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- ことこ ひろなが
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1
2
3 OECD OECD
4 NOEC LC 50 EC
5 OECD TG210Fish, Early-life Stage toxicity Test ISO 12890Water quality - Determination of toxicity to embryos and larvae of freshwater fish Semi-static method OECD TG201Freshwater Alga and Cyanobacteria, Growth Inhibition Test ISO 8692 Water quality - Freshwater algal growth inhibition test with unicellular green algae OECD TG211Daphnia magna Reproduction Test ISO 10706Water quality - Determination of long term toxicity of substances to Daphnia magnastraus (Cladocera, Crustacea) ISO10253: Water quality. Marine algal growth inhibition test with Skeletonema costatum and Phaeodactylum tric rnutum
6 OECD TG212Fish, Short-term Toxicity Test on Embryo and Sac-Fry Stages OECD TG203Fish, Acute Toxicity Test OECD TG215Fish, Juvenile Growth Test ISO 10229Water quality - Determination of the prolonged toxicity of substances to freshwater fish - Method for evaluating the effects of substances on the growth rate of rainbow trout[oncorhychus mykiss Walbaum (Teleostei, Salmonidae) OECD TG202Daphnia sp., Acute Immobilisation Test ISO 6341 Water quality - Determination of the inhibition of the mobility of Daphnia magna Straus (Cladocera, Crustacea) - Acute toxicity test 1 ISO 14669Water quality - Determination of acute lethal toxicity to marine copepods (Copepoda, Crustacea)
7 (US EPA) AQUIRE AQUatic toxicity Information REtrieval) (EU)IUCLID International Union Chemical Information Database ECETOC ECETOC Aquatic ToxicityEAT) () NEDO () OECD HPVC SIDS Screening Information Data Set EU-RAR European Union Risk Assessment Report WHO EHC Environmental Health Criteria Canadian Environmental Protection ActPriority Substances List Assessment Report (JST) (JDream, JSTPlus, JST7580, JMEDPlus, MEDLINE) NII (CiNii) Science Direct, BlackWell Synergy, SpringerLink 5
8 80% ph AQUIRE Document code 1 Moderate Incomplete 1 Document Code Incomplete 5185 Moderate 86 Complete
9 A B B1 B2 OECD C 7
10 D A B1 A ( ) ( ) B C B1 A A B 8
11 * OECD OECD cm cm 2.510cm ph DO 60% mg/l / DO /ml /ml 9
12 Early life ph DO 60% 60% / DO DO DO 10
13 Organisation for Economic Co-operation and DevelopmentOECD 1. OECD TG201Freshwater Alga and Cyanobacteria, Growth Inhibition Test 2. OECD TG202Daphnia sp., Acute Immobilisation Test 3. OECD TG203Fish, Acute Toxicity Test 4. OECD TG210Fish, Early-life Stage toxicity Test 5. OECD TG211Daphnia magna Reproduction Test 6. OECD TG212Fish, Short-term Toxicity Test on Embryo and Sac-fry Stages 7. OECD TG215Fish, Juvenile Growth Test 8. OECD TG221Lemna sp. Growth Inhibition Test International Organization for StandardizationISO 9. ISO 6341 Water quality - Determination of the inhibition of the mobility of Daphnia magna Straus (Cladocera, Crustacea) - Acute toxicity test 