List of Applications Vitamins Carbohydrates
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- あきお にいだ
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1 Vitamins Carbohydrates APPLICATION DATA YMC APPLICATION DATA YMC Contents List of Applications Vitamins Carbohydrates Nucleic acids Amino acids, Peptides, Proteins Organic acids, Fatty acid derivatives Food additives Natural products Steroids Drugs, Metabolites Antibiotics Pesticides, Environmental The others Optical isomers Index of Analytes Nucleic acids Amino acids, Peptides, Proteins Organic acids, Fatty acid derivatives Food additives Natural products Steroids Drugs,Metabolites Antibiotics Pesticides, Environmental The others Optical isomers
2 List of Applications Vitamins Carbohydrates
3 INDEX Nucleic acids Amino acids, Peptides, Proteins Organic acids, Fatty acid derivatives 3
4 List of Applications Food additives Natural products Steroids 4
5 INDEX Drugs, Metabolites 5
6 List of Applications Antibiotics Pesticides, Environmental 6
7 INDEX The others Optical isomers 7
8 Oil-soluble vitamins. Menadione (Vitamin K3). Retinol (Vitamin A) 3. Retinol acetate 4. Menaquinone (Vitamin K) 5. -Tocopherol 6. Ergocalciferol (Vitamin D) 7. Cholecalciferol (Vitamin D3) 8. -Tocopherol (Vitamin E) 9. -Tocopherol acetate 0. Phylloquinone (Vitamin K) Vitamin A fatty acid ester. Retinol palmitate (Vitamin A palmitate) (G9045B) (G9053T) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : acetonitrile Temperature : 30 Detection : UV at 80 nm, 0.08 AUFS Injection : 5 L (0.00. mg/ml) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : cyclohexane/dichloromethane/acetic acid (00/0.5/0.5) Temperature : 30 Detection : UV at 350 nm, 0.3 AUFS Injection : 5 L (.0 mg/ml) Retinol Carotene. -Carotene. -Carotene Retinol (A970708A) (G9053Q) Column : YMC-Pack Pro C8 (5m, nm) mm I.D. Eluent : methanol/water (9/8) Temperature : 35 Detection : UV at 35 nm, 0.0 AUFS Injection : 0 L (0.5 g/ml) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : acetonitrile/methanol/thf (50/45/5) Temperature : 30 Detection : VIS at 450 nm, 0.6 AUFS Injection : 5 L (0.05 mg/ml) 8
9 - -Carotene. -Carotene - -Carotene. -Carotene (M9059A) (A97076K) Column : YMC-Pack CN (5m, nm) mm I.D. Eluent : acetonitrile/water/thf (35/35/30) Temperature : 30 Detection : VIS at 450 nm, 0.3 AUFS Injection : 7 L (0.5 mg/ml) Column : YMC-Pack ODS-AL (5m, nm) mm I.D. Eluent : methanol/chloroform (96/4) Flow rate :.5 ml/min Temperature : 35 Detection : VIS at 455 nm, 0.04 AUFS Injection : 0 L (4.0 g/ml) D Vitamin D D Vitamin D Ergocalciferol (Vitamin D) Cholecalciferol (Vitamin D3) (C970808E) (C970808H) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : hexane/-propanol (99.6/0.4) Flow rate :.6 ml/min Temperature : ambient (8 ) Detection : UV at 65 nm, 0.0 AUFS Injection : 00 L (.0 g/ml) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : hexane/-propanol (99.6/0.4) Flow rate :.6 ml/min Temperature : ambient (8 ) Detection : UV at 65 nm, 0.0 AUFS Injection : 00 L (.0 g/ml) 9
10 Vitamin D and vitamin D3 Vitamin D and vitamin D3 (P04088A) (P04089C) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : acetonitrile/water (95/5) Temperature : 40 Detection : UV at 65 nm Injection : 0 L (0.0 mg/ml) Column : YMC-Pack ODS-AL (5m, nm) mm I.D. Eluent : acetonitrile/water (95/5) Temperature : 40 Detection : UV at 65 nm Injection : 0 L (0.0 g/ml) Tocopherols. -Tocopherol. -Tocopherol 3. -Tocopherol 4. -Tocopherol Tocopherols -Tocopherol 3 -Tocopherol 4 -Tocopherol -Tocopherol (G9053S) (S97070A) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : hexane/thf/acetic acid (97/3/0.5) Temperature : 30 Detection : UV at 95 nm, 0.08 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : hexane/-propanol/acetic acid (000/6/5) Flow rate :.4 ml/min Temperature : 35 Detection : FLS at Ex 98 nm, Em 35 nm Injection : 0 L (50 g/ml) 0
11 Tocopherols. -Tocopherol. -Tocopherol 3. -Tocopherol 4. -Tocopherol Tocopherols -Tocopherol -Tocopherol 3 -Tocopherol 4 -Tocopherol (T9050A) (T9078E) mm I.D. Eluent : n-hexane/tetrahydrofuran/acetic acid/water (93/7/0.4/0.0) Temperature : 30 Detection : UV at 95 nm, 0.08 AUFS Injection : 7 L (0.5 mg/ml) mm I.D. Eluent : hexane/ethyl acetate (70/30) Temperature : 30 Detection : UV at 95 nm, 0.08 AUFS Injection : 7 L (0.5 mg/ml) Tocopherols Tocopherols -Tocopherol -Tocopherol -Tocopherol -Tocopherol 3 -Tocopherol 3 -Tocopherol 4 -Tocopherol 4 -Tocopherol Column : J'sphere ODS-M80 (4m, 8nm) mm I.D. Eluent : -propanol/water (68/3) Flow rate : 0.5 ml/min Temperature : 30 Detection : UV at 95 nm, 0.03 AUFS Injection : 7 L (0.5 mg/ml) (S93076A) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : -propanol/water (75/5) Flow rate : 0.3 ml/min Temperature : 30 Detection : UV at 95 nm, 0.08 AUFS Injection : 7 L (0.5 mg/ml) (S97A) Ref.) Y.Satomura, M. Kimura and Y. Itokawa, J.Chromatogr., 65, (99)
