2 Michael Kiselewsky Product Manager Analytical Reagents L-MS G-MS UPL L-NMR G sigma-aldrich.com/ gc-hs With kind regards, L-MS MS Dr. Michael Kiselew
|
|
|
- よしたか いまいだ
- 5 years ago
- Views:
Transcription
1 Analytix Issue , Issue G-HS TraceERT
2 2 Michael Kiselewsky Product Manager Analytical Reagents L-MS G-MS UPL L-NMR G sigma-aldrich.com/ gc-hs With kind regards, L-MS MS Dr. Michael Kiselewsky Product Manager Analytical Reagents michael.kiselewsky@sial.com Analytix is published five times per year by Sigma-Aldrich hemie GmbH, Marom Europe, Industriestrasse 25, H-9471 Buchs SG, Switzerland Publisher: Sigma-Aldrich Marketing ommunications Europe Publication director: Ingo Haag, PhD Editor: Daniel Vogler sigma-aldrich.com/analytix
3 3 4 G Ph.Eur, USPIH G 6 Analytix 8 G-MS 10 A 14 AAS IPI TraceERT 16 L-MS L-MS 18 H 2 H 2 Sensoric 21 Titration sigma-aldrich.com/analytix
4 4 G G-SH G-SH Ph.Eur. USP Ph.Eur. USP 0.2 μm USPPh.Eur. IH G-SH [1-3] G-SH [4,5] Figure 1 G-HS Ph.Eur.USP IH G-SH DMSN,N- N,N-N,N- N,N G [6] IH 61 Supelco VI-G43 61 Supelco G VI-G43 USP 467 Ph.Eur. USP 5 m VI-G43 at. G Ph.Eur, USP IH G Katherine K. Stenerson, Application hemist Gas Separations katherine.stenerson@sial.com Michael Jeitziner, Market Segment Manager Analytical Reagents & Standards michael.jeitziner@sial.com Figure 1 DMS G-HS [2] 50'000 uv 40'000 30'000 20'000 10' '000 min sigma-aldrich.com/gc-hs
5 5 Figure 2 -G VI-G43 G ven: 35, hold 15 min., 5 /min to 200 Inj.: 225 Det.: FID, 250 Flow: 30 cm/sec (constant) He at 35 Inject.: 1 μl, 33:1 split Liner: single taper Sample: lass II, III: ppm In DMS lass 2 Solvents on VI-G43 olumn: 30 m x 0.53 mm ID x 3.0 μm w/5 m intermediate polarity guard at. No.: lass 3 Solvents on VI-G43 olumn: 30 m x 0.53 mm ID x 3.0 μm w/5 m intermediate polarity guard at. No.: G G lass 2 Solvents on VI-G43 Peak # Identification 1 Methanol 2 Acetonitrile 3 Methylene chloride 4 Nitromethane 5 Hexane 6 cis-1,2-dichloroethylene 7 hloroform 8 2-Methoxyethanol 9 1,2-Dimethoxyethane 10 yclohexane 11 Ethylene glycol 12 Formamide Trichloroethylene 14 1,4-Dioxane 15 2-Ethoxyethanol 16 Methylcyclohexane 17 Pyridine 18 Toluene 19 Dimethylformamide 20 Methyl butyl ketone 21 hlorobenzene 22 Dimethylacetamide 23 m-xylene 24 p-xylene 25 o-xylene 26 n-methylpyrrolidone 27 Tetralin 28 Sulpholane lass 3 Solvents on VI-G43 Peak # Identification 1 Ethanol 2 Acetone 3 2-Propanol 4 Pentane 5 Ethyl ether 6 Ethyl formate 7 Methyl acetate 8 1-Propanol 9 Methyl-t-butyl ether 10 Acetic acid 11 2-Butanone 12 sec-butanol Ethyl acetate 14 Tetrahydrofuran 15 iso-butanol 16 n-butanol 17 Isopropyl acetate 18 Heptane 19 Propyl acetate 20 Isoamyl alcohol 21 4-Methyl-2-pentanone 22 n-amyl alcohol 23 Isobutyl acetate 24 Butyl acetate 25 Dimethyl sulphoxide 2 26 Anisole 27 umene No Supelco Technical Bullentin 933 (sigma-aldrich.com/supelco) References 1. United States Pharmacopeia, 31st Edition (2008), <467> Residual Solvents. 2. Ph.Eur. 6.0 (2008) Method , Identification and control of residual solvents. 3. IH Guideline Q3, Impurities: Guideline for Residual Solvents, The Fourth International onference on Harmonization, July 17, amarasu,.. Residual Solvents Determination in Drug Products by Static Headspace-Gas hromatography. hromatographia 2002, 56, S7 S Lee,. R.; Nguyen van Dau,.; Krstulović, A. M. Artefact formation in the determination of residual solvents according to a method of the European Pharmacopeia. Int. J. Pharm. 2000, 195, Supelco Technical Bulletin 933. apillary G olumn hoices for Residual Solvent Analyses Using Direct Injection or Solid Phase Microextraction (SPME). Table 1 G-HS at. No L Fluka N,N-Dimethylacetamide, puriss. p.a. for G-HS L L Fluka Dimethyl sulphoxide, puriss. p.a. for G-HS L L Fluka N,N-Dimethylformamide, puriss. p.a. for G-HS L NEW L Fluka 1,3-Dimethyl-2-imidazolidinone puriss. p.a., for G-HS L L Fluka Water, puriss. p.a. for G-HS L Table 2 at. No Supelco lass 1 Mix DMS 25 x 2.5 ml Supelco lass 2 Mix DMS 25 x 2.5 ml Fluka Ph Eur 5.0 G alibration Solution for Residual Solvents in DMS 2 ml U Supelco USP 467 Mix 1 ml U Supelco USP 467 VI Mix 1, 24th ed. DMS 1 ml 4M4626-U Supelco USP 467VI Mix 2 DMS 5 x 1 ml U Supelco USP 467VI Mix 2, 24th ed. DMS 1 ml sialjpsp@sial.com Table 3 G at. No Supelco VI-G43, L I.D. 30m 0.53mm, df 3.00 μm 1 each Supelco VI-G43, L I.D. 5m 0.53 mm 1 each sigma-aldrich.com/gc-hs
6 6 [1] Discovery Ascentis HILI 5 ml Fluka at. No ml 100 mm, ph 2.51 ml rpm 10 SPE Supelco Discovery DS-SX 500 mg / 6 ml SPE at. No U SPE3 ml 3 ml 100 mm ph ml SPE 3 ml 100 mm, ph 3 3 ml 4 ml 5 % 505 psi 1 ml L A L-MS-MS Figure 1 pka 5.6 Log P [2] ANP ANP ANP HILI HILI ANP Supelco Ascentis Express HILI at. No U HILI HILI log P HILI ABI/MDS Sciex 3200 Q Trap MS/MS 2 MRM 127/85 MRM Analytix lga Shimelis, Sr. Research & Development olga.shimelis@sial.com armen T. Santasania, Sr. Applications hemist carmen.santasania@sial.com Q1 Q3 Declustering potential (DP) Entrance potential (EP) ollision energy (E) ollision cell exit potential (XP) ther instrument parameters were as follows: urtain Gas: 20 Ion Spray Voltage: 5000 Gas 1: 20 Temperature: 350 Gas 2: 40 Quantitation An external calibration curve was used for melamine. External calibration standards were prepared in the mobile phase. No matrixmatched standards were used. sigma-aldrich.com/standards
7 7 Figure 1 % n=3 10 ng/ml 71 a ng/ml ng/ml ng/ml 83 2 a 2.4 ng/ml 1000 ng/ml ng/ ml 94 % L/MS/MS 100 ng/ml 105 ng/ml 1 127/68 127/85 Supelco Discovery DS-SX SPE 10 ng/ml 500 ng/ ml Ascentis Express HILI HPL HILI HILI MS References: 1. Spears, L.; Lawrence, D. hina Milk Scandal Widens as Melamine Found in Yogurt. Bloomberg [nline] 2008, updated Sept 16, apps/news?pid= &sid=apye0jvtlhqa&refer=ho me (accessed Nov 7, 2008). 2. AD/ LogP DB, version 11.01, Advanced hemistry Development, Inc., Toronto N, anada, Figure 1 Figure ng/ml L-MS-MS H 2 N N NH 2 N NH 2 N 1 sigma-aldrich.com/standards Time (min) L-MS-MS onditions: Instrument: Agilent 1100 HPL system with ABI/MDS Sciex 3200 Q Trap MS/MS olumn: Ascentis Express HILI, 10 cm x 2.1 mm I.D., 2.7 µm particles Mobile Phase A: 10 mm ammonium formate in 90:10 acetonitrile:water Mobile Phase B: 10 mm ammonium formate in 70:30 acetonitrile:water Table Time (min) Gradient: Time Flow %A %B µl/min µl/min µl/min µl/min Temperature: 30 Flow Rate: as above Injection Volume: 2 μl Sample: 100 ng/ml of melamine from milk Detection: MS-MS with MRM at 127 -> 85 and 127 -> 68 at. No U Supelco Discovery DS-SX SPE Tube, 500 mg/6ml, pk of U Supelco Ascentis Express HILI HPL olumn, 2.7 μm particle size, 10 cm 2.1 mm I.D MG Fluka Melamine, 99 % 250 mg MG Fluka yanuric acid, 98 % 250 mg