10. ISO 8692 Water quality - Freshwater algal growth inhibition test with unicellular green algae 11. ISO 10229Water quality - Determination of the prolonged toxicity of substances to freshwater fish - Method for evaluating the effects of substances on the growth rate of rainbow trout[oncorhychus mykiss Walbaum (Teleostei, Salmonidae) 12. ISO 10253Water quality - Marine algal growth inhibition test with Skeletonema costatum and Phaeodactylum tricornutum 13. ISO 10706Water quality - Determination of long term toxicity of substances to Daphnia magnastraus (Cladocera, Crustacea) 14. ISO 12890Water quality - Determination of toxicity to embryos and larvae of freshwater fish Semi-static method 15. ISO 14442Water quality - Guidelines for algal growth inhibition tests with poorly soluble materials, volatile compounds, metals and waste water 16. ISO 14669Water quality - Determination of acute lethal toxicity to marine copepods (Copepoda, Crustacea) 17. Organisation for Economic Co-operation and DevelopmentOECD 18. OECD TG204Fish, Prolonged Toxicity Test 11
14 Toxic Substances Control ActTSCA Federal Insecticide, Fungicide and Rodenticide Act (FIFRA) 32. OPPTS Aquatic invetebrate acute toxicity, test, freshhwater daphnids 33. OPPTS Gammarid acute toxicity test 34. OPPTS Oyster acute toxicity test (shell deposition) 35. OPPTS Mysid acute toxicity test 36. OPPTS Penaeid acute toxicity test 37. OPPTS Bivalve acute toxicity test (embryo larval) 38. OPPTS Fish acute toxicity test, freshwater and marine 39. OPPTS Fish acute toxicity mitigated by humic acid 40. OPPTS Daphnid chronic toxicity test 41. OPPTS Mysid chronic toxicity test 42. OPPTS Fish early-life stage toxicity test 43. OPPTS Fish life cycle toxicity 850 Toxic Substances Control ActTSCA Code of Federal Regulations Title 40 Protection of Environment Algal acute toxicity test Daphnid acute toxicity test Daphnid chronic toxicity test Fish acute toxicity test. 12
15 Fish early life stage toxicity test Mysid shrimp acute toxicity test Mysid shrimp chronic toxicity test. Federal Insecticide, Fungicide and Rodenticide Act (FIFRA) 51. OPP 72-1 Freshwater Fish Acute-warm and coldwater species with TGAI or TEP(FIFRA ) 52. OPP 72-2 Freshwater Invertebrate Acute TGAI or TEP(FIFRA ) 53. OPP 72-3 Estuarine/ Marine Fish, Shellfish, Shrimp Acute using TGAI or TEP(FIFRA ) 54. OPP 72-4a Freshwater or Marine/Estuarine Fish Early Life Stage Chronic Toxicity using TGAI or TEP(FIFRA ) 55. OPP 72-4b Freshwater Invertebrate Life Cycle Chronic Toxicity using TGAI or TEP(FIFRA ) 56. OPP 72-5 Full Fish Life Cycle TGAI(FIFRA ) * TGAI= Technical Grade Active Ingredient TEP=Typical End-Use Product 57. SEP: Acute Toxicity Test for Freshwater Invertebrates (EPA-540/ ;1985) 58. SEP: Acute Toxicity Test for Freshwater Fish (EPA-540/ ; 1985) 59. SEP: Fish Life-Cycle Toxicity Tests (EPA-540/ ; 1986) 60. SEP: Fish Early Life-Stage Test (EPA-540/ ; 1986) 61. SEP: Daphnia magna Life-Cycle (21-Day Renewal) Chronic Toxicity Test (EPA-540/ ; 1986) 62. SEP: Non target Plants: Growth and Reproduction of Aquatic Plants-Tiers 1 and 2 (EPA-540/ ;1986) 63. SEP: Acute Toxicity Test for Estuarine and Marine Organisms (Estuarine Fish 96-Hour Acute Toxicity) (EPA-540/ , 1985) 64. SEP: Acute Toxicity Test for Estuarine and Marine Organisms (Shrimp 96-Hour Acute Toxicity Test) (EPA-540/ O, 1985). 65. SEP: Acute Toxicity Test for Estuarine and Marine Organisms (Mollusc 96-Hour Flow Through Shell Deposition Study) (EPA-540/ , 1985) / 66. SEP: Acute Toxicity Test for Estuarine and Marine Organisms (Mollusc 48-Hour Embryo Larvae Study) (EPA-540/ , 1985) *SEPStandard Evaluation Procedure American Society for Testing and MaterialsASTM 67. E Standard Guide for Conducting Static Acute Toxicity Tests Starting with Embryos Four Species of Saltwater Bivalve Molluscs 68. E Standard Guid for Conducting Acute Toxicity Tests on Test Materials with Fishes, Macroinvertebrates, and Amphibians 69. E Standard guide for conducting life-cycle toxicity tests with saltwater rmysids 70. E Standard Guid for Conducting Daphnia magna Life-cycle Toxicity Tests 71. E aStandard guide for conducting static 96-h toxicity tests with microalgae 13
16 72. E Standard guide for conducting early life-stage toxicity tests with fishes 73. E Standard guide for conducting three-brood, renewal toxicity test with Ceriodaphnia dubia 74. E Standard guide for conducting static toxicity tests with Lemma gibba G3 75. E Standard guide for acute toxicity test with the rotifer Barchionus 76. E Standard guide for conducting static and flow-through acute toxicity tests with mysids from the west coast of the United States 77. E Standard guide for conducting acute, chronic, and life-cycle aquatic toxicity tests with polychaetous annelids 78. E Standard guide for conducting static acute toxicity tests with echinoid embryos 79. EPS1/RM/ 9Biological Test Method: Acute Lethality Test Using Rainbow Trout 80. EPS1/RM/ 10 Biological Test Method: Acute Lethality Test Using Threespine Stickleback (Gasterosteus aculeatus) 81. EPS1/RM/ 11Biological Test Method: Acute Lethality Test Using Daphnia spp. 82. EPS1/RM/21Biological Test Method: Test of Reproduction and Survival Using thecladoceran Ceriodaphnia dubia 83. EPS1/RM/24Biological Test Method: Toxicity Test Using Luminescent Bacteria 84. EPS1/RM/25Biological Test Method: Growth Inhibition using a Freshwater Alga 85. EPS1/RM/26Biological Test Method: Acute Test for Sediment Toxicity Using Marine or Estuarine Amphipods. 