12 Tocopherols Tocopherol and tocopherol acetate -Tocopherol -Tocopherol 3 -Tocopherol 4 -Tocopherol -Tocopherol -Tocopherol acetate (S96C) (S97046E) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : -propanol/water (65/35) Flow rate : 0.7 ml/min Temperature : 30 Detection : UV at 95 nm, 0.04 AUFS Injection : 7 L (0.5 mg/ml) Ref.) Y.Satomura, M. Kimura and Y. Itokawa, J.Chromatogr., 65, (99) Column : YMC-Pack Pro C8 (5m, nm) mm I.D. Eluent : methanol/water (98/) Temperature : 30 Detection : UV at 84 nm, 0.5 AUFS Injection : 0 L ( mg/ml) 3 Tocopherol and tocopherol acetate K Vitamin K -Tocopherol Menaquinone (Vitamin K) -Tocopherol acetate Phylloquinone (Vitamin K) (S97046C) (A97078B) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : methanol/water (98/) Temperature : 30 Detection : UV at 84 nm, 0.5 AUFS Injection : 0 L ( mg/ml) 3 Column : YMC-Pack Pro C8 (5m, nm) mm I.D. Eluent : methanol/ethanol (5/) Flow rate : 0.8 ml/min Temperature : 40 Detection : FLS at Ex 30 nm, Em 430 nm reduction column (platinum black, 0 x 4.0 mmi.d.) Injection : 0 L (00 ng/ml)
13 Water-soluble vitamins. L-Ascorbic acid (Vitamin C). Nicotinic acid 3. Pyridoxine HCl (Vitamin B6) 4. Nicotinamide 5. Thiamine HCl (Vitamin B) 6. Folic acid 7. Cyanocobalamin (Vitamin B) 8. Riboflavin (Vitamin B) Water-soluble vitamins. Nicotinic acid. Pantothenic acid (Na salt) 3. Pyridoxine HCl (Vitamin B6) 4. Nicotinamide 5. Thiamine HCl (Vitamin B) (G9045A) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : A)0mM KHPO4 - KHPO4 (ph 6.6) B)0mM KHPO4 - KHPO4 (ph 6.6)/acetonitrile (80/0) 0%B (0-5min), 0-00%B (5-0min, linear), 00%B (0-5min) Temperature : 30 Detection : UV at 54 nm, 0.3 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluent : 0mM NaHPO4 - NaHPO4 (ph 6.5) Temperature : 30 Detection : UV at 0 nm, 0.08 AUFS Injection : 5 L ( mg/ml) (G9053O) Water-soluble vitamins A drink including vitamins. L-Ascorbic acid (Vitamin C). Pyridoxine HCl (Vitamin B6) 3. Nicotinamide 4. Panthenol 5. Caffeine 6. Flavin mononucleotide sodium salt (Vitamin B). L-Ascorbic acid (Vitamin C). Pyridoxine HCl (Vitamin B6) 3. Nicotinamide 4. Panthenol 5. Caffeine 6. Flavin mononucleotide sodium salt (Vitamin B) (F00004B) (F00004A) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : A)50mM KHPO4-H3PO4(pH3.5) B)50mM KHPO4-H3PO4(pH3.5)/acetonitrile (80/0) 0-60%B(0-0min), 60%B(0-30min) Temperature : 30 Detection : UV at 0 nm, 0.3AUFS Injection : 5 L ( mg/ml) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : A)50mM KHPO4-H3PO4(pH3.5) B)50mM KHPO4-H3PO4(pH3.5)/acetonitrile (80/0) 0-60%B(0-0min), 60%B(0-30min) Temperature : 30 Detection : UV at 0 nm, 0.3AUFS Injection : 5 L Sample : 5 times dilution with 5% metaphosphoric acid 3
14 Water-soluble vitamins. Thiamine HCl (Vitamin B). Pyridoxine HCl (Vitamin B6) 3. Nicotinamide 4. Caffeine 5. Flavin mononucleotide sodium salt (Vitamin B) A drink including vitamins. Thiamine HCl (Vitamin B). Pyridoxine HCl (Vitamin B6) 3. Nicotinamide 4. Caffeine 5. Flavin mononucleotide sodium salt (Vitamin B) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : A)50mM KHPO4-H3PO4(pH3.5) B)50mM KHPO4-H3PO4(pH3.5)/acetonitrile (80/0) 0-90%B(0-0min), 90%B(0-30min) Temperature : 30 Detection : UV at 54 nm, 0.3AUFS Injection : 5 L ( mg/ml) (F000A) (F000B) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : A)50mM KHPO4-H3PO4(pH3.5) B)50mM KHPO4-H3PO4(pH3.5)/acetonitrile (80/0) 0-90%B(0-0min), 90%B(0-30min) Temperature : 30 Detection : UV at 54 nm, 0.3AUFS Injection : 5 L Sample : 5 times dilution with water Water-soluble vitamins.p-aminobenzoic acid (PABA).Biotin (Vitamin H) 3.Riboflavin (Vitamin B) 4.Cyanocobalamin (Vitamin B) Water-soluble vitamins.p-aminobenzoic acid (PABA).Biotin (Vitamin H) 3.Cyanocobalamin (Vitamin B) 4.Riboflavin (Vitamin B) (M90B) (M90A) Column : YMC-Pack Ph (5m, nm) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (0/90) Temperature : 37 Detection : UV at 0 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (0/90) Temperature : 37 Detection : UV at 0 nm, 0.6 AUFS Injection : 0 L ( mg/ml) 4