8 8 A T-2 HT-2 Figure 1 Andreas Breidbach [1] Wolfgang Brodacz [2,3,4] T-2 HT-2 G-MS 2 5 ppb 24 T-2 22 HT-2 Fluka Figure 1 T-2HT-2 H 3 H 3 H 3 H 3 IDMS IDMS H H 3 H R H T-2 Toxin: R = Ac HT-2 Toxin: R = H G-MS Matthias Nold, Product Manager Analytical Standards matthias.nold@sial.com Figure 2 T-2 HT-2 T-2HT-2TMS-EI- Abundance m/z--> 105 Abundance #962: HT-2 Toxin -TMS 245 HT-2 Toxin (TMS) Q1 347 M=568 (not visible) (H 3 ) 2 H H 2 H H m/z--> #963: T-2 Toxin -TMS T-2 Toxin (TMS) 244 Q2 290 Q (H 3 ) T M=538 (not visible) Q2 (H 3 ) 2 H H 2 H T 436 Abundance m/z--> #968: 22-HT-2 Toxin (voll isotopenmarkiertes HT-2 Toxin) als TMS HT-2 Toxin (TMS) M=590 (not visible) (H 3 ) 2 H H 2 H Abundance Q1 #967: 24-T-2 Toxin als TMS (voll -isotopenmarkiertes T-2 Toxin) 24 -T-2 Toxin (TMS) 367 T T M=562 (H 3 ) 2 H H 2 H (H 3 ) m/z--> (not visible) Q1 sigma-aldrich.com/standards
9 9 G-MS G 35% 65% T-2 HT-2 SIM MS HT-2 T ppb EU 96/23/EG SIM qualifierfigure HT-2 Toxin T-2 Toxin Figure 2 MSTFA G 1 % N- -N- MSTFA MSTFA 1G Figure 3 SIM T= 1. Qualifier Q1= 2. Qualifier Q2= HT mg/kg T=466 Q1=347 Q2=478T mg/ kg T=436 Q1=350 Q2= HT-2 T=483 Q1= T-2 T=365 Q1= HT-2 Toxin 24 - T-2 Toxin IDMS Table References: 1. Breidbach, A.; Povilaityte, V.; Mischke,.; Doncheva, I.; Stroka, J; T-2 and HT-2 by G/MS for official food control a validated method ; Poster anl. 29. Mykotoxin-Workshop Fellbach, Germany. 2. Brodacz, W. Isotopenverdünnungsanalytik von Mykotoxinen mit G/MSD. LaborPraxis. 2007, 9, Brodacz, W. Entwicklung optimierter G-Trennungen in der Mykotoxinanalytik. LaborPraxis. 2004, 6, Brodacz, W. Stabilisotopenverdünnungs-G/MS: Hochtoxischen Mykotoxinen auf der Spur. hemiereport. 2008, 1, Acknowledgements: This article was developed in cooperation with Wolfgang Brodacz of the Austrian Agency for Health and Food Safety (AGES) in Linz, Austria. at. No ML-F Fluka MSTFA (N-Methyl-N-(trimethylsilyl) trifluoroacetamide) with 1% trimethylchlorosilane 5 ml ML Fluka T-2 Toxin- 24 EKANAL, 25 μg/ml 1 ml ML Fluka HT-2 Toxin- 22 EKANAL, 25 μg/ml 1 ml sigma-aldrich.com/standards Table 2 at. No ML Fluka Deoxynivalenol- 15 EKANAL, 25 μg/ml 1 ml ML Fluka Fumonisin B1-34 EKANAL, 25 μg/ml 1 ml ML Fluka chratoxin A- 20 EKANAL, 25 μg/ml 1 ml
10 10Analytix Issue 4, Water Framework Directive 2000/ 60/E SPAR onvention for the Protection of the Marine Environment Figure G-MS [1,2] G/MS A IS German Institute for Standardisation DIN IS IS/D [3] IS/D A laf P. Heemken, Member of Working Group DIN NA Phenols with G olaf.heemken@hanse-analytics.de Ernst Stottmeister, onvener of Working Groups IS T 147/S 2/ WG 17 Phenols and DIN NA Phenols with G ernst.stottmeister@uba.de Figure 1 Abundance P NP P1E NP1E P2E BPA Target Analyte Mix NP2E P2E NP2E P- 6 P1E NP1E- 6 BPA-D 16 Internal Standard Mix 363NP Time min > sigma-aldrich.com/standards
11 11 IS 5725 [4] μg/l 2 1 L μg/l ml 1 ph 2 2 Table MSTFA 6 References [3] Bad Elster, Germany Table 1 V R V r IS/D A IS/D IS/D sigma-aldrich.com/standards Figure 2 H H H P [ 6 ] P1E [ 6 ] P2E [ 6 ] H H H 363NP [ 6 ] 363NP1E [ 6 ] 363NP2E [ 6 ] (continued on page 12)
12 12 Matrix ompound No. of labs. * Table 1 P NP 1,2 EA BPAIS/D spiked surface water [ng/l] Results used* utliers [%] Total mean** Assigned value** Recovery [%] P P 1 E P 2 E NP NP 1 E NP 2 E BPA V R [%] V r [%] Table 2 G-MS L-MS/MS References 1] Loos, R.; Wollgast, J.; astro-jimenez, J.; et al., TrA Trends in Analytical hemistry 2008, 27 (1), ] Sobiecka, E.; Van der Sloot, H.; Hansen, N.; Gawlik, B. M., Project HRIZNTAL Validation Report, ffice for fficial Publications of the European ommunities, Luxembourg 2007, ISBN ] International Standardisation rganisation, IS/D , ] International Standardisation rganisation, IS/D , spiked waste water [µg/l] P P 1 E P 2 E NP NP 1 E NP 2 E BPA * without outliers ** all mass concentrations in ng/l (surface water) or µg/l (waste water) Table 2 at. no. Package size at. no. 4-tert-octylphenol (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-tert-octylphenol monoethoxylate (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-tert-octylphenol diethoxylate (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-(3,6-dimethyl-3-heptyl)-phenol (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-(3,6-dimethyl-3-heptyl)-phenol monoethoxylate (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-(3,6-dimethyl-3-heptyl)-phenol diethoxylate (Ring 6 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-tert-octylphenol (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-tert-octylphenol monoethoxylate (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-tert-octylphenol diethoxylate (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-(3,6-dimethyl-3-heptyl)-phenol (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML 4-(3,6-dimethyl-3-heptyl)-phenol monoethoxylate (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/mll ML 4-(3,6-dimethyl-3-heptyl)-phenol diethoxylate (Ring D 2 ) 1 ml / 10 μg/ml ML 10 ml / 1 μg/ml ML Target analyte mix according to IS/D ml / 1 μg/ml ML mix according to IS/D ml / 1 μg/ml ML sigma-aldrich.com/standards
13 Analytix Issue 3, /36/E EFSA B EFSA Annex 1 B Annex 2 IAR NTP sigma-aldrich.com/standards Ingrid Hayenga, Senior hemist R&D Europe ingrid.hayenga@sial.com Table 1 at. No. Purity MG Fluka Rhodamine B > 97 % 25 mg MG Fluka Para Red > 97 % 100 mg MG Fluka range II > 98 % 25 mg MG Fluka Acid Red > 97 % 25 mg MG Fluka Metanil Yellow > 98 % 100 mg MG Fluka ongo Red > 97 % 25 mg MG Fluka Butter Yellow > 98 % 25 mg MG Fluka Solvent Red I > 96 % 25 mg MG Fluka Naphtol Yellow S 25 mg MG Fluka Leucomalachite Green > 98 % 25 mg MG Fluka Ponceau MX > 96 % 25 mg Annex 1 Annex 2 N N N N N Na S N N H N N N l S Na H Acid Red 73 Sodium salt Butter Yellow Leucomalachite Green Rhodamine B Na S N 2 N N N N N H Para Red N H Metanil Yellow N N H Solvent Red I N N H S Na S N N H range II Sodium salt NH 2 N N S Na S N N ongo Red Na 2 N H Na Ponceau MX H S xh 2 NH 2 S Na N Napthol Yellow
![14 TraceERT IS 17025IS Guide 34 [1,2] TraceERT 2 NIST BAM SI unit kg IP 4 IP 70 AAS IP I TraceERT Matthias Nold, Product Manager Analytical Standards matthias.nold@sial.](/docs-images/91/105462507/images/14-0.jpg "com Jürg Wüthrich, Senior Scientist R&D Europe juerg.wuethrich@sial.com AAS IP 30 15 Table 1 IP Table 2 I Table 3 TraceERT sigma-aldrich.com/tracecert Table 1 Fluka TraceERT AAS IP 1000 mg/l at. No.")