86. EPS1/RM/27Biological Test Method: Fertilization Assay Using Echinoids(Sea Urchins and Sand Dollars) 87. EPS1/RM/28Biological Test Method: Toxicity Tests Using Early Life Stages of Salmonid Fish (Rainbow Trout) 88. EPS1/RM/37Biological Test Method: Test for Measuring the Inhibition of Growth Using the Freshwater Macrophyte, Lemna minor (Deutsche Normen) DIN German standard methods for the examination of water, waste water and sludge; Test methods using water organisms (group L); Determination of the effect on microcrustacea of substances contained in water (Daphnia short-time test) (L 11) 90. DIN German standard methods for the examination of water, waste water and sludge; bio-assays (group L); determining the tolerance of green algae to the toxicity of waste water (Scenedesmus chlorophyll fluorescence test) by way of dilution series (L 33) 91. DIN German standard methods for the examination of water, waste water and sludge - Bio-assays (group L) - Part 37: Determination of the inhibitory effect of water on the growth of 14
17 bacteria (Photobacterium phosphoreum cell multiplication inhibition test) (L 37) 92. DIN EN ISO 10253Water quality - Marine algal growth inhibition test with Skeletonema costatum and Phaeodactylum tricornutum (ISO 10253:2006); German version EN ISO 10253: DIN EN ISO 10712Water quality - Pseudomonas putida growth inhibition test (Pseudomonas cell multiplication inhibition test) (ISO 10712:1995); German version EN ISO 10712: DIN EN ISO 20079Water quality - Determination of the toxic effect of water constituents and waste water on duckweed (Lemna minor) - Duckweed growth inhibition test (ISO 20079:2005); German version EN ISO 20079: DIN EN ISO 6341Water quality - Determination of the inhibition of the mobility of Daphnia magna Straus (Cladocera, Crustacea) - Acute toxicity test (ISO 6341:1996); German version EN ISO 6341: DIN EN ISO Water quality - Determination of the acute lethal toxicity of substances to a freshwater fish [Brachydanio rerio Hamilton-Buchanan (Teleostei, Cyprinidae)] - Part 2: Semi-static method (ISO :1996); German version EN ISO : DIN EN ISO 8692Water quality - Freshwater algal growth inhibition test with unicellular green algae (ISO 8692:2004); German version EN ISO 8692:
18 NO YES NO YES NO YES 16
19 ( ) NO YES 17
20 * *
21 10 19
0 0 0 0............ PNEC.............................. PNECsed.................. 0 0 0 0 PNEC logpow. * Oncorhynchus mykisslc0. mg/l UFs0,000 0.000 mg/l0. µg/lpnec PNECwater PNECwater * Sangster, J. ()
,161 t 9,753 t 2,408 t LC 50 mg/ L EC 50 mg/l * 5 : Selenastrum 6772-h, Sb 2 O 3, : capricornutum 6 3 Selenastrum h, Sb
1 20017 1543 CAS 1309644 125 Sb 2 O 3 291.52 1 99 1. 2 655 1,425 2 2 2 3 5.2 5.67 2 2 2. 10 12,161 t 9,753 t 2,408 t 4 3. 1 2 3 4. LC 50 mg/ L EC 50 mg/l * 5 : Selenastrum 6772-h, Sb 2 O 3, : capricornutum
CAS NC(CH 2 ) 4 CN 1,4- C 6 H 8 N c.c d = Pa
1 200117 21512 CAS 111693 110 NC(CH 2 ) 4 CN 1,4- C 6 H 8 N 2 108.14 1 99 2-1. 2 1 295 159 c.c. 550 3 1.7-4.9 20 d 0.965 4 3.73 = 1 0.3 Pa 0.002 mmhg20 2 log Pow-0.32 m/z 41, 1.0 68 0.54 54 0.43 4 Koc9-16