15 Water-soluble vitamins.p-aminobenzoic acid (PABA).Biotin (Vitamin H) 3.Riboflavin (Vitamin B) 4.Cyanocobalamin (Vitamin B) Water-soluble vitamins.p-aminobenzoic acid (PABA).Biotin (Vitamin H) 3.Riboflavin (Vitamin B) 4.Cyanocobalamin (Vitamin B) (M90C) (M90D) Column : YMC-Pack TMS (5m, nm) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (0/90) Temperature : 37 Detection : UV at 0 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack C4 (5m, nm) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (0/90) Temperature : 37 Detection : UV at 0 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Water-soluble vitamins.l-ascorbic acid (Vitamin C).Orotic acid (Vitamin B3) 3.Pyrroloquinoline quinone (PQQ) 4.Pyridoxine HCl (Vitamin B6) 5.Nicotinamide Water-soluble vitamins.l-ascorbic acid (Vitamin C).Orotic acid (Vitamin B3) 3.Pyrroloquinoline quinone (PQQ) 4.Pyridoxine HCl (Vitamin B6) 5.Nicotinamide (M9007B) (M9007A) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluent : 00mM CH3COOH/00mM CH3COONH4 (30/70, ph 5.) Temperature : 37 Detection : UV at 54 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack TMS (5m, nm) mm I.D. Eluent : 00mM CH3COOH/00mM CH3COONH4 (30/70, ph 5.) Temperature : 37 Detection : UV at 54 nm, 0.6 AUFS Injection : 0 L ( mg/ml) 5
16 Water-soluble vitamins.nicotinic acid.erythorbic acid 3.L-Ascorbic acid Water-soluble vitamins.nicotinic acid.erythorbic acid 3.L-Ascorbic acid (T9055A) (T9055B) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (70/30) Temperature : 40 Detection : UV at 50 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (70/30) Temperature : 40 Detection : UV at 50 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Water-soluble vitamins.pyridoxine HCl.Nicotinamide 3.Benfotiamine 4.Cyanocobalamin 5.Riboflavin Water-soluble vitamins Xanthine(I.S.) Pyridoxal HCl 3 Pyridoxine HCl 4 Nicotinamide (S9307E) (S9609B) Column : J'sphere ODS-H80 (4m, 8nm) mm I.D. Eluent : acetonitrile/50mm (NH4)HPO4 (0/90) Temperature : 30 Detection : UV at 54 nm, 0.3 AUFS Injection : 5 L ( mg/ml) Column : YMC-Pack Pro C8 (5m, nm) mm I.D. Eluent : 0mM KHPO4 - KHPO4 (ph 6.9) Temperature : 37 Detection : UV at 54 nm, 0.3 AUFS Injection : 5 L ( mg/ml) 6
17 Water-soluble vitamins Allantoin and water-soluble vitamins (S005A) (S97D) Column : Hydrosphere C8 (3m, nm) 50.0 mm I.D. Eluent : 0mM CH3COONH4 Flow rate : 0. ml/min Temperature : 37 Detection : UV at 54 nm, 0.8 AUFS Injection : L (0.00. mg/ml) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : 50mM NH4HPO4 - H3PO4 (ph.5) / acetonitrile (0/80) Temperature : 37 Detection : UV at 0 nm, AUFS Injection : 8 L ( mg/ml) Urea, allantoin and water-soluble vitamins B Thiamine and its modified compounds 6. CH 3 OH HOCH C CH CONH(CH ) 3 OH CH 3 Panthenol (Pantothenyl alcohol). COOH N Nicotinic acid 3. H NCONH Urea 5. CH OH HCOH O O HO OH L-Ascorbic acid (Vitamin C) 6. CH OH HO CH OH CH 3 N HCl Pyridoxine HCl (Vitamin B6) 3 Thiamine HCl Benfotiamine Dicethiamine HCl H NCONH H N O NH O Allantoin 4 Bisbentiamine min (S9400D) mm I.D. Eluent : 50mM NH4HPO4-H3PO4 (ph.8)/acetonitrile (0/80) Temperature : 37 Detection : UV at 0 nm, 0.6 AUFS Injection : 0 L ( mg/ml) (J03064B) Column : J'sphere ODS-H80 (4m, 8nm) mm I.D. Eluent : A)50mM (NH4)HPO4 B)methanol/50mM (NH4)HPO4 (60/40) 0-00%B (0-5min, linear), 00%B (5-30min) Temperature : 37 Detection : UV at 60 nm, 0.6 AUFS Injection : 0 L (0.0. mg/ml) 7
18 Riboflavin and related compounds Nicotinic acid and derivatives 3 H3C H3C H3C H3C OH OH OH CHCH CH CH CHO N N O NH O N OH OH OH CHCH CH CH CHO N O P O ONa O P ONa N O CH N O NH N N OH OH Flavin adenine dinucleotide disodium O P ONa OH N O N NH O Flavin sodium phosphate (Flavin mononucleotide sodium salt). Nicotinamide adenine dinucleotide phosphate oxidized form (NADP). Nicotinic acid 3. Nicotinamide adenine dinucleotide phosphate reduced form (NADPH) 4. Nicotinamide 5. -Nicotinamide adenine dinucleotide (NAD) 6. -Nicotinamide adenine dinucleotide reduced form (NADH) 3 H3C OH OH OH CHCH CH CH CHOH N O N H3C N Riboflavin NH O min (S000803B) (F000707B) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 50mM KHPO4 - KHPO4 (ph 5.9) / acetonitrile (90/0) Temperature : 37 Detection : UV at 60 nm, 0.3 AUFS Injection : 0 L (0. mg/ml) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 0mM KHPO4-KHPO4(pH6.9)/acetonitrile (99/) Temperature : 37 Detection : UV at 60 nm, 0.3 AUFS Injection : 6 L ( mg/ml) Pantothenyl alcohol A Coenzyme A and derivatives. Malonyl-CoA Pantothenyl alcohol Coenzyme A glutathione disulfide Coenzyme A Methylmalonyl-CoA 5. Resorcinol(I.S.) 6. Sccinyl-CoA 3-Hydroxy-3-methylglutaryl- CoA (HMG-CoA) 7. Acetoacetyl-CoA 8. Acetyl-CoA 9. Coenzyme A oxidized 0. Propionyl-CoA Courtesy of Dr. Takamura, Ibaraki University (S940630E) Column : YMC-Pack Pro C8 (5m, nm) mm I.D. Eluent : acetonitrile/water (5/95) Temperature : 37 Detection : UV at 0 nm, 0.3 AUFS Injection : 5 L ( mg/ml) 8 (S969B) Column : J'sphere ODS-M80 (4m, 8nm) mm I.D. Eluent : A)methanol/50mM KHPO4 (0/90) B)methanol/50mM KHPO4 (30/70) 0%B (0-5min), 0-00%B (5-30min) Flow rate : 0.7 ml/min Temperature : 37 Detection : UV at 60 nm, 0.06 AUFS Injection : 0 L (6.7 nmol/ml)