14 14 TraceERT IS 17025IS Guide 34 [1,2] TraceERT 2 NIST BAM SI unit kg IP 4 IP 70 AAS IP I TraceERT Matthias Nold, Product Manager Analytical Standards matthias.nold@sial.com Jürg Wüthrich, Senior Scientist R&D Europe juerg.wuethrich@sial.com AAS IP Table 1 IP Table 2 I Table 3 TraceERT sigma-aldrich.com/tracecert Table 1 Fluka TraceERT AAS IP 1000 mg/l at. No. AAS at. No. IP ML Antimony 250 ml ML Antimony 100 ml ML Beryllium 250 ml ML Beryllium 100 ml ML Bismuth 250 ml ML Bismuth 100 ml ML erium 250 ml ML erium 100 ml ML esium 250 ml ML esium 100 ml ML Gallium 100 ml ML Gallium 100 ml ML Indium 100 ml ML Indium 100 ml ML Lithium 250 ml ML Lithium 100 ml ML Molybdenum 250 ml ML Molybdenum 100 ml ML Palladium 100 ml ML Palladium 100 ml ML Platinum 100 ml ML Platinum 100 ml ML Rhodium 100 ml ML Rhodium 100 ml ML Rubidium 100 ml ML Rubidium 100 ml ML Silicon 250 ml ML Silicon 100 ml ML Vanadium 250 ml ML Vanadium 100 ml sigma-aldrich.com/standards
15 15 Table 2 Fluka TraceERT at. No. IP ML ML ML ML 10 % Ag, Ba, a, d, o, u, Fe, Mg, Mn, Sr, Zn: 10 mg/l Al, B, r, Li, Mo, Na, Ni, Tl: 50 mg/l Bi, K, Pb: 100 mg/l III 5 % K: 200 mg/l Mg: 400 mg/l Na: 1000 mg/l a: 2000 mg/l IV 10 % Be, d, o, Mn: 10 mg/l r, u, Ni: 20 mg/l Al, As, Ba, Pb, V: 40 mg/l B, Fe, Se, Tl, Zn: 100 mg/l V 10 % Ag, Al, Ba, Be, Bi, d, o, r, s, u, Ga, In, Li, Mg, Mn, Mo, Ni, Pb, Rb, Sr, Tl, V, Zn: 10mg/L a, Fe, a, Na: 100 mg/l Table 3 Fluka TraceERT at. No ML Bromide (Br - ) 1000 mg/ml 100 ml ML hloride (l - ) 1000 mg/ml 100 ml ML hromate (r 4 2- ) 1000 mg/ml 100 ml ML Fluoride (F - ) 1000 mg/ml 100 ml ML Iodide (I - ) 1000 mg/ml 100 ml ML Nitrate (N 3- ) 1000 mg/ml 100 ml ML Nitrite (N 2- ) 1000 mg/ml 100 ml ML Phosphate (P 4 3- ) 1000 mg/ml 100 ml ML Sulfate (S 4 2- ) 1000 mg/ml 100 ml at. No ML Ammonium (NH 4+ ) 1000 mg/ml 100 ml ML Barium (Ba 2+ ) 1000 mg/ml 100 ml ML admium (d 2+ ) 1000 mg/ml 100 ml ML alcium a 2+ ) 1000 mg/ml 100 ml ML obalt (o 2+ ) 1000 mg/ml 100 ml ML opper (u 2+ ) 1000 mg/ml 100 ml ML Lead (Pb 2+ ) 1000 mg/ml 100 ml ML Lithium (Li + ) 1000 mg/ml 100 ml ML Magnesium (Mg 2+ ) 1000 mg/ml 100 ml ML Manganese (Mn 2+ ) 1000 mg/ml 100 ml ML Nickel (Ni 2+ ) 1000 mg/ml 100 ml ML Potassium (K + ) 1000 mg/ml 100 ml ML Sodium (Na + ) 1000 mg/ml 100 ml ML Strontium (Sr 2+ ) 1000 mg/ml 100 ml ML Zinc (Zn 2+ ) 1000 mg/ml 100 ml 100 ml 100 ml 100 ml 100 ml sigma-aldrich.com/standards References: 1. TraceERT Traceable ertified Reference Materials. Analytix, Vol 5, 2006; Analytix Vol 1 4, Double Accreditation brings a new class of RMs. Analytix, Vol 2, 2008.
16 16 Figure 1 L-MS L-MS HRMASLV / 100% Fluka L-MS HR- MASLV at.no % Fluka L-MS HRMASLV at.no HPL L-MS L-MS Figure ppm Figure 1 Fluka L-MS HRMASLV at.no.39253fluka L-MS HRMASLV at.no L-MS L-MS Figure 3 2 at. No at.no Figure 4 at. No Figure 2 Intens. x Intens. x Time [min] Time [min] L-MS HRMASLV 0.1% 0.01% TFA- 0.1% TFA-0.1% - L-MS HRMASLV L-MS L-MS Rudolf Köhling, L-MS Application Scientist rudolf.koehling@sial.com Michael Kiselewsky, Product Manager Analytical Reagents michael.kiselewsky@sial.com L-MS L-MS L Figure 1 Intens. x Time [min] sigma-aldrich.com/lc-ms
17 17Table 1 L-MS HRMASLV at. No. Fluka L 1 L Fluka L 1 L Fluka L-R 1 L Fluka L 2-1 L Fluka L-R 1 L Fluka L n- 1 L Fluka L n- 1 L Table 2 L-MS HRMASLV at. No. Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 0.01% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 0.01% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Fluka L-R, 0.1% (V/V) 2.5 L Table 3 L-MS at. No. Fluka X1ML-F 10 x 1 ml Fluka ML-F 50 ml Fluka X1ML-F 10 x 1 ml Fluka ML-F 50 ml Fluka ML-F 50 ml Fluka ML-F 50 ml Fluka G-F 50 G Fluka G-F 50 G Fluka G-F 50 G Fluka G-F 50 G Fluka ML-F 25% (V/V) 100 ml Fluka ML-F 50 ml Fluka L-R, /2-50/50 (V/V) 1 L Fluka L, 8% (V/V) 1 L sigma-aldrich.com/lc-ms Figure 3 Intens. x10 4 +MS, min #(1-787) Figure 4 Intens. x m/z +MS, min #(1-7) m/z
18 18 Buchs ASTM, AP / NLS,USP HPL T HPL-MS HPL-NMR TraceSELET Ultra Buchs Buchs UV ASTM I AP/NL I USP27 HPL L-MS Figure nmuv L-MS Figure 2 H2 H2 Michael Weber, Manager R&D Europe, Sigma-Aldrich Switzerland michael.weber@sial.com Jürg Wüthrich, Senior Scientist R&D Europe, Sigma-Aldrich Switzerland juerg.wuethrich@sial.com T GMP sigma-aldrich.com/water
19 19Figure 1 L-MS HRMASLV Buchs μg/l ng/l PFA FEP HPL -UV L-MS HRMASLV ppm L-MS (continued on page 20) Figure 2 purification steps containers specification handling pre-filtration material metal traces ambient atmosphere UV irradiation HD-PE anion traces clean room electro-deionisation glass, hydrolysis class I HPL gradient test inert gas reverse osmosis glass, hydrolysis class II L-MS test sterile handling activated charoal perfluorinated plastic T / organic traces molecular biology ion-exchange microfiltration fluorescence test endotoxine free microfiltration cleaning luminescence test ultrafiltration rinsing UV absorbation DEP treatment leaching particles autoclaving washing machine non-volatile residue autoclaving endotoxine test DEP treatment DNases / RNases phosphatases proteases mycoplasma sigma-aldrich.com/water
20 20 HDPE I HPL Table 1 3 HPL Specified parameter UV- HPL HPL - Water for HPL (Prod. no ) hromasolv Plus, for gradient HPL (Prod. no ) Water for L-MS (Prod. no ) L-MS UV HPL-MS Table 1 3 HPL Table 2 H 2 H 2 Table 2 Fluka Aldrich H= at. No L-R L-MS, HRMASLV,H-I, 1 L L HPL, HRMASLV Plus, H-II, 2.5 L L HPL, H-II, 2.5 L L HD-PE () L G-HS G-, H-II, 1 L L-F, TraceSELET Ultra, AS UltraTrace HD-PE ( ), 1 L L TraceSELET HD-PE (), 1 L L, H-II, 1 L L T, H-II, 1 L L (Aqua Purificata), Ph Eur, H-II, 1 L L, PESTANAL, H-II, 1 L sigma-aldrich.com/water
21 21 Michael Jeitziner, Market Segment Manager, Analytical Reagents & Standards PV S,S,S-2- - Figure 1 Fluka 305 Mexitil sensorics WEB sigma-aldrich.com/sensoric - [1] : Slope 53.8 mv/dec 150 mm Nal 10 mm HEPES-NaH 40 mm ph mg NaHFPB Fluka at.no mg Fluka at.no mg PV Fluka at.no [2] : Slope 58.8 mv/dec 150 mm Nal 10 mm NaH 2 P 4 /Na 2 HP 4 2 mm ph mg NaHFPB Fluka at.no mg Fluka at.no mg PV Fluka at.no.892 Table 1 at. No. as.no MG Fluka S,S,S-Tris(2-ethylhexyl)phosphorotrithioate, Selectophore mg G Fluka Poly(vinyl chloride) high molecular weight (PV), Selectophore g MG Fluka Sodium tetrakis[3,5-bis(1,1,1,3,3,3-hexafluoro-2-methoxy-2-propyl) phenyl]borate trihydrate (NaHFPB), Selectophore mg References 1] Katsu, T.; Hirodo, H. Serotonin-Selective Membrane Electrode Made with the Solvent Mediator S,S,S-Tris (2-ethylhexyl)phosphorotrithioate. Sensor Lett. 2003, 1, ] Katsu, T.; Tsunamoto, Y.; Hanioka, N.; Komagoe, K.; Masuda, K.; Narimatsu, S. S,S,S-Tris(2-ethylhexyl) phosphorotrithioate as an effective solvent mediator for a mexiletine-sensitive membrane electrode. Anal Bioanal hem. 2007, 387, Sensoric sigma-aldrich.com/sensoric
22 22 Helga Hoffmann, Technical Service HYDRANAL Manager Andrea Felgner, Product Manager Analytical Reagents I % Table 1 [1] % 7 % % % 24% 8 18% % 11 15% 0.8 4% 4.1% Figure 1 KFT Ipol 4,5 V [ml] 3,5 2,5 1,5 0,5 Titration NMRLD t[s] Figure 1 Figure 1a sigma-aldrich.com/hydranal
![23 Figure 1a Figure 2 KFT Ipol 40 KF -1-2 30 3000 606 455 dv/dt [μl/min] 20 Wasser [μlg] 2000 1000 303 152 Drift [μg/min] 10 o 0 1000 2000 3000 t[s] o 0 0 200 400 600 800 1000 t[s] LD LD 10g 10516 16](/docs-images/91/105462507/images/23-0.jpg "50 2501 4 mg/min Figure 2 50 90 90 150 150 140 0 140 1 9.01 % 8.93 % 2 8.82 % 8.94 % 3 8.58 % 8.92 % A B 16.43 %.81 % 21.67 % 14.00 % 37 14.04 % 14.36 % 53 14.19 % 14.")