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 2 16 17 18 19 20 29 1 21 22 23 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21... 1... 1... 1 PNEC... 2... 2... 3... 4... 4... 5... 6... 6... 6... 6... 6... 7...
3, ,104 t mg/l 30 mg/l BOD mg 14 C 8, /kg 11 8, 1 11 OH = cm 3 / sec 11 OH /cm ppm
3, 3-1 200019 4800 CAS 91941 1138 3, 3-4, 4 - -3, 3 - H 2 N Cl Cl NH 2 C 12 H 10 C l2 N 2 253.13 1 95 1. 2 3, 4 132-133 402 5 >200 5 700kg/m 3 5 8.73 = 1 5.610-8 kpa 4.210-7 mmhg20 4 6 log Pow3.51 3.57
橡三酸化二アンチモン.PDF
1 2001 7 1 543( ) CAS 1309 64 4 1 25 ( ) Sb 2 O 3 291.52 1) 99 1. 2) 655 3) 1,425 3) ( ) 2) ( ) 2) ( ) 2) 5.2 ( ) 5.67 ( ) 3) 2) 2. 10 12,161 t ( 9,753 t 2,408 t) 4 2 1) 3. 1) 2) 3) 4. Selenastrum capricornutum
,309 t 22,069 t 7,240 t µg/l µg/l < ,431-70, , , mg/l m
1 20019 1527 CAS 1317368 1230 PbO 223.20 1 99 1. 2 888 2 9.53 0.017 g/l 20 3 3 2 2. 10 29,309 t 22,069 t 7,240 t 4 1 3. 1 2 3.5 6 1 µg/l 9.1-24 2 µg/l < 43 6 27,431-70,000 4.5-1,300 13.4-17 31.7 0.48-3,459
資料２
OECD GLP OECD OECD 1960 30 OECD TG 2001 10 17 8 TG 202 208 TG 201 1984 6 TG 202 1984 4 TG 202 2000 10 TG 203 1992 7 TG 204 14 1984 4 TG 205 1984 4 TG 206 1984 4 TG 207 1984 4 TG 208 1984 4 2000 TG 209
橡96-07.PDF
1 967 2482 CAS 50000 CH 2 O 30.03 2952% 12.5 % 1. 2) -92 2) -19.5 2) 5085 3) 424 3) 7.073.0% 4) 20 d 4 0.815 5) 1.03 ( = 1) 5) 1.33 kpa (10 mmhg) (-88.0) 2) log Pow0.35 ( ) 6) 0.35 ( ) 7) 1) m/z 29 ( 1.0
CAS H 3 C C CH 2 C 9 H tert d = hpa
1 200140 35 CAS 98839 1335-2- H 3 C C CH 2 C 9 H 10 118.18 1 99 4-tert- 1. 2-23.2 2 163164 2 54 574 3 0.96.6 20 d 4 0.9082 2 4.07 = 1 2.5 hpa 1.9 mmhg20 2 4 log Pow3.48 3.44 m/z 118, 1.0 103 0.58 91 0.21
CAS O C O * DOP* DEHP 2- C O O * n- C 24 H 38 O CH 2 CH 2 CH 2 CH 3 CH (CH 2 ) % 2- A BHT , 4
2-1 9628 31307 CAS 117817 2- O C O * DOP* DEHP 2- C O O * n- C 24 H 38 O 4 390.56 CH 2 CH 2 CH 2 CH 3 CH (CH 2 ) 3 1 99 % 2- ABHT 1. 2-55 3 3, 4 386 171 350 6 0.1 % d 20 4 0.9861 4 13.48 0.30410-4 Pa 2.2810-7
橡アジポニトリル.PDF
1 200117 21512( ) CAS 111693 110( ) 1,4- NC(CH 2 ) 4 CN C 6 H 8 N 2 108.14 1) 99 2-1. 2) 1 2) 295 2) 159(c.c.) 3) 550 3) 1.7-4.9 vol % ( ) 3) d 20 0.965 2) 3.73 ( = 1) 4 0.3 Pa (0.002 mmhg) (20) 2) log
橡フタル酸ブチルベンジル.PDF
1 97 7 3 1312 CAS 85 68 7 O BBP 1, 2- C 19 H 20 O 4 312.4 C C O O O (CH 2 ) 3 1 99.9 % 1. 2-35 3 2, 3 370 3, 4 199 d 25 4 1.117 2 10.8 = 1 5 1.15 10-3 Pa 8.6 10-6 mmhg 20 5 253 Pa 1.9 mmhg 200 5 log Pow
http://www.who.int/ipcs/publications/ehc/en/index.html EHC 1 2 3 4 / EHC http://www.nihs.go.jp/dcbi/publist/ehchsg/ 1-8) WHO/IPCS CICAD (Concise Inter
3 [ ] Priority IARC JMPR 2004 10 Priority 1 Priority 1 Priority 2 Priority 3 Priority 1 1-1) CERI) http://www.cerij.or.jp/ceri_jp/koukai/sheet/sheet_indx4.htm http://www.safe.nite.go.jp/data/sougou/pk_list.html?table_name=hyoka&rank=sh
橡99-24_00 アリルアルコール.PDF