19 L- L-Ascorbic acid and erythorbic acid. Erythorbic acid. L-Ascorbic acid (Vitamin C) L- L-Ascorbic acid and erythorbic acid. L-Ascorbic acid (Vitamin C). Erythorbic acid mm I.D. Eluent : acetonitrile/50mm NH4HPO4 (70/30) Temperature : 30 Detection : UV at 50 nm, 0.6 AUFS Injection : 0 L (0. mg/ml) (T9045A) (G9053N) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluent : 0mM CH3COONH4 in 5mM tetrabutylammonium bromide Temperature : 30 Detection : UV at 50 nm, 0.08 AUFS Injection : 5 L (0.05 mg/ml) L-,4-DNPH,4-Dinitrophenylhydrazone of L-ascorbic acid. L-Ascorbic acid,4-dnph (C970808K) Column : YMC-Pack SIL (5m, nm) mm I.D. Eluent : hexane/ethyl acetate/-propanol/acetic acid (40/30//) Flow rate :.5 ml/min Temperature : 35 Detection : VIS at 540 nm, 0.0 AUFS Injection : 0 L (0 g/ml) 9
20 Monosaccharides and disaccharides Monosaccharides and disaccharides.fructose.glucose 3.Sucrose 4.Maltose 5.Lactose.Fructose.Glucose 3.Sucrose 4.Maltose 5.Lactose (T9076A) (T9073A) Column : YMC-Pack Polyamine mm I.D. Eluent : acetonitrile/water (75/5) Temperature : 6 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L ( mg/ml) mm I.D. Eluent : ethanol/ethyl acetate/acetonitrile/water (30/40/5/5) Temperature : 6 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L ( mg/ml) Monosaccharides and disaccharides Monosaccharides.Fructose.Glucose 3.Sucrose 4.Maltose 5.Lactose.Rhamnose.Fucose 3.Xylose 4.Fructose 5.Mannose 6.Glucose 7.Galactose mm I.D. Eluent : ethanol/ethyl acetate/acetonitrile/water (30/40/5/5) Temperature : 35 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L ( mg/ml) (T9078E) mm I.D. Eluent : ethanol/ethyl acetate/acetonitrile/water (30/30/3/7) Temperature : 6 Detection : RI, 6 x 0-6 RIU/FS Injection : 5 L ( mg/ml) (T9078D) 0
21 Unsaturated chondro-disaccharides.di-0s.di-6s 3.Di-4S 4.Di-diSD 5.Di-diSE 6.Di-triS Sugar alcohols. Glycerol. Erythritol 3. Xylitol 4. Sorbitol 5. Maltitol 6. Lactitol min (T9090A) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : A)0.0M NH4HPO4 - (NH4)HPO4(pH 6.7) B) 0.5M NH4HPO4 - (NH4)HPO4(pH 6.7) 0%B (0-5min), 0-00%B (5-30min,linear), 00%B (30-40min) Temperature : 37 Detection : UV at 3 nm, 0.3 AUFS Injection : 9 L (0.0.4 mg/ml) mm I.D. Eluent : acetonitrile/water (75/5) Temperature : 5 Detection : RI, RIU/FS Injection : 5 L (5.0 mg/ml) (F030603A) Sugar alcohols Palatinose and Palatinit. Glycerol. Erythritol 3. Xylitol 4. Ribitol 5. Arabitol 6. Sorbitol 7. Mannitol 8. Maltitol 9. Inositol. Palatinose. Palatinit ( * ) (Isomalt) min (*)Mixture of 6-O--D-Glucopyranosyl-D-sorbitol and -O--D-Glucopyranosyl-D-mannitol (T9078B) (F03066B) mm I.D. Eluent : ethanol/ethyl acetate/acetonitrile/water (30/30/5/5) Temperature : 30 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L (.73.3 mg/ml) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : 5 Detection : RI, 64 x 0-6 RIU/FS Injection : 5 L (5.0 mg/ml)
22 Sugars and sweeteners Sugars in hard candy A) Standard 3 4. Sucralose. Erythritol 3. Xylitol 4. Fructose 5. Sorbitol 6. Glucose 7. Sucrose 8. Palatinose 9. Maltitol 0. Maltose. Lactitol F03067F B) Hard candy (Sample KM) 7 40 min. Sucralose. Erythritol 3. Xylitol 4. Fructose 5. Sorbitol 6. Glucose 7. Sucrose 8. Palatinose 9. Maltitol 0. Maltose. Lactitol F03068A 40 min min (F03068A) mm I.D. Eluent : acetonitrile/water (75/5) Temperature : 5 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L (5.0 mg/ml) (F03063C) mm I.D. Eluent : acetonitrile/water (75/5) Temperature : 5 Detection : RI, 3 x 0-6 RIU/FS Injection Sample : 5 L : A) 5 mg/ml B) 50 mg/ml (50% ethanol solution of candy) Oligosaccharides Oligosaccharides.... (A97065G) (A97070G) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (6 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (4.0 mg/ml) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (7 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (4.0 mg/ml)