23 23 Figure 1a Figure 2 KFT Ipol 40 KF dv/dt [μl/min] 20 Wasser [μlg] Drift [μg/min] 10 o t[s] o t[s] LD LD 10g mg/min Figure % 8.93 % % 8.94 % % 8.92 % A B %.81 % % % % % % % Figure % Titration (continued on page 24) sigma-aldrich.com/hydranal
24 24 40 ml 5 0.2g 15 50mL g ml G 100 ml AG-oven 100 ml AG-oven 0.02g 140 AG-oven AG AD Literature 1] Belitz, H. D.; Grosch, W.; Schieberle, P., Lehrbuch der Lebensmittelchemie (Handbook of Food hemistry). Springer: Berlin, Table 2 Titration at. no L-R Fluka L L-R Fluka - 1 L L-R Fluka - 1 L ML-R Fluka - AG ven 500 ml ML-R Fluka - AG 500 ml ML-R Fluka - AD 500 ml ML-R Fluka - G 50 ml ML Fluka -Water Standard ml (8 ml x 10) ML-R Fluka -Water Standard ml (4 ml x 10) G-R Fluka -Water Standard KF ven g * TEL mpd@hpc-j.co.jp sigma-aldrich.com/hydranal
25 25 Helga Hoffmann, Technical Service HYDRANAL Manager Andrea Felgner, Product Manager Analytical Reagents 1 g 2 2 No.616, No.612 KF mg 30 ml 1 g 1 g No M - M 1 2g Titration (continued on page 26) sigma-aldrich.com/hydranal
![26 2 M 2 M No.6No.615 1 3 50 250 Figure 1 50 160 160 0 ph ph 50 250 1 3 170 AG-ven AG AD G AG-ven AG AD no.614 no.617 Figure 1 KF 18.000 2.030 16.000 1.804 14.000 1.579 12.000 1.353 Titration Water [µg] 10.](/docs-images/91/105462507/images/26-1.jpg "000 8.000 6.000 4.000 1.128 902 677 451 Drift [µg/min] 2.000 226 0 50 70 90 110 0 150 170 190 210 230 250 270 Temperature 1 [ ] sigma-aldrich.com/hydranal")
26 26 2 M 2 M No.6No Figure ph ph AG-ven AG AD G AG-ven AG AD no.614 no.617 Figure 1 KF Titration Water [µg] Drift [µg/min] Temperature 1 [ ] sigma-aldrich.com/hydranal
27 27 Table 1 at. No L Fluka - 2 E L-R Fluka L-R Fluka L Fluka - M L Fluka L-R Fluka L Fluka - M* L-R Fluka ML-R Fluka - AG ven ML-R Fluka - AG ML-R Fluka - AD ML-R Fluka - G * TEL mpd@hpc-j.co.jp 1 L 1 L 1 L 1 L 1 L 1 L 1 L 1 L 500 ml 500 ml 500 ml 50 ml (10x5mL ampules) Riedel-de Haën Fluka Titration For assistance in choosing the correct product, contact our Technical Service at: Phone: / Fax: / techservice@sial.com or go to sigma-aldrich.com sigma-aldrich.com/hydranal
28 TraceSELET 本カタログに掲載の製品及び情報は 2009 年 5 月 1 日現在の内容であり 収載の品目 製品情報 価格等は予告なく変更される場合がございます 最新の情報は 弊社 Web サイト (sigma-aldrich.com/japan) をご覧ください 掲載価格は希望納入価格 ( 税別 ) です 詳細は販売代理店様へご確認ください 弊社の試薬は試験研究用のみを目的として販売しております 医薬品 家庭用その他試験研究以外の用途には使用できません
PowerPoint プレゼンテーション
溶媒 工業溶媒 Column : Equity-, 0 m x 0. mm ID,.0 µm Cat. No. : 0- Column : SPELCOWAX 0, 0 m x 0. mm ID,.0 µm Cat. No. : Column : Equity-0, 0 m x 0. mm ID,.0 µm Cat. No. : - Oven : ( min), /min to 0 ( min) Inj.:
<4D F736F F D F90858C6E5F C B B B838B>
Isobutyl alcohol IUPAC 2-methylpropan-1-ol 2--1-2-Methyl-1-Propanol, Isobutanol CH 3 H 3 C OH CAS 78-83-1 C 4 H 10 O log P ow ( C) ( C) (kpa) (g/l) 74.12 74.14 1) -108 2) 108 2) 1.2 2) 87 2) 0.8 2) (74.1214)
平成26年度 化学物質分析法開発報告書
N,N- N,N-Dimethylacetamide Acethyldimethylamine CAS 127-19-5 C 4 H 9 NO 87.12 ~ 87.14 87.68413 163-165 C 1) - 18.59 C 2) 1 mg/l 25 C 3) 3.3 hpa 2 C 4) log P ow -.77 2).9429 2/4 C 1) 3.1 4) 1.31E - 8 atm-m
untitled
Tl Thallium CAS 7440-28-0 CH 3 COOTl Thallium Acetate CAS 563-68-8 Tl 2 CO 3 Thallium Carbonate CAS 6533-73-9 Tl 2 SO 4 Thallium Sulfate CAS 7446-18-6 TlNO 3 Thallium Nitrate CAS 10102-45-1 TlClO 3 Thallium
Contents 4 06 IP2 41 Thermo Scientific Nalgene Nalgene
Nalgene & Packaging plastic Bottles & Vials Contents 4 06 IP2 41 Thermo Scientific Nalgene 5 07 42 8 08 43 9 09 45 11 10 46 Nalgene 12 11 50 13 12 53 01 20 13 61 02 28 14 64 03 33 15 66 04 37 16 / 67 05
PALL NEWS vol.126 November 2017
PALL NEWS November 2017 Vol.126 PALL NEWS vol.126 November 2017 NEW =2000 9660 41.4 MPa 24 MPa NFPA T2.06.01 R2-2001 CAT C/90/* (1x10 6 0-28 MPa 1x10 6 29 120 C 60 C 450 Pa 340 Pa 1 MPa JIS B 8356-3/ISO
untitled
2017 5 26 350 Restek time time time increasing time μ = = k = t r t o t o = t r ' t o van Deemter Equation H A B H = height equivalent theoretical plate (HETP) A = Eddy diffusion term B = Molecular diffusion
<4D F736F F D C6E30385F A B B83932E444F43>
1,2,4-1,2,4-Trimethylbenzene Pseudocumene 1,3,5-1,3,5-Trimethylbenzene Mesitylene CH 3 CH 3 CH 3 CH 3 CH 3 CH 3 1,2,4-trimethylbenzene 1,3,5-trimethylbenzene CAS 95-63-6 CAS 108-67-8 C 9 H 12 C 9 H 12
平成26年度 化学物質分析法開発報告書
2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
平成26年度 化学物質分析法開発報告書
2,2-2,2 -Iminodiethanol Diethanol amine CAS 111-42-2 C 4 H 11 NO 2 105.1356-105.0790-28 C 1) 1.0881 g/cm 3 1)
ヒト血漿中オキシステロールの高感度分析法
High sensitive determination of oxysterols in human plasma using gas chromatography-mass spectrometry (GC-MS) Saori Nakagawa and Susumu Yamato Oxysterols, cholesterol oxidation products, have been important
untitled
CONTENTS 1 004 005 006 2 008 010 010 010 011 011 012 012 013 013 014 014 3 016 016 017 018 019 019 020 020 020 021 021 022 022 022 023 023 023 023 024 024 025 025 025 025 4 028 030 031 032 032 032 032
CH 2 CH CH 2 CH CH 2 CH CH 2 CH 2 COONa CH 2 N CH 2 COONa O Co 2+ O CO CH 2 CH N 2 CH 2 CO 9 Change in Ionic Form of IDA resin with h ph CH 2 NH + COO
CH 2 CH CH 2 CH CH 2 CH CH 2 CH 2 COONa CH 2 N CH 2 COONa O Co 2+ O CO CH 2 CH N 2 CH 2 CO 9 Change in Ionic Form of IDA resin with h ph CH 2 NH + COOH COOH COOH COO - CH 2 NH + + CH 2 NH COO - COO - COO
Agilent Infinity ELSD ELSD ( ) ( ºC ) W x D x H mm LED ELSD ELSD ELSD UV UV LC/MS RSD % Column: Agilent Pursuit C8, x.6 mm, µm Eluent: Water: Acetonit
