided in Notification No.1116 Article 4, Ministry of Health, Labour and Welfare (November 16, 2012) 1. The presence of a superscript F means that the laboratory performs testing of the indicated parameter at its fixed location. Example: Outside Micrometer F would mean that the laboratory performs this testing at its fixed location. Issue: 2/2016 This supplement is in conjunction with certificate #L16-61-R1 Page 3 of 3

4 ペリージョンソンラボラトリーアクレディテーションインク 認定証 ペリージョンソンラボラトリーアクレディテーションインクは 下記の試験所を審査しました 厚生労働省神戸検疫所 兵庫県神戸市兵庫区遠矢浜町 1 番 1 号 ここに本組織が 以下の認知された国際規格に基づき 認定されたことを証します ISO/IEC 17025:2005 本認定により 以下の範囲及び試験所品質マネジメントシステムの運営における技術的能力を実証するものとします (2009 年 1 月発行 ISO-ILAC-IAF 共同コミュニケに準ずる ) 動物用医薬品等の一斉分析法に基づく鶏肉及びえびの LC/MS/MS を用いたサルファ剤 5 種分析試験 PCR 及び濁度測定器を用いた一般食品の腸管出血性大腸菌の同定検査 GC/MS/MS を用いた農産物の残留農薬 ( イサゾホス他 4 種 ) 分析試験 誘導結合プラズマ発光分光分析計を用いた米中のカドミウム及びその化合物 鉛の分析試験 PCR を用いた米中の害虫抵抗性組換え遺伝子の検知検査 ( 詳細は付属書に記述 ) 上記試験及び / 又は校正サービスに対する認定資格は本認定証内で言及された住所のみを対象とする 本認定は 上記規格の認定を管理するシステム規定に従い授与され 組織はその規定を遵守し 認定機関の任務を尊重することをここに誓約する PJLA 初回認定日 発行日 認定証有効期限 2014 年 2 月 14 日 2016 年 2 月 23 日 2018 年 4 月 30 日 改訂日認定番号認定証番号 トレーシーサーツェンプレジデント / オペレーションマネージャー Perry Johnson Laboratory Accreditation, Inc. (PJLA) 755 W. Big Beaver Rd., Suite 1325 Troy, Michigan 年 3 月 9 日 L16-61-R1 この認定証の有効性は 持続された認定に基づく継続審査を通して維持されています PJLA ウェブサイト ( でご確認いただけます 尚 本認定証は日本語翻訳版であり 英文の認定証を正式のものとする 1/3 頁

5 認定証付属書 厚生労働省神戸検疫所 兵庫県神戸市兵庫区遠矢浜町 1 番 1 号井村俊郎 Tel: 本認定を 上記組織の実施する下記試験について授与する 試験分野 試験された 試験の内容または 適用された仕様 範囲および 化学的試験 F 品目 材料 製品鶏肉えび 測定された属性残留動物用医薬品スルファジミジン (SDD) スルファメラジン (SMR) スルファモノメトキシン (SMM) スルファジメトキシン (SDM) スルファキノキサリン (SQX) 規格に規定された方法または手法 LC/MS/MS 厚生労働省通知 ( 平成 17 年 1 月 24 日食安発第 号 ) に規定する試験法に基づく動物用医薬品等の一斉分析 Ⅰ-1( 畜水産物 ) 検査実施標準作業書 KCC/MT/138 検出限界 SDD, SMR, SMM SDM, SQX 定量下限 0.01 mg / kg (ppm) 野菜 残留農薬イサゾホスイソプロカルブシアノホスジクロフェンチオンピリメタニル GC/MS/MS 厚生労働省通知 ( 平成 17 年 1 月 24 日食安発第 号 ) に規定する試験法に基づく GC/MS による農薬等の一斉試験法 ( 農産物 ) 検査実施標準作業書 KCC/MT/291 定量下限 0.01 mg / kg (ppm) 米 重金属カドミウム及びその化合物 ( カドミウムとして ) 鉛 誘導結合プラズマ発光分光分析計 (ICP) 食品 添加物等の規格基準 ( 昭和 34 年厚生省告示第 370 号 ) を一部変更し 妥当性を確認した試験法に基づく米の重金属 (Cd 及び Pb) 検査実施標準作業書 KCC/MT/053 基準値 0.4 ppm コーデックス基準値 0.2 ppm 2016 年 2 月発行本付属書は 認定証番号 L16-61-R1 の認定証を補足するものである 2/3 頁

6 認定証付属書 厚生労働省神戸検疫所 兵庫県神戸市兵庫区遠矢浜町 1 番 1 号井村俊郎 Tel: 本認定を 上記組織の実施する下記試験について授与する 試験分野 試験された 試験の内容または 適用された仕様 範囲および 生物的試験 F 品目 材料 製品食品一般 測定された属性病原微生物腸管出血性大腸菌 O26 O103 O111 O121 O145 及び O157 規格に規定された方法または手法リアルタイム PCR 装置リアルタイム濁度測定装置厚生労働省通知 ( 平成 26 年 11 月 20 日食安監発第 1120 第 3 号 ) に基づく腸管出血性大腸菌 O26 O103 O111 O121 O145 及び O157 検査実施標準作業書 KCB/MT/072 検出限界陰性 陽性 米 害虫抵抗性組換え遺伝子 63Bt,NNBt,CpTI リアルタイム PCR 装置厚生労働省通知 ( 平成 24 年 11 月 16 日食安発 1116 第 4 号 ) に規定する試験法に基づく害虫抵抗性遺伝子組換えコメ DNA(63Bt,NNBt,CpTI) の検知検査実施標準作業書 KCB/MT/ 上付き文字 F は 試験所が固定された位置で示されたパラメータの試験を実行することを意味している ( 例 : Outside Micrometer F は 試験所が固定された位置でこの試験を行うことを明確にしている ) 2016 年 2 月発行本付属書は 認定証番号 L16-61-R1 の認定証を補足するものである 3/3 頁

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