23 Fructooligosaccharides Oligosaccharides. FrufGlc (Sucrose). FrufFrufGlc (-Kestose) 3. Fruf[Fruf]Glc (Nystose) 4. Fruf[Fruf]3Glc (-Fructofuranosyl-D-nystose) min (F00075B) (A97067F) Column : Hydrosphere C8 (5m, nm) mm I.D. Temperature : 30 Detection : RI, 64 x 0-6 RIU/FS Injection : 5L (0 mg/ml) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (6 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (4.0 mg/ml) Oligosaccharides of soft drink Oligosaccharides... (Lactosyl fructoside) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (7 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L Sample : 0 times dilution with water (A970630C) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (6 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (4.0 mg/ml) (A97068H) 3
24 Oligosaccharides Maltooligosaccharides(GG7). (Lactosyl fructoside). Glucose (G). Maltose (G) 3. Maltotriose (G3) 4. Maltotetraose (G4) 5. Maltopentaose (G5) 6. Maltohexaose (G6) 7. Maltoheptaose (G7) min (A970703A) (F03060A) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : acetonitrile/water (70/30) Temperature : ambient (7 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (4.0 mg/ml) mm I.D. Eluent : acetonitrile/water (60/40) Temperature : 5 Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (.4 mg/ml) Maltooligosaccharides(GG7) Maltooligosaccharides(GG7). Glucose (G). Maltose (G) 3. Maltotriose (G3) 4. Maltotetraose (G4) 5. Maltopentaose (G5) 6. Maltohexaose (G6) 7. Maltoheptaose (G7).Glucose(G).Maltose(G) 3.Maltotriose (G3) 4.Maltotetraose (G4) 5.Maltopentaose (G5) 6.Maltohexaose (G6) 7.Maltoheptaose (G7) (F0006D) Courtesy of Dr.Kimura and Dr.Chiba, Hokkaido University, Japan (Y9050A) Column : Hydrosphere C8 (5m, nm) mm I.D. Temperature : ambient (6) Detection : RI, 64 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Column : YMC-Pack ODS-AQ (5m, nm) mm I.D. Flow rate : 3.0 ml/min Temperature : ambient (5 ) Detection : RI 4
25 Maltooligosaccharides(GG5).Maltoundecaose (G).Maltododecaose (G) 3.Maltotridecaose (G3) 4.Maltotetradecaose (G4) 5.Maltopentadecaose (G5) Maltooligosaccharides(GG5).Maltoundecaose (G).Maltododecaose (G) 3.Maltotridecaose (G3) 4.Maltotetradecaose (G4) 5.Maltopentadecaose (G5) (T9078A) (M90604K) mm I.D. Eluent : acetonitrile/water (55/45) Temperature : 6 Detection : RI, 3 x 0-6 RIU/FS Injection Sample : 00 L ( mg/ml) : Manufactured by Nakano Vinegar Co., Ltd., Nakano Central Research Institute Column : YMC-Pack ODS-A (5m, 30nm) mm I.D. Temperature : 0 Detection : RI, 8 x 0-6 RIU/FS Injection : 5 L ( mg/ml) Sample : Manufactured by Nakano Vinegar Co., Ltd., Nakano Central Research Institute Maltooligosaccharides(GG5).Maltoundecaose (G).Maltododecaose (G) 3.Maltotridecaose (G3) 4.Maltotetradecaose (G4) 5.Maltopentadecaose (G5) Maltooligosaccharides(GG5).Maltoundecaose (G).Maltododecaose (G) 3.Maltotridecaose (G3) 4.Maltotetradecaose (G4) 5.Maltopentadecaose (G5) (M90604L) (M90604M) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Temperature : 0 Detection : RI, 8 x 0-6 RIU/FS Injection : 5 L ( mg/ml) Sample : Manufactured by Nakano Vinegar Co., Ltd., Nakano Central Research Institute Column : YMC-Pack ODS-AQ (5m, nm) mm I.D. Eluent : methanol/water (5/995) Temperature : 37 Detection : RI, 8 x 0-6 RIU/FS Injection Sample : 5 L ( mg/ml) : Manufactured by Nakano Vinegar Co., Ltd., Nakano Central Research Institute 5
26 Maltooligosaccharides(GG5).Maltoundecaose (G).Maltododecaose (G) 3.Maltotridecaose (G3) 4.Maltotetradecaose (G4) 5.Maltopentadecaose (G5) Maltooligosaccharides(GG5).Maltopentadecaose (G5).Maltotridecaose (G3) 3.Maltoundecaose (G) 4.Maltoheptaose (G7 ) 5.Maltopentaose (G5 ) 6.Maltotriose (G3 ) 7.Glucose (G ) (M90604N) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : methanol/water (5/995) Temperature : 37 Detection : RI, 8 x 0-6 RIU/FS Injection Sample : 5 L ( mg/ml) : Manufactured by Nakano Vinegar Co., Ltd., Nakano Central Research Institute Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 64 x 0-6 RIU/FS Injection : 60 L ( mg/ml) (G96E) Maltooligosaccharides(GG5).Maltopentadecaose (G5).Maltotridecaose (G3) 3.Maltoundecaose (G) 4.Maltoheptaose (G7 ) 5.Maltopentaose (G5 ) 6.Maltotriose (G3 ) 7.Glucose (G ) Cyclodextrins (G96F) (F03067B) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 64 x 0-6 RIU/FS Injection : 60 L ( mg/ml) mm I.D. Eluent : acetonitrile/water (60/40) Temperature : 5 Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L ( mg/ml) 6