Agilent Infinity ELSD Agilent 6 Infinity ELSD Agilent 9 Infinity ELSD 6 8 ELSD 9 LC/MS ELSD Agilent Infinity ELSD ELSD ( ) ( ºC ) W x D x H mm LED ELSD ELSD ELSD UV UV LC/MS RSD % Column: Agilent Pursuit
MP-AES ICP-QQQ Agilent 5100 ICP-OES Agilent 5100 (SVDV) ICP-OES (DSC) 1 5100 SVDV ICP-OES VistaChip II CCD Agilent 7900 ICP-MS 7700 / 10 7900 ICP-MS ICP-MS FTIR Agilent 7900 ICP-MS Agilent Cary 7000 (UMS)
1 1 H Li Be Na M g B A l C S i N P O S F He N Cl A e K Ca S c T i V C Mn Fe Co Ni Cu Zn Ga Ge As Se B K Rb S Y Z Nb Mo Tc Ru Rh Pd Ag Cd In Sn Sb T e
No. 1 1 1 H Li Be Na M g B A l C S i N P O S F He N Cl A e K Ca S c T i V C Mn Fe Co Ni Cu Zn Ga Ge As Se B K Rb S Y Z Nb Mo Tc Ru Rh Pd Ag Cd In Sn Sb T e I X e Cs Ba F Ra Hf Ta W Re Os I Rf Db Sg Bh
薬物分析法の開発
API5000 TM LC/MS/MS Junichi_Hirokawa@trc.toray.co.jp 1. LC/MS/MS 2. 3. MS/MS 4. 5. API5000 6. 7. 8. 1. LC/MS/MS API 5000 AB/MDS Sciex UPLC API 4000 AB/MDS Sciex Agilent1100 PAL PAL ew wash 4000 QTRAP AB/MDS
36 th IChO : - 3 ( ) , G O O D L U C K final 1
36 th ICh - - 5 - - : - 3 ( ) - 169 - -, - - - - - - - G D L U C K final 1 1 1.01 2 e 4.00 3 Li 6.94 4 Be 9.01 5 B 10.81 6 C 12.01 7 N 14.01 8 16.00 9 F 19.00 10 Ne 20.18 11 Na 22.99 12 Mg 24.31 Periodic
03J_sources.key
Radiation Detection & Measurement (1) (2) (3) (4)1 MeV ( ) 10 9 m 10 7 m 10 10 m < 10 18 m X 10 15 m 10 15 m ......... (isotope)...... (isotone)......... (isobar) 1 1 1 0 1 2 1 2 3 99.985% 0.015% ~0% E
JAJP.indd
アジレントの認定標準物質 原子分光分析用の 無機金属および有機金属の標準溶液 MP-AES ICP-QQQ Agilent 5100 ICP-OES Agilent 5100 (SVDV) ICP-OES (DSC) 1 5100 SVDV ICP-OES VistaChip II CCD Agilent 7900 ICP-MS 7700 / 10 7900 ICP-MS ICP-MS FTIR Agilent
t 492 t mg/l 30 mg/l BOD 95 OH = cm 3 / sec 25 8 OH /cm 3 12 = ph ph
2-1 200169 2740 CAS 110-49-6 1103 2- O H 3 C C O CH 2 CH 2 O CH 3 C 5 H 10 O 3 118.13 200168 2-1 99 2-1. 2 2, 3-65 2, 3 144145 45 o.c. 3 392 3 1.512.3 d19 1.009 2 4.07 = 1 30 Pa 0.23 mmhg20 2 4 log Pow0.10
ｽﾗｲﾄﾞ ﾀｲﾄﾙなし
1 2 3 4 27,500 5 6 2000 7 8 9 10 11 12 < 13 SPECIFICATION CHARACTERISTICS UNIT Regular Gasoline Premium Gasoline METHOD A Type C Type A Type C Type ABNT ASTM Color - (1) (2) (1) (2) Appearance - (4) (4)
J. Brew. Soc. Japan. Vol.101, No.7, p.519 `525 (2006) Simple Method for the Determination of Ethyl Carbamate in Alcoholic Beverages Tomokazu HASHIGUCH
J. Brew. Soc. Japan. Vol.101, No.7, p.519 `525 (2006) Simple Method for the Determination of Ethyl Carbamate in Alcoholic Beverages Tomokazu HASHIGUCHI, Yukari IGI, Kuniyasu GoTo (National Research Institute
42 3 u = (37) MeV/c 2 (3.4) [1] u amu m p m n [1] m H [2] m p = (4) MeV/c 2 = (13) u m n = (4) MeV/c 2 =
![42 3 u = (37) MeV/c 2 (3.4) [1] u amu m p m n [1] m H [2] m p = (4) MeV/c 2 = (13) u m n = (4) MeV/c 2 =](/thumbs/73/68712188.jpg "42 3 u = (37) MeV/c 2 (3.4) [1] u amu m p m n [1] m H [2] m p = (4) MeV/c 2 = (13) u m n = (4) MeV/c 2 =")
3 3.1 3.1.1 kg m s J = kg m 2 s 2 MeV MeV [1] 1MeV=1 6 ev = 1.62 176 462 (63) 1 13 J (3.1) [1] 1MeV/c 2 =1.782 661 731 (7) 1 3 kg (3.2) c =1 MeV (atomic mass unit) 12 C u = 1 12 M(12 C) (3.3) 41 42 3 u
Agilent
Agilent Agilent CE Agilent Checklist CEC CE/MS Agilent CE CEC / CE/MS Agilent Agilent 10 High sensitivity detection cell 75 µm i.d. capillary Agilent CE Agilent Agilent CE Agilent CE/MS Agilent CE/MS Agilent
A-2 cyclopropane cyclobutane cyclopentane cyclohexane cycloheptane cyclooctane methylc
ethene H 2 H 2 169 104 propene H 2 HH 3 185 47 1 1-butene H 2 HH 2 H 3 185 6.3 11-pentene H 2 H(H 2 ) 2 H 3 138 30 0.641 11-hexene H 2 H(H 2 ) 3 H 3 140 64 0.673 11-heptene H 2 H(H 2 ) 4 H 3 119 94 0.697
ポリスチレン CAS.No Polystyrene certified by BAM Polystyrene Standard 88,000 * 正確な重量分子量 有効期限及び詳細情報は付属の証明書に記載されています 100mg MG-F 38,800 F Po
Analytical Standard News アナリティカルスタンダードニュース Vol. 08 分子量スタンダード GPC GFC / MALDI validation set 備考 F:FLUKA A:ALDRICH P1:PRTR 法第一種指定化学物質冷 : 冷蔵 脂溶性ポリマー ポリスチレン CAS.No.9003-53-6 Polystyrene 472 470 520 1g 81401-1G
元素分析
: このマークが付してある著作物は 第三者が有する著作物ですので 同著作物の再使用 同著作物の二次的著作物の創作等については 著作権者より直接使用許諾を得る必要があります (PET) 1 18 1 18 H 2 13 14 15 16 17 He 1 2 Li Be B C N O F Ne 3 4 5 6 7 8 9 10 Na Mg 3 4 5 6 7 8 9 10 11 12 Al Si P
H1-H4
42 S H He Li H He Li Be B C N O F Ne Be B C N O F Ne H He Li Be B H H e L i Na Mg Al Si S Cl Ar Na Mg Al Si S Cl Ar C N O F Ne Na Be B C N O F Ne Na K Sc T i V C r K Sc Ti V Cr M n F e C o N i Mn Fe Mg
平成25年度 化学物質分析法開発報告書
2,4-2,4-Dimethylaniline 2,4-2,4-Xylidine CH 3 CH 3 CAS 95-68-1 C 8 H 11 N 121.18 121.0892-14.3 C 2) 214 C 2) 0.9723 g/cm 3 2) 0.133 mmhg (25 C) 1) 1390 mg/l (25 C) 1) 3.710 3 mg/l 25 C WSKOWWIN 5) 6.0710
LCMS14003:UHPLC-Orbitrap質量分析計による環境汚染物質のターゲット分析、ノンターゲット分析
UHPLC Orbitrap Application Note LCMS14003 Orbitrap CEC CEC 61 CEC 312 CEC SPE UHPLCThermo Scientifi c Orbitrap Thermo Scientifi c TraceFinder WWTP S1 PS 5 ºC S2 TWAS 5 ºC 1 WWTP 1 2 WWTP 2 1 2 S1 1 S2
2 1 7 - TALK ABOUT 21 μ TALK ABOUT 21 Ag As Se 2. 2. 2. Ag As Se 1 2 3 4 5 6 7 8 9 1 1 2 3 4 5 6 7 8 9 1 1 2 3 4 5 6 7 8 9 1 Sb Ga Te 2. Sb 2. Ga 2. Te 1 2 3 4 5 6 7 8 9 1 1 2 3 4 5 6 7 8 9 1 1 2 3 4
untitled
HILIC ILIC BEH BEH 009 9 0 5 009 ihon Waters K.K. HILIC HILIC HILIC MS Sub-µm 009 ihon Waters K.K. HILIC? HILIC - Hydrophilic Interaction Chromatography 990 * HILIC (> 80%) *Alpert A. J. J.Chromatogr.