1 9924 2260 CAS 107186 H 2 C CH CH 2 OH 2- -1- C 3 H 6 O 58.08 1 99 1. 2, 3 3, 4, 5-129 96-97 2 21c.c. 24o.c. 2 6, 7 378 6, 7 2.5-18 d 20 4 0.8540 2, 5 2.00 = 1 2.7 kpa 20 mmhg204.3 kpa 32 mmhg30 4 log
t 492 t mg/l 30 mg/l BOD 95 OH = cm 3 / sec 25 8 OH /cm 3 12 = ph ph
2-1 200169 2740 CAS 110-49-6 1103 2- O H 3 C C O CH 2 CH 2 O CH 3 C 5 H 10 O 3 118.13 200168 2-1 99 2-1. 2 2, 3-65 2, 3 144145 45 o.c. 3 392 3 1.512.3 d19 1.009 2 4.07 = 1 30 Pa 0.23 mmhg20 2 4 log Pow0.10
化学物質の環境リスク初期評価（平成９～１２年度）結果[39物質]
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(1) CAS 302-01-2 N 2 H 4 32.0 CAS 7803-57-8 2 1) 2.0 2,3) 113.5 2,4) 1.011 (15 ) 2,3) 1.0036 (25 ) 2,4) 2.1 kpa (16 mmhg) (20 ) 3) 1ppm=1.31 mg/m 3 at 25, n- / -1.37 ( ) 3) 5) K b1 8.510-7 K b2 8.910-16
98-02.PDF
1 982 2207 CAS 67630 2- H 3 C H 3 C CH OH C 3 H 8 O 60.10 1 99.9 % n- 1. 2-88.5 3 82.5 3 11.7c.c. 455 4 212 d 20 4 0.78505 3 2.1 = 1 4 4.4 kpa 33 mmhg20 4 log Pow0.05 0.07 5 m/z45, 1.0 43 0.19 27 0.17
資料３ 諸外国における位置づけ
1 1. ( 1) ) 2) 3) 4) 5) 6) 7) 8) 9) 10) 11) 12) 13) 14) 15) 16) ( 1) ) 2) 3) 4) 5) 6) 7)28 8)Ames 9) 10) 11) ( 1) ) 2) 3) 4) ( 1) ) 2) 3) 4) 2 TSCA (a) FIFRA (b) (c) FFDCA (d) FFDCA (e) FFDCA (f) (g) PMN
,977 t 157,977 t mg l mg l BOD 9398 % OH = cm 3 / sec 11 = cm 3 / sec OH = /
1 9625 2219 CAS 75569 1, 2-1, 2- H 2 C CH CH 3 C 3 H 6 O 58.08 1 99 % 1. 2 2, 3-112.13 2, 3 34.23-37 449 2.8-37 % 2 d 0 4 0.859 4 d 20 0.8304 2 2, 4 2.00 = 1 53.33 kpa 400 mmhg18 59.33 kpa 445 mmhg20 5
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(1) 1,2- DMP CAS 131-11-3 C 10 H 10 O 4 194.2 2 1) 5.5 2,3) 283.7 2,3) 1.192 (20 ) 4) 133 Pa (1 mmhg) (20 ) 5) 1ppm=7.94 mg/m 3 at 25, n- / 1.56 ( ) 6) 4) ( )3.2 (30 ph 7)11.6 (30 ph 9)25 (18 ph 9) 5)
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137 7 33 pco 2 2005 pco 2 340ppm pco 2 http://www.data.kishou.go.jp/kaiyou/shindan/sougou/html/1.4.html GEOSECS Geochemical Ocean Sections Study Nakano et al.(2006) 1 pco 2 500m 500ppm 1,000m 1,000ppm
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橡96-01.PDF
1 961 31 CAS 71432 C 6 H 6 78.11 1) 99 % 1. 5.5 2) 80.1 2) -11 3) 293563 3) 1.48.0% 3) d 20 0.8786 4) 2.77 ( = 1) 4) 4 13.33 kpa (100 mmhg) (26.9) 2) log Pow2.13 ( ) 5) 2.14 ( ) 6) m/z78 ( 1.0 )77 ( 0.20
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1,2,4-1,2,4-Trimethylbenzene Pseudocumene 1,3,5-1,3,5-Trimethylbenzene Mesitylene CH 3 CH 3 CH 3 CH 3 CH 3 CH 3 1,2,4-trimethylbenzene 1,3,5-trimethylbenzene CAS 95-63-6 CAS 108-67-8 C 9 H 12 C 9 H 12
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1,3-1,3- (1) 1,3-1,3- - CAS 542-75-6 C 3 H 4 Cl 2 110.97 2 1) -84 2) 108 2,3) 112 (trans-) 4) 104 (cis-) 4) 1.225 (20 ) 2) 5.2 kpa (39 mmhg) (25 ) 2) 4.5 kpa (34 mmhg) (25 ) 4) 5.7 kpa (43 mmhg) (25 )
NPE EO NPE NPE 1 NPE NPE1 EO n NPE NPEn NP 1
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