27 Cyclodextrins.-Cyclodextrin.-Cyclodextrin 3.-Cyclodextrin Cyclodextrins.-Cyclodextrin.-Cyclodextrin 3.-Cyclodextrin (M9047B) (M9047A) Column : YMC-Pack ODS-AQ (5m, nm) mm I.D. Eluent : methanol/water (7/93) Temperature : 30 Detection : RI, 3 x 0-6 RIU/FS Injection : 8 L (55 mg/ml) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : methanol/water (7/93) Temperature : 30 Detection : RI, 3 x 0-6 RIU/FS Injection : 8 L (55 mg/ml) Cyclodextrins.-Cyclodextrin.-Cyclodextrin 3.-Cyclodextrin Cyclodextrins.-Cyclodextrin.-Cyclodextrin 3.-Cyclodextrin 4.O-Dimethyl- -cyclodextrin 5.O-Trimethyl--cyclodextrin (M9043A) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 30 L (.67 mg/ml) (G96I) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : A)water B)methanol %B (0-5min), -30%B (5-5min, linear), 30-00%B (5-0min, linear), 00%B (0-30min) Temperature : 30 Detection :Evaporative Mass Analyzer (ACS Ltd.) Temp 50 Time Constant 5 PMT 3 Attenuation 6 Pressure 0 psi Injection : 00 L (.55 mg/ml) 7
28 Cyclodextrins N-Acetyl-chitooligosaccharides.O-Dimethyl- -cyclodextrin.o-trimethyl--cyclodextrin. N-Acetylglucosamine. N-Acetyl-chitobiose 3. N-Acetyl-chitotriose 4. N-Acetyl-chitotetraose 5. N-Acetyl-chitopentaose min (M9047C) (F03060A) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : methanol/water (80/0) Temperature : 30 Detection : RI, 3 x 0-6 RIU/FS Injection : 5 L (50 mg/ml) mm I.D. Eluent : acetonitrile/water (65/35) Temperature : 5 Detection : RI, 6 x 0-6 RIU/FS Injection : 5 L (0. mg/ml) (PA) Pyridylamino(PA)-Sugar chains (PA) Pyridylamino(PA)-Sugar chains.pa-sugar Chain 04.PA-Sugar Chain 04.PA-Sugar Chain 00.PA-Sugar Chain 00 3.PA-Sugar Chain 00 3.PA-Sugar Chain 00 (G90607C) Column : YMC-Pack ODS-AQ (5m, nm) mm I.D. Eluent : methanol/0mm NH4HPO4 (5/95) Temperature : 37 Detection : FLS at Ex.30 nm, Em. 400 nm, 8 mv/fs Injection : L (3.3 pmol/ml) Sample : PA-Sugar Chain Series, manufactured by TAKARA SHUZO CO., LTD. (G90607B) Column : YMC-Pack ODS-A (5m, 30nm) mm I.D. Eluent : methanol/0mm NH4HPO4 (5/95) Temperature : 37 Detection : FLS at Ex.30 nm, Em. 400 nm, 6 mv/fs Injection : L (3.3 pmol/ml) Sample : PA-Sugar Chain Series, manufactured by TAKARA SHUZO CO., LTD. 8
29 (PA) Pyridylamino(PA)-Sugar chains.pa-sugar Chain 04.PA-Sugar Chain 00 (PA) Pyridylamino(PA)-Sugar chains.pa-sugar Chain 04.PA-Sugar Chain 00 3.PA-Sugar Chain 00 3.PA-Sugar Chain 00 (G90607A) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : methanol/0mm NH4HPO4 (5/95) Temperature : 37 Detection : FLS at Ex.30 nm, Em. 400 nm, 6 mv/fs Injection : L (3.3 pmol/ml) Sample : PA-Sugar Chain Series, manufactured by TAKARA SHUZO CO., LTD. (G9060B) mm I.D. Eluent : acetonitrile/0mm NH4HPO4 (60/40) Temperature : 37 Detection : FLS at Ex. 30 nm, Em. 400 nm, 8 mv/fs Injection : 5 L (3.3 pmol/ml) Sample : PA-Sugar Chain Series, manufactured by TAKARA SHUZO CO., LTD. (PA) Pyridylamino(PA)-Sugar chains.pa-sugar Chain 04 Polydextrose.Polydextrose II.PA-Sugar Chain 00 3.PA-Sugar Chain 00 (G9060A) mm I.D. Eluent : methanol/0mm NH4HPO4 (80/0) Temperature : 37 Detection : FLS at Ex.30 nm, Em. 400 nm, 4 mv/fs Injection : 3 L (3.3 pmol/ml) Sample : PA-Sugar Chain Series, manufactured by TAKARA SHUZO CO., LTD. Column : YMC-Pack Diol mm I.D. Temperature : ambient (5 ) Detection : RI, 64 x 0-6 RIU/FS Injection : 40 L (5 mg/ml) (G96A) 9
30 Pullulans.Pullulan P-800 (MW 853,000).Pullulan P-50 (MW 48,000) 3.Pullulan P-0 (MW 3,700) 4.Pullulan P-5 (MW 5,800) Pullulans.Pullulan P-800 (MW 853,000).Pullulan P-50 (MW 48,000) 3.Pullulan P-0 (MW 3,700) 4.Pullulan P-5 (MW 5,800) (G96A) (G96B) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 80 L (0.5 mg/ml) Sample : Shodex STANDARD P-8, manufactured by SHOWA DENKO K.K. Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 80 L (0.5 mg/ml) Sample : Shodex STANDARD P-8, manufactured by SHOWA DENKO K.K. Pullulans.Pullulan P-800 (MW 853,000).Pullulan P-50 (MW 48,000) 3.Pullulan P-0 (MW 3,700) 4.Pullulan P-5 (MW 5,800) Pullulans.Pullulan P-800 (MW 853,000).Pullulan P-50 (MW 48,000) 3.Pullulan P-0 (MW 3,700) 4.Pullulan P-5 (MW 5,800) (G96C) (G96D) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 80 L (0.5 mg/ml) Sample : Shodex STANDARD P-8, manufactured by SHOWA DENKO K.K. Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 80 L (0.5 mg/ml) Sample : Shodex STANDARD P-8, manufactured by SHOWA DENKO K.K. 30
31 Chondroitin.Chondroitin, Na salt Chondroitin sulfate A.Chondroitin sulfate A, Na salt (G9007A) (G9007C) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Chondroitin sulfate B.Chondroitin sulfate B, Na salt Chondroitin sulfate C.Chondroitin sulfate C, Na salt (G9007E) (G9007D) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 6 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) 3