橡A PDF
2 1 MS 300 TRT MS JDI-800 2 g MS Py MS GC Py-GC Py GC 50 Py MS MS Py GC PY-GC 2 JDI-800 MS JDI-800 QP 2000 QP 1000 QP 2000 Fig 1 QP 1000 CI PEG 300 600 423 MS EI CI MS PEG 3 10 g Fig.1 300 600 MS 3 JDI-800
外因性内分泌攪乱化学物質調査暫定マニュアル（水質、底質、水生生物）
p,p -DDT p,p -DDE p,p -DDD trans- cis- trans- cis- (PBB) (BaP) 25ng/L 5µg/kg GC/MS-SIM GC/MS-SIM GC/MS-SIM GC/MS-SIM (2-, 3-, 4- ) (4,4'- ) p,p'-ddt- 13 C 12 HCB- 13 C 6 BaP-d 12 -d10 -d 10 p- -d 14 1000
バイアル新規ユーザー様限定 ガラス製容器 -Si-O H シラノール -Si-O H -Si O -Si イオン的吸着 疎水的吸着シロキサン logp pka + N 塩基性化合物 疎水的吸着 水溶液 P P 製容器, 7,7
P. P. P. LC P. GC P. P.7 GC P.8 GC ナツ 夏トク!! ワッショイ! SUMMER.7-.9 消耗品だいしょうもうひん まつり! 祭 Vol. バイアル新規ユーザー様限定 ガラス製容器 -Si-O H シラノール -Si-O H -Si O -Si イオン的吸着 疎水的吸着シロキサン logp pka + N 塩基性化合物 疎水的吸着 水溶液 P P 製容器, 7,7
untitled
Alkane n 2n+2 () 4 4 10 ( 2 6 5 12 ( 3 8 6 14 ( Alkane n 2n+2 () 4 4 10 ( Methane 2 2 Butane 2-Methylpropane 2 6 5 12 ( Ethane 2 2 2 Pentane 3 8 2 Propane 2,2-Dimethylpropane 2 2-Methylbutane 6 14 ( 2
Ⅱ6.3界面活性剤
6.3 6.3.1 6.3.1 6.3.1.1 (1) (2) a) JIS K 0557 A3 b) JIS K 8891 c) (5g/L) d) (10g/L)JIS K 8576 1g 100mL e) (7+993)JIS K 8951 f) JIS K 8322 g) 0.1g 100mL 30mL 1L 500mL6.8mL 50g 1L h) 1L 500mL6.8mL 50g 1L
JAJP
Agilent 7500ce ORS ICP-MS Glenn Woods Agilent Technologies Ltd. 5500 Lakeside, Cheadle Royal Business Park Stockport UK Agilent 7500ce ICP-MS 5 7500ce (ORS) 1 ORS 7500ce ORS ICP-MS ( ) 7500 ICP-MS (27.12
*1 *2 *1 JIS A X TEM 950 TEM JIS Development and Research of the Equipment for Conversion to Harmless Substances and Recycle of Asbe
*1 *2 *1 JIS A 14812008X TEM 950 TEM 1 2 3 4 JIS Development and Research of the Equipment for Conversion to Harmless Substances and Recycle of Asbestos with Superheated Steam Part 3 An evaluation with
Agilent 7900 ICP-MS 1 1 Ed McCurdy 2 1 Agilent Technologies, Japan 2 Agilent Technologies, UK
Agilent 7900 ICP-MS 1 1 Ed McCurdy 2 1 Agilent Technologies, Japan 2 Agilent Technologies, UK Na P K Ca Co Cu Sr Cd Ce Cs Tl 11 [1]18 [2] (FAO) (WTO) (Codex) Pb Cd As Sn Pb 0.3 mg/kg Cd 0.4 mg/kg 0.2 mg/kg
JAMSTEC Rep. Res. Dev., Volume 12, March 2011, 27 _ 35 1,2* Pb 210 Pb 214 Pb MCA 210 Pb MCA MCA 210 Pb 214 Pb * 2
JAMSTEC Rep. Res. Dev., Volume 12, March 2011, 27 _ 35 1,2* 1 1 1 1 210 Pb 210 Pb 214 Pb MCA 210 Pb MCA MCA 210 Pb 214 Pb 2010 10 4 2010 12 10 1 2 * 237-0061 2-15 046-867-9794 ogurik@jamstec.go.jp 27 210
Adenosine Triphosphate Adenosine Monophosphate min min Fig.2 Chromatograms of Nucleotides Peak
Hydrocortisone Sodium Phosphate 3.5 1.0 0.5 1 μg/ml 3.0 2.5 25 ng/ml 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min Fig.1 Chromatograms of Hydrocortisone
Introduction ur company has just started service to cut out sugar chains from protein and supply them to users by utilizing the handling technology of
Standard PA-Sugar Chain Catalogue Masuda Chemical Industries Co., LTD. http://www.mc-ind.co.jp Introduction ur company has just started service to cut out sugar chains from protein and supply them to users
untitled
1 2 3 4 Alteration of program parameters Effect Increase hybridization temperature Can prevent false positive signals, decrease background, can also increase dynamic range Decrease hybridization temperature
A4冊子1P-P20.ai
REVERSE PHASE CLUMN GUIDE 1 2 Luna 5 μm Phenyl-Hexyl, 150x4.6 mm Luna 5 μm C8(2), 150x4.6 mm Luna 5 μm C18(2), 150x4.6 mm : 50:15:35 Methanol:Acetonitrile: 20mM Ammonium Formate ph 3.5 : 1.0 ml/min : 1.
untitled
Frank David Research Institute for Chromatography President Kennedy Park B- Kortrijk, Belgium Pat Sandra University of Gent Krijgslaan 281 S4, B-9000 Gent Belgium Allen K. Vickers Agilent Technologies,
X線分析の進歩36 別刷
X X X-Ray Fluorescence Analysis on Environmental Standard Reference Materials with a Dry Battery X-Ray Generator Hideshi ISHII, Hiroya MIYAUCHI, Tadashi HIOKI and Jun KAWAI Copyright The Discussion Group
Aqua Way Philic Aqua Way Cation Technology platform Cell-sheet engineering (1) Technology platform Cell-sheet engineering (2) 1) Collection of cells in a form of thin film 2) o suture required for transplantation
外因性内分泌攪乱化学物質調査暫定マニュアル（水質、底質、水生生物）
(PCB) 1 ng/l (µg/kg, wet) (µg/kg) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001) 1 (0.001) 10 (0.01) 1 (0.001)
Green Light GxP HPLC 2
Excellence Plus Good Manufacturing Practice (GMP) 1 (OOS) (OOT) (OOE) 2 2 3 5 5 5 8 8 LevelControl 8 9 profact profact Advanced 9 TestManager 11 11 12 Green Light GxP HPLC 2 GMP GLP (USP) FDA (PAI) 7346.832
2
1 2 3 4 5 (written by Dr. ) Stock Solution (one liter) in 4 Buffer A: 0.05 M glucose 20% (1.1 M) glucose 22.7 ml 0.025 M Tris-Cl ph8 1 M Tris (ph8.0) 12.5 ml 0.01 M EDTA 0.5 M EDTA 10 ml Buffer B: 5 M
食糧 その科学と技術 No.46( )
, IARC A ppb ppm, WHOµg/L GC GC GCMS GC MS, d O O O NH 2 Br 2 NEt 3 Br NH 2 NH 2 Br Br GC, [C H NO Br] + m/z [C H NO Br] m/z SIM [C H D NO Br] m/z [C H D NO Br] + m/z Br Br HBr [C H NO Br] + m/z GC -d
xxxxEN.qxd
Ultron ES-VM : HPLC HPLC 28,000, 1-120Å 5-µm Ultron ES-VM [1-] Ultron ES-VM HPLC ph pi 3.8 4.3 Ultron ES-VM ph pi ph pka = 4.4 ph 3.0 6.0 pka = 4.0 9.2 k' 1 αph 1 Ibuprofen H3 C CHCH 2 CH CH H 3 C Chlorpheniramine
ッ ー ー ー() () 2.5 () () 21 1) -1 2) -2 10 m 5 7 23 6 1)2) 3) -1-2 H23.4.25 -15-20 4 75 5 1) -1 (5) (3) (3) (2) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) 1) ( 23 6 8 ) 2) 22 3)
000..\..