32 Hyaluronic acid.hyaluronic acid, Na salt Heparin.Heparin, Na salt (G9007B) (G9007I) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 8 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Heparan sulfate.heparan sulfate, Na salt Keratan sulfate.keratan sulfate, Na salt (G9007F) (G9007G) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) 3
33 Keratan polysulfate.keratan polysulfate, Na salt Column : YMC-Pack Diol mm I.D. Temperature : ambient (4 ) Detection : RI, 3 x 0-6 RIU/FS Injection : 0 L (5.0 mg/ml) (G9007H) 33
34 3 Nucleosides and bases.cytocine.cytidine 3.Uracil 4.Deoxycytidine 5.Guanine 6.Adenine 7.Hypoxanthine 8.Uridine 9.Xanthine 0.Thymine.Inosine.Guanosine 3.Deoxyinosine 4.Deoxyguanosine 5.Xanthosine 6.Thymidine 7.Adenosine 8.Deoxyadenosine Nucleosides and bases.cytocine.cytidine 3.Uracil 4.Deoxycytidine 5.Guanine 6.Adenine 7.Hypoxanthine 8.Uridine 9.Xanthine 0.Thymine.Inosine.Guanosine 3.Deoxyinosine 4.Deoxyguanosine 5.Xanthosine 6.Thymidine 7.Adenosine 8.Deoxyadenosine (T90404C) (T90404A) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : A)0mM CH3COOH - CH3COONH4 (ph 3.5) B)0mM CH3COOH - CH3COONH4 (ph 3.5)/methanol (90/0) 30%B (0-5min), 30-00%B (5-3min,linear), 00%B (3-40min) Flow rate : 0.7 ml/min Temperature : 30 Detection : UV at 60 nm, 0.08 AUFS Injection : L ( mg/ml) Column : YMC-Pack ODS-AQ (5m, nm) mm I.D. Eluent : A)0mM CH3COOH - CH3COONH4 (ph 3.5) B)0mM CH3COOH - CH3COONH4 (ph 3.5)/methanol (90/0) 30%B (0-5min), 30-00%B (5-3min,linear), 00%B (3-40min) Flow rate : 0.7 ml/min Temperature : 30 Detection : UV at 60 nm, 0.08 AUFS Injection : L ( mg/ml) Nucleic acid bases Nucleic acid bases NH N O N H Cytosine. NH N F O N H 5-Fluorocytosine 3. O HN O N H Uracil 4. O HN F O N H 5-Fluorouracil 5. HN HN O N N NH Guanine 6. O HN CH3 O N H Thymine 7. NH N N N NH Adenine min (J0009E) (S9909A) Column : Hydrosphere C8 (3m, nm) mm I.D. Eluent : 0mM KHPO4 - KHPO4 (ph 6.9) Temperature : 37 Detection : UV at 54 nm, 0.8 AUFS Injection : 0 L ( mg/ml) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 0mM KHPO4 - KHPO4 (ph 6.9) Temperature : 37 Detection : UV at 54 nm, AUFS Injection : 8L ( mg/ml) 34
35 3 Orotic acid Nucleosides (A0007A) (A00080B) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 0mM H3PO4 Temperature : 37 Detection : UV at 54 nm, 0.56 AUFS Injection : 0L ( mg/ml) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 0mM NH4HPO4 - H3PO4 (ph 3.5) / methanol (9/8) Temperature : 30 Detection : UV at 60 nm, AUFS Injection : 5 L (55 g/ml) Nucleotides. 5'-CMP. 5'-UMP 3. 5'-dCMP 4. 5'-CDP 5. 5'-GMP 6. 5'-UDP 7. 5'-IMP 8. 5'-CTP 9. 5'-UTP 0. 5'-GDP. 5'-TMP. 5'-AMP 3. 5'-dGMP 4. 5'-GTP 5. 5'-TDP 6. 5'-ADP 7. 5'-TTP 8. 5'-dAMP 9. 5'-ATP Nucleotides '-UTP. 5'-UDP 3. 5'-CMP 4. 5'-UMP 5. 5'-dCMP 6. 5'-GMP 7. 5'-ATP 8. 5'-IMP 9. 5'-ADP 0. 5'-TMP. 5'-AMP min (T9044A) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluen : A) 0.M TEAA* (ph6.6) B) 0.M TEAA (ph6.6)/acetonitrile (95/5) 4%B (0-0min), 4-00%B (0-35min, linear), 00%B (35-50min) Temperature : 30 Detection : UV at 60 nm, 0.6 AUFS Injection : 4 L ( mg/ml) * TEAA:triethylamine-acetic acid Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 00mM KHPO4 - KHPO4 (ph 5.5) Temperature : 30 Detection : UV at 60 nm, 0.56 AUFS Injection : 0 L ( mg/ml) (A0009A) 35
36 3 Nucleotides. 5'-CMP. 5'-UMP 3. 5'-GMP 4. 5'-IMP 5. 5'-TMP 6. 5'-AMP Nucleotides. 5'-CMP. 5'-AMP 3. 5'-UMP 4. 5'-IMP 5. 5'-GMP (A0009B) (T9055C) Column : Hydrosphere C8 (5m, nm) mm I.D. Eluent : 00mM KHPO4 Temperature : 30 Detection : UV at 60 nm, 0.56 AUFS Injection : 0L (0.0.3 mg/ml) mm I.D. Eluent : 50mM KHPO4 - H3PO4 (ph 3.5) Temperature : 40 Detection : UV at 60 nm, 0.6 AUFS Injection : 0 L ( mg/ml) Nucleotides. 5'-CMP. 5'-AMP 3. 5'-UMP 4. 5'-IMP 5. 5'-GMP Oligonucleotides.c-Ha-ras/ (0mer) GTGGGCGCC-AGC-GGTGTGGG Ser.c-Ha-ras/ (0mer) GTGGGCGCC-GCC-GGTGTGGG Ala 3.c-Ha-ras/ (0mer) GTGGGCGCC-GAC-GGTGTGGG Asp 4.c-Ha-ras/ (0mer) GTGGGCGCC-GTC-GGTGTGGG Val 5.c-Ha-ras/ (0mer) GTGGGCGCC-CGC-GGTGTGGG Arg (G9060C) Column : YMC-Pack NH (5m, nm) mm I.D. Eluent : 50mM KHPO4 - H3PO4 (ph 3.5) Temperature : 40 Detection : UV at 60 nm, 0.6 AUFS Injection : 0 L ( mg/ml) 36 (T9055D) Column : YMC-Pack ODS-A (5m, 30nm) mm I.D. Eluent : A)00mM triethylamine - acetic acid (ph 6.5)/acetonitrile (94/6) B)00mM triethylamine - acetic acid (ph 6.5)/acetonitrile (85/5) 0-00%B (0-5min,linear) Temperature : 30 Detection : UV at 60 nm,0.0 AUFS Injection : 5 L (.0 pmol/l ) Sample : TAKARA ras Gene Probe set, manufacutured by TAKARA SHUZO CO., LTD.
37 3 poly(a) Poly(A) Sugar nucleotides.cdp-d-glucose.udp-d-glucose 3.UDP-N-acetyl-D-glucosamine 4.GDP-D-mannose 5.ADP-D-glucose Courtesy of Dr.Y.Baba, Kobe Women's College of Pharmacy (Y90608A) Column : YMC-Pack ODS-AM (5m, nm) mm I.D. Eluent : A)0.M phosophate buffer (ph 7) B)0.M phosophate buffer (ph 7) / acetonitrile (75/5) 0-7%B (0-5min), 7-35%B (5-90min) Temperature : ambient Detection : UV at 60 nm Injection : 0 L Sample : Poly(A) Column : YMC-Pack Ph (5m, nm) mm I.D. Eluent : 00mM TEAA ) (ph 6.0) Temperature : 37 Detection : UV at 60 nm, 0.6 AUFS Injection : 5 L ( mg/ml) ) TEAA: triethylamine-acetic acid (T906D) Sugar nucleotides.cdp-d-glucose.udp-d-glucose 3.UDP-N-acetyl-D-glucosamine 4.GDP-D-mannose 5.ADP-D-glucose Sugar nucleotides.cdp-d-glucose.udp-d-glucose 3.UDP-N-acetyl-D-glucosamine 4.GDP-D-mannose 5.ADP-D-glucose (T906B) (T906E) Column : YMC-Pack ODS-A (5m, nm) mm I.D. Eluent : 0mM TEAA ) (ph 5.7)/acetonitrile (99/) Temperature : 37 Detection : UV at 60 nm, 0.6 AUFS Injection : 5 L ( mg/ml) ) TEAA: triethylamine-acetic acid Column : YMC-Pack ODS-A (5m, 30nm) mm I.D. Eluent : 00mM TEAA ) (ph 6.0) Temperature : 37 Detection : UV at 60 nm, 0.6 AUFS Injection : 5 L ( mg/ml) ) TEAA: triethylamine-acetic acid 37
38 3 pbr3msp I Plasmid pbr3 restriction fragments.plasmid pbr3 cleaved with restriction endonuclease Msp (G9009B) Column : YMC-Pack Diol Diol mm I.D. Eluent : 0.M KHPO4 - KHPO4 (ph 7.0) containing 0.M NaCl Flow rate : 0.7 ml/min Temperature : ambient (6 ) Detection : UV at 60 nm, 0.0 AUFS Injection : 3 L (0.49 mg/ml) Sample : Plasmid pbr3 cleaved with restriction endonuclease Msp 38
YMC APPLICATION DATA Contents List of Applications Vitamins Carbohydrates Nucleic acids Amino acids, Peptides, Proteins Organic acids, Fatty acid deri
YMC APPLICATION DATA Contents List of Applications Vitamins Carbohydrates Nucleic acids Amino acids, Peptides, Proteins Organic acids, Fatty acid derivatives Food additives Natural products Steroids Drugs,
MC iosep ro duc CONTENTS CO NTENTS 7
PB-9 Proteins, Peptides & Nucleic acids http://www.ymc.co.jp Ion Ex change Chr omat atog ogra raph phy Size Exclusion Chr omat ography Re verseded Phase Chr om at ogra phy Normal Phase Chr hrom omat og
Agilent Infinity ELSD ELSD ( ) ( ºC ) W x D x H mm LED ELSD ELSD ELSD UV UV LC/MS RSD % Column: Agilent Pursuit C8, x.6 mm, µm Eluent: Water: Acetonit
Agilent Infinity ELSD Agilent 6 Infinity ELSD Agilent 9 Infinity ELSD 6 8 ELSD 9 LC/MS ELSD Agilent Infinity ELSD ELSD ( ) ( ºC ) W x D x H mm LED ELSD ELSD ELSD UV UV LC/MS RSD % Column: Agilent Pursuit
COSMOSIL.indd
Column: 5C 18 -MS-II Column size: 4.6mmI.D.-150mm Mobile phase: Methanol/ H 2 = 60/40 Detection: UV254nm Sample: 1; Acetophenone (0.05μg) 2; Methyl Benzoate (0.5μg) 3; Benzene (2.0μg) 4; Toluene (2.0μg)
Adenosine Triphosphate Adenosine Monophosphate min min Fig.2 Chromatograms of Nucleotides Peak
Hydrocortisone Sodium Phosphate 3.5 1.0 0.5 1 μg/ml 3.0 2.5 25 ng/ml 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min Fig.1 Chromatograms of Hydrocortisone
Adenosine Triphosphate Adenosine Monophosphate min Fig.2 Chromatograms of Nucleotides min Peak
Adenosine Triphosphate Adenosine Monophosphate 0.0 1.0 2.0 3.0 4.0 5.0 6.0 min Fig.2 Chromatograms of Nucleotides 0.0 1.0 2.0 3.0 4.0 5.0 6.0 min Peak Asymmetry Peak 1 Peak 2 1.39 1.14 5.10 1.49 Instrument
mastro_nakamen三校.ai
Hydrocortisone Sodium Phosphate 3.5 1.0 0.5 1 μg/ml 3.0 2.5 25 ng/ml 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 min Fig.1 Chromatograms of Hydrocortisone
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HILIC ILIC BEH BEH 009 9 0 5 009 ihon Waters K.K. HILIC HILIC HILIC MS Sub-µm 009 ihon Waters K.K. HILIC? HILIC - Hydrophilic Interaction Chromatography 990 * HILIC (> 80%) *Alpert A. J. J.Chromatogr.
カ9 ラム順相系用分析用順相カラムの種類と特長 順相クロマトグラフィーは 逆相では分離が難しい位置異性体の分離などに有用です ワイエムシィの順相カラムには シリカゲルカラムのほか極性基で修飾した充填剤を充填したカラムがあります ラインナップ 製品名 細孔径粒子径 (nm)(μm) 使用 ph 範囲
汎用分析用カラム順相系 順相カラムの種類と特長 8,9 YMC-Pack SIL, YMC-Pack SIL-6, YMC-Pack C, YMC-Pack Diol-P, YMC-Pack Polyamine Ⅱ 6,7 YMC-Pack H 8 7 カ9 ラム順相系用分析用順相カラムの種類と特長 順相クロマトグラフィーは 逆相では分離が難しい位置異性体の分離などに有用です ワイエムシィの順相カラムには
1 WSV SIR m/z Analyte RT (Min) SIR m/z Cone voltage (V) Ascorbic Acid (C).91 177 2 Thiamine (B1) 1.1 265 5 Nicotinic Acid (B3) 1.27 124 15 Pyridoxal (
ACQUITY UPLC H-Class ACQUITY QDa Mark E. Benvenuti, Dimple Shah, and Jennifer A. Burgess Waters Corporation, Milford, MA, USA MS ACQUITY QDa UPLC HPLC UV ACQUITY QDa LC EC 1925/26 CFR 21 HPLC 1 LC-MS ACQUITY
HILIC UPLC /QTof MS Giuseppe Paglia, 1 James Langridge, 2 and Giuseppe Astarita 3 Center for Systems Biology, University of Iceland, Iceland; 2-3. Wat
HILIC UPLC /QTof MS Giuseppe Paglia, James Langridge, 2 and Giuseppe Astarita 3 Center for Systems Biology, University of Iceland, Iceland; 2-3. Waters Corporation, Manchester, UK and Milford, MA, USA
ACQUITY UPC 2 ACQUITY UPC 2 A A+D3 D ml E 10 ml K μm K μm PDA ACQUITY UPC 2 BEH mm, 1.7 μm ACQUITY UPC 2 HSS C 18 SB 3.
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: このマークが付してある著作物は 第三者が有する著作物ですので 同著作物の再使用 同著作物の二次的著作物の創作等については 著作権者より直接使用許諾を得る必要があります (PET) 1 18 1 18 H 2 13 14 15 16 17 He 1 2 Li Be B C N O F Ne 3 4 5 6 7 8 9 10 Na Mg 3 4 5 6 7 8 9 10 11 12 Al Si P
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