Bull. Nagoya Univ. Museum No. 20, 79 91, 2004 Quantitative chemical analysis of rocks with X-ray fluorescence analyzer XRF-1800 NAKAZAKI Mineko TSUBOI Motohiro KANAGAWA Kazuyo KATO Takenori SUZUKI Kazuhiro
untitled
DC Fan 8mm sq. General Specifications San Ace 8 15mm thick (GA type), 15mm thick, 2mm thick (GA type) 2mm thick, 25mm thick (GA type), 25mm thick (S type) 25mm thick (GV type), 25mm thick 25mm thick (San
Table 1 Air cleaning system of air cleaners tested *1: Eelectrostatic precipitation system without air filtration. I-3 and I-4 air cleaners are same w
Studies on Removal Performance of Odorants with Air Cleaners Masahiro FUSAYA1),2), Takashi AMAGAI1), Hidetsuru MATSUSHITA2) and Mitsuyuki SOMA1) 1) Graduate School of Nutritional & Environ. Sciences,University
COSMOSIL.indd
Column: 5C 18 -MS-II Column size: 4.6mmI.D.-150mm Mobile phase: Methanol/ H 2 = 60/40 Detection: UV254nm Sample: 1; Acetophenone (0.05μg) 2; Methyl Benzoate (0.5μg) 3; Benzene (2.0μg) 4; Toluene (2.0μg)
リサイクルデータブック2015
EUEconomy-wide Material Flow AccountsEW-MFA Domestic Extraction UsedDEU Direct Material InputDMI Domestic Material ConsumptionDMC A resource-effi cient Europe Flagship initiative under the Europe 22 Strategy
橡H10タイ第２章..doc
53 55 14001 1 5 BOD 1 2 2 56 1 1993 10 1998 23 ISO14001 20 1997 JICA ERTC: Environmental Research Training Center 10 1997 7 57 12 1 11 12 1 11 2 9 Federation of Thai Industries 58 59 1 1 A 9 I 2,900 1996
名称未設定
1 a C CF b c 4 5 Me Me S Jacobsen's catalyst Scheme 1. eagents and conditions: (a) C (1.5 equiv), Jacobsen's catalyst (0.05 equiv), toluene, 0 C, 40 h, then trifluoroacetic anhydride (4.0 equiv), 60 C,
Adenosine Triphosphate Adenosine Monophosphate min Fig.2 Chromatograms of Nucleotides min Peak
Adenosine Triphosphate Adenosine Monophosphate 0.0 1.0 2.0 3.0 4.0 5.0 6.0 min Fig.2 Chromatograms of Nucleotides 0.0 1.0 2.0 3.0 4.0 5.0 6.0 min Peak Asymmetry Peak 1 Peak 2 1.39 1.14 5.10 1.49 Instrument
☆H23 13－農薬一斉分析（大垣）.doc
13 56 2011 Examination of Determination of Residual Pesticides in Agricultural Products Yuki OHGAKI, Katsuhiro HAYASHI, Hiroyuki KAWAI, and Kyoko SHIMURA GC/MS 92 LC/MS/MS 60 150 n- 5 GC/MS 92 79 70% LC/MS/MS
RAA-05(201604)MRA対応製品ver6
M R A 対 応 製 品 ISO/IEC 17025 ISO/IEC 17025は 試験所及び校正機関が特定の試験又は 校正を実施する能力があるものとして認定を 受けようとする場合の一般要求事項を規定した国際規格 国際相互承認 MRA Mutual Recognition Arrangement 相互承認協定 とは 試験 検査を実施する試験所 検査機関を認定する国際組織として ILAC 国際試験所認定協力機構
2 (FDA) 1 1 A D E K 1 LC UV 15 HPLC 3.5 UHPLC Agilent 12 Infinity LC Agilent 12 Infinity (G1311B) Agilent 12 Infinity (G13E) Agilent 12 Infinity (G131
1 Agilent 12 Infinity 1 Siji Joseph Agilent Technologies, Inc. Bangalore, India 12 1 2 4 5 3 2 1 4 1 12 14 4 2 Agilent 12 Infinity 2 4 5 3 2.5 1. 1.5 2. 2.5 3. 2 (RP-HPLC) Agilent Poroshell EC-C1 Agilent
SIｻｲｴﾝｽ株式会社 stable isotope metal
12 マグネシウム Magnesium 24 Mg 酸化物 78.99 99.7 12 マグネシウム Magnesium 25 Mg 酸化物 10.0 97.0 12 マグネシウム Magnesium 26 Mg 酸化物 11.01 97.0 12 マグネシウム Potassium 39 K 塩化物 93.11 99.97 12 マグネシウム Potassium 40 K 塩化物 0.011 2.10
23 1 Section ( ) ( ) ( 46 ) , 238( 235,238 U) 232( 232 Th) 40( 40 K, % ) (Rn) (Ra). 7( 7 Be) 14( 14 C) 22( 22 Na) (1 ) (2 ) 1 µ 2 4
23 1 Section 1.1 1 ( ) ( ) ( 46 ) 2 3 235, 238( 235,238 U) 232( 232 Th) 40( 40 K, 0.0118% ) (Rn) (Ra). 7( 7 Be) 14( 14 C) 22( 22 Na) (1 ) (2 ) 1 µ 2 4 2 ( )2 4( 4 He) 12 3 16 12 56( 56 Fe) 4 56( 56 Ni)
Di(2-ethylhexyl) adipate C22H42O Dimethyl phthalate C10H10O Diethyl phthalate C12H14O D
) SVOC 1 Fluoranthene-d10 ( : C16D10 : 212.3 : 99.3%) 2. SVOC 1.2 1.5 m WHO 5.0 L/min 24 SVOC 50-100 240-260 (Volatile Organic Compounds: VOC)240-260 380-400 (Semi Volatile Organic Compounds: SVOC) VOC
3 夢を実現した加熱脱着導入システム GERSTEL TDS A2, /3C, CIS 4 -GC VVOC SVOC GERSTEL TDS A2 /3C CIS 4 Agilent 7890GC 5977MSD 1バルブレス流路を実現したオートサンプラー SVOC C 20 TDS A2 CIS
GERSTEL /3C 加熱脱着導入システム C www.gerstel.co.jp 3 夢を実現した加熱脱着導入システム GERSTEL TDS A2, /3C, CIS 4 -GC VVOC SVOC GERSTEL TDS A2 /3C CIS 4 Agilent 7890GC 5977MSD 1バルブレス流路を実現したオートサンプラー SVOC C 20 TDS A2 CIS 4 Agilent
01-表紙.ai
B 0 5 0-5 双極子核 I=1/ 2 四極子核 I 1 e Li Be B C N F Ne Na Mg 黒字はNMR 観測不可 Al Si P S Cl Ar K Ca Sc Ti V Cr MnFe Co Ni Cu ZnGaGe As Se Br Kr RbSr Y Zr NbMoTc RuRhPdAgCd In Sn SbTe I Xe Cs Ba La f Ta W Res Ir Pt
JIS Z 9001:1998JIS Z 9002:1998 ISO/IEC 17025ISO/IEC Guide 25
JIS Q 17025 IDT, ISO/IEC 17025 IT JIS Z 9001:1998JIS Z 9002:1998 ISO/IEC 17025ISO/IEC Guide 25 JIS Q 17025 IDT, ISO/IEC 17025 IT IT JIS Q 17025ISO/IEC 17025 (2) JIS Z 9358 ISO/IEC Guide 58 (3) testing
橡ﾏﾆｭｱﾙv4c.PDF
LC/MS MS LC/MS LC LC (APCI) (ESI) FAB 2 LC (APCI) 4.1.1.1 LC LC/MS LC MS LC 3 ph APCI/MS LC (1) APCI ESI 100% 100% ESI 4.1.1-1 LC 1.00cp 100 34 a 4.1.1-1 LC b ( /mpas) n- 0.23 36 0.5 99 0.31 69 n- 0.92
untitled
(F76A) .% TFA/acetonitrile TFA ph acetonitrile -propanol TFA Triart YMC-Triart C8 / C8 YMC-Triart C8 / C8 C8 C8 ( ).9 µm 3 µm µm nm C8 % C8 7% ph - 7 for ph -7 for ph 7- YMC-Triart % of initial retention
I N S T R U M E N T A T I O N & E L E C T R I C A L E Q U I P M E N T Pressure-resistant gasket type retreat method effective bulk compressibility Fro
Cable Gland This is the s to use for Cable Wiring in the hazardous location. It is much easier to install and maintenance and modification compared with Conduit Wiring with Sealing Fitting. The Standard
2 A B A B A A B Ea 1 51 Ea 1 A B A B B A B B A Ea 2 A B Ea 1 ( )k 1 Ea 1 Ea 2 Arrhenius 53 Ea R T k 1 = χe 1 Ea RT k 2 = χe 2 Ea RT 53 A B A B
5. A B B A B A B B A A B A B 2 A [A] B [B] 51 v = k[a][b] 51 A B 3 0 273.16 A B A B A B A A [A] 52 v= k[a] 52 A B 55 2 A B A B A A B Ea 1 51 Ea 1 A B A B B A B B A Ea 2 A B Ea 1 ( )k 1 Ea 1 Ea 2 Arrhenius
Fig. 1. Structures of NM394, NAD-358 and NAD-245 Fig. 2. Typical HPLC chromatograms of NM394 in human plasma by organic solvent extraction method (a): Blank plasma (b): Plasma spiked with NM394 and internal
mastro_nakamen三校.ai
Hydrocortisone Sodium Phosphate 3.5 1.0 0.5 1 μg/ml 3.0 2.5 25 ng/ml 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min Fig.1 Chromatograms of Hydrocortisone
Microsoft Word - 14_LCMS_アクリルアミド
3--2-3-Iodo-2-propynyl butylcarbamate (IPBC) Carbamic acid, butyl-, 3-iodo-2-propynyl ester Iodocarb CAS 55406-53-6 C 8 H 12 NO 2 I C (g/cm 3 ) (mmhg) log P ow 281.09 (280.9910) 64 68 1.51 1.57 (20 C)
2010 1 1 7 2 16 2 2 06in 3 3 錆 錆 06in 4 4 0.1 5 5 HCl Cl NaOH H Cl O 2 H H 2 O NaCl Na OH H 2 O NaCl 2010 6 6 ph3.0 30 mg/l 30 1 O-157 H7 2010 7 7 100 Cl 80 60 40 20 HClO ClO CL ph 10 100,000ppm 12 01
まえがき
JAAS0012006 1 -------------------------------------------------------------------------------------------------------- 1 2 --------------------------------------------------------------------------------------------------------
untitled
254nm UV TiO 2 20nm :Sr 5 Ta 4 O 15 3 4 KEY-1 KEY-2 (Ti,Nb,Ta) 5 KEY-1 KEY-2 6 7 NiO/ Sr 2 Ta 2 O 7 mmol h -1 g -1 20 15 10 5 H 2 O 2 H 2 O 2 0 0 2 4 6 8 10 12 NiO/Sr 2 Ta 2 O 7 The synthesis of photocatalysts
CRA3689A
AVIC-DRZ90 AVIC-DRZ80 2 3 4 5 66 7 88 9 10 10 10 11 12 13 14 15 1 1 0 OPEN ANGLE REMOTE WIDE SET UP AVIC-DRZ90 SOURCE OFF AV CONTROL MIC 2 16 17 1 2 0 0 1 AVIC-DRZ90 2 3 4 OPEN ANGLE REMOTE SOURCE OFF
Bond Elut 25%OFF Bond Elut 25 %OFF Bond Elut, Mega Bond Elut Bond Elut AL-A Bio Bond Elut Bond Elut AccuCAT Bond Elut Carbon Bond Elut Atrazine Bond E
2016 Bond Elut : 2 GC/MSD IDP-3 : 9 Captiva : 3-4 : 10-11 ZORBAX / Poroshell120 LC : 5-6 J&W DB-WAX GC : 7-8 ICP-OES MP-AES ICP-MS : 12 Bond Elut 25%OFF Bond Elut 25 %OFF Bond Elut, Mega Bond Elut Bond
gc-guide
...1...3 (Direct Injection)...5 OCI...7 PTV (...9 FID...11 ECD...13 AOC-20i/s...15...17...19 10 1 10 1 2µL 1µL 1mL 0.10.2mL He (He) 25cm/sec40cm/sec 30mL/min 1:501:100 Table Ex. Rtx-1, 515m :Ex. 100cm/sec
CHROMATOGRAPHY, Vol.32 No.3 (2011) Technical Review CoronaCAD Recent Developments in Charged Aerosol Detection Technology and Applications Kyoko Fukus
Technical Review CoronaCAD Recent Developments in Charged Aerosol Detection Technology and Applications Kyoko Fukushima, Kusuo Hashiguchi, Takahiro Suzuki, Masamitsu Okawara Yoko Sekiguchi NIPPON DIONEX
xEffect_SG_MV_Part2_E_xEffect_SG_MV_E
Miniature Circuit Breakers FAZ-NA, FAZ-RT, FAZ-DU SG56912 FAZ-NA/-RT/-DU According to UL 489, CSA C22.2 No. 5 and also IEC 60947-2 standard For Applications, wich are permitted for UL 1077 or CSA C22.2
PAXgene Tissue DNA Kitプロトコールとトラブルシューティング(2301605 06/2009)
January 2009 PAXgene Tissue DNA Kit PAXgene Tissue Containers DNA PAXgene Tissue Container PAXgene DNA 3 PAXgene DNA 6 PAXgene DNA 9 13 2 PAXgene Tissue DNA Kit 01/2009 PAXgene DNA DNA PAXgene Tissue Containers
ステンレス鋼用高性能冷間鍛造油の開発
Development of High Performance Cold Forging Oil for Stainless Steel Toshihide Ohmori, Kazuhiko Kitamura ClP ( ) Cl P-Zn ( P ) ClP-Zn High performance cold forging oil for stainless steel has been developed
1 WSV SIR m/z Analyte RT (Min) SIR m/z Cone voltage (V) Ascorbic Acid (C).91 177 2 Thiamine (B1) 1.1 265 5 Nicotinic Acid (B3) 1.27 124 15 Pyridoxal (
ACQUITY UPLC H-Class ACQUITY QDa Mark E. Benvenuti, Dimple Shah, and Jennifer A. Burgess Waters Corporation, Milford, MA, USA MS ACQUITY QDa UPLC HPLC UV ACQUITY QDa LC EC 1925/26 CFR 21 HPLC 1 LC-MS ACQUITY
LC-MS LC-MS NMR NMR LC-NMR [1] LC-NMR LC-NMR LC-NMR NMR [2] LC-NMR MHz NMR HPLC NMR LC-NMR LC-NMR LC-NMR WET water suppression enhanced through T1 eff
![LC-MS LC-MS NMR NMR LC-NMR [1] LC-NMR LC-NMR LC-NMR NMR [2] LC-NMR MHz NMR HPLC NMR LC-NMR LC-NMR LC-NMR WET water suppression enhanced through T1 eff](/thumbs/91/106638573.jpg "LC-MS LC-MS NMR NMR LC-NMR [1] LC-NMR LC-NMR LC-NMR NMR [2] LC-NMR MHz NMR HPLC NMR LC-NMR LC-NMR LC-NMR WET water suppression enhanced through T1 eff")
Technical Review LC-NMR How do you use liquid chromatography-nuclear magnetic resonance (LC-NMR) effectively for structural determinations of pharmaceutical impurities and metabolites? Toray Research Center,
微粒子合成化学・講義
http://www.tagen.tohoku.ac.jp/labo/muramatsu/mura/main.html E-mail: mura@tagen.tohoku.ac.jp 1 2 3 1m 10cm 1cm 1mm 100 m 10 m 1 m 100nm 10nm 1nm 1 100 m 10 m 1 m 1nm 100nm 10nm 4 5 6 7 1m 10cm 1cm 1mm 100
RN201602_cs5_0122.indd
ISSN 1349-1229 No.416 February 2016 2 SPECIAL TOPIC113 SPECIAL TOPIC 113 FACE Mykinso 113 SPECIAL TOPIC IUPAC 11320151231 RI RIBFRILAC 20039Zn30 Bi83 20047113 20054201283 113 1133 Bh107 20082009 113 113
ICP-OES ICP-MS
ICP-OES ICP-MS AGILENT CROSSLAB Agilent CrossLab Agilent CrossLab Agilent CrossLab ICP-OES ICP-MS ICP-OES ICP-MS 24 48 (www.agilent.com/chem/jp) AGILENT CROSSLAB Agilent CrossLab Agilent CrossLab Agilent
PowerPoint プレゼンテーション
2004 3 3 2 3 4 5 6 7 8 9 10 T. Ito, A. Yamamoto, et al., J. Chem. Soc., Chem. Commun., 136 (1974) J. Chem. Soc., Dalton Trans., 1783 (1974) J. Chem. Soc., Dalton Trans., 1398 (1975) 11 T.Ito, A. Yamamoto,
14 15 12 17 3 24 iii 1 1. 1 1 1. 2 1 1. 3 2 1. 4 3 2 2. 1 6 2. 2 7 2. 2. 1 7 2. 2. 2 12 3 3. 1 14 3. 2 15 4 4. 1 17 4. 2 17 4. 2. 1 17 4. 2. 2 17 4. 2. 3 20 4. 2. 4 22 4. 2. 5 25 4. 3 25 4. 3. 1 25 4.
-------------------------------------------------------------------------------------------------- 1 ----------------------------------------- 3 --------------------------------------------------------------------------------
/
333 344 / 332 03-6264-066003-6264-0663 03-6264-0620 334 LAL 335 336 LAL 338 QCL-1000 LAL 33 LAL 340 C 341 LAL 343 ELx808 344 FLx800 345 PyroTec 346 WinKQCL 347 CSE 348 / 03-6264-066003-6264-0663 03-6264-0620
Description
Metal Hybrid Inductor Description Metal Hybrid Inductor Magnetically shielded Suitable for Large Current Size: 4.3 x 4.3 x H2.1 mm Max. Product weight:.18g (Ref.) Halogen Free available Operating temperature
振動充填燃料の粒子焼結試験実施計画書
C JNCTJ8410 2004-006 2004 3 ( ) UPRISE Nd 250mL 0.2 mol Nd Nd (FP)DF DOBA DOiBA NN'-2--1.6 mol/l NN'- -1.7 mol/l NN'-1.5 mol/l DOBA 1mol/L 3.5mol/L 2 NN'--1.7 mol/l NN' -1.5 mol/l ZrRu Ce DF 150 100